• Title/Summary/Keyword: Temperature hardening

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Rapidly Solidified Microstructure and Phase Decomposition of Al-Cr alloys by the Single Roller Method (Single Roller법에 의한 Al-Cr 계 합금의 급냉응고 조직과 상분해)

  • Cho, Soon-Hyoung;Yoon, Eui-Pak
    • Journal of Korea Foundry Society
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    • v.7 no.2
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    • pp.108-113
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    • 1987
  • Al-Cr alloy with composition in the range from 1.5 wt% to 10 wt% Cr were rapidly solidified from the melt by the single roller method. The supersaturated solid solution was obtained up to 6 wt% Cr in Al-Cr alloy for $20{\mu}m$ thickness. Lattice parameter decreased with increasing Cr content at the rate of 0.00456A per wt% Cr up to 6 wt% Cr. Microhardness increased with increasing Cr content at the rate of $10\;Kg/mm^2$ per wt% Cr up to 6 wt% Cr. Microhardness measurements on the Al-6 wt% Cr supersaturated solid solution annealed isothermally showed no sign of age hardening. Decomposition temperature, determined by lattice parameter changes and microhardness changes, was $470^{\circ}C$ for Al-6 wt% Cr supersaturated solid solution. Transmission electron microscopy showed that decomposition within one hour below $400^{\circ}C$ occurred at grain boundaries only, and also the additional decomposition within grains being evident at $450^{\circ}C$ The coarse precipitate structure showed at $500^{\circ}C$ and $550^{\circ}C$, respectively. The coarse precipitate structure is considered $Al_7Cr$.

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Enhancement of Hardness and Moderation of Surface Defects of 14K, 18K Yellow Gold Alloy by Heat Treatment (열처리에 의한 14K, 18K yellow gold alloy의 경도 향상 및 표면 결함 완화)

  • Ahn, Ji-Hyun;Seo, Jin-Kyo;Ahn, Yoeng-Gil;Park, Jong-Wang
    • Journal of Surface Science and Engineering
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    • v.43 no.2
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    • pp.86-90
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    • 2010
  • In this study, we conducted heat treatment on 14K, 18K yellow gold alloy at various temperature conditions for improving their hardness and moderating their surface defects. Also after the heat treatment we used EPMA (Electron Probe Micro Analyzer), XRF (x-ray Fluorescence spectroscopy) for qualitative analysis and OM (optical microscope), SEM (scanning electron microscope) to investigate the changes of surface grain boundary. We used Vickers hardness tester to verify the changes of hardness. After the heat treatment, 14K, 18K gold alloys showed improved hardness and moderated surface defects at specific temperatures and duration.

Dynamic Material Characteristics of Superalloy INCONEL 718 with the Variation of Strain Rates (변형률속도 변화에 따른 INCONEL 718 초내열합금의 동적 물성특성)

  • Song J. H.;Huh H.
    • Proceedings of the Korean Society for Technology of Plasticity Conference
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    • 2005.05a
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    • pp.275-278
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    • 2005
  • INCONEL 718, nickel based superalloy, has good formability, high strength, excellent corrosion resistance and mechanical properties at high temperature. Owing to theses attractive properties, it finds use in applications such as combustion system, turbine engines and nuclear reactors. In such applications, components are typically required to be tolerant of high stress impact loading. This may cause material degradation and lead to catastrophic failure during service operation. In order to design optimal structural parts made of INCONEL 718, accurate understanding of material's mechanical properties, dynamic behavior and fracture characteristic as a function of strain rates are required. This paper concerned with the dynamic material properties of the INCONEL 718 for the various strain rates. The dynamic response of the INCONEL 718 at intermediate strain rate is obtained from the high speed tensile test machine test and at the high strain rate is from the split Hopkinson pressure bar test. Based on the experimental results, the effects of strain rate on dynamic flow stress, work hardening characteristics, strain rate sensitivity and elongation to the failure are evaluated. Experimental results from both quasi-static and high strain rate up to the 5000/sec are interpolated in order to construct the Johnson-Cook model as the constitutive relation that should be applied to simulate and design the structural parts made of INCONEL 718.

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Dynamic Material Characteristics of Superalloy INCONEL 718 with the Variation of Strain Rates (변형률속도 변화에 따른 INCONEL 718 초내열합금의 동적 물성특성)

  • Song J. H.;Huh H.
    • Transactions of Materials Processing
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    • v.14 no.6 s.78
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    • pp.559-564
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    • 2005
  • INCONEL 718, nickel based superalloy, has good formability, high strength, excellent corrosion resistance and mechanical properties at high temperature. Owing to theses attractive properties, it is utilized in applications such as combustion system, turbine engines and nuclear reactors. In such applications, components are typically required to be tolerant of high stress impact loading. This may cause material degradation and lead to catastrophic failure during service operation. Accurate understanding of material's mechanical properties with various strain rates is required in order to guarantee the reliability of structural parts made of INCONEL 718. This paper is concerned with the dynamic material properties of the INCONEL 718 at various strain rates. The dynamic response of the INCONEL 718 at the intermediate strain rate is obtained from the high speed tensile test and at the high strain rate is from the split Hopkinson pressure bar test. The effect of the strain rate on dynamic flow stress, work hardening characteristics, strain rate sensitivity and elongation to the failure is evaluated with the experimental results. Experimental results from both the quasi-static and the high strain rate up to 5000/sec are interpolated in order to construct the Johnson-Cook model as the constitutive relation that should be applied to simulate and design the structural parts made of rNCONEL 718.

Texture Evolution of Extruded AZ80 Mg Alloy under Various Compressive Forming Conditions (AZ80 마그네슘 합금 압출재의 압축 성형조건에 따른 방위특성 분석)

  • Yoon, J.H.;Lee, S.I.;Lee, J.H.;Park, S.H.;Cho, J.H.
    • Transactions of Materials Processing
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    • v.21 no.4
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    • pp.240-245
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    • 2012
  • With the increasing demand for light-weight materials to reduce fuel consumption, the automobile industry has extensively studied magnesium alloys which are light weight metals. The intrinsic poor formability and poor ductility at ambient temperature due to the hexagonal close-packed (HCP) crystal structure and the associated insufficient number of independent slip systems restricts the practical usage of these alloys. Hot working of magnesium alloys using a forging or extrusion enables net-shape manufacturing with enhanced formability and ductility since there are several operative non-basal slip systems in addition to basal slip plane, which increases the workability. In this research, the thermomechanical properties of AZ80 Mg alloy were obtained by compression testing at the various temperatures and strain rates. Optical microscopy and EBSD were used to study the microstructural behavior such as misorientation distribution and dynamic recrystallization. The results were correlated to the hardening and the softening of the alloy. The experimental data in conjunction with a physical explanation provide the optimal conditions for net-shape forging under hot or warm temperatures through control of the grain refinement and the working conditions.

Effect of Subsequent Annealing Temperature on Dynamic Deformation and Fracture Behavior of Submicrocrystalline Al-4.4%Mg Alloy via Equal-Channel Angular Pressing (ECAP 가공된 초미세 결정립 Al-4.4%Mg 합금의 동적 변형 및 파괴거동에 미치는 후-열처리 온도의 영향)

  • Kim, Y.G.;Ko, Y.G.;Shin, D.H.;Lee, C.S.;Lee, S.
    • Proceedings of the Korean Society for Technology of Plasticity Conference
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    • 2008.05a
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    • pp.427-430
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    • 2008
  • The influence of subsequent annealing treatment on the dynamic deformation and the fracture behavior of submicrocrystalline Al-4.4%Mg alloy is investigated in this study. After inducing an effective strain of 8 via equal-channel angular pressing at $200^{\circ}C$, most of the grains are considerably reduced to nearly equiaxed grains of $0.3{\mu}m$ in size. With an increment of various subsequent heat treatments for 1 hour, resultant microstructures are found to be fairly stable at temperatures up to $200^{\circ}C$, suggesting that static recovery will be dominantly operative, whereas grain growth is pronounced above $250^{\circ}C$. The results of tensile tests show that yield and ultimate tensile strength decrease, but elongation-to-failure and strain hardening rate increase with an increase in annealing temperatures. The dynamic deformation and the fracture behavior retrieved with a series of torsional tests are explored with respect to annealed microstructures. Such mechanical response is analyzed in relation to resultant microstructure and fracture mode.

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Application of the full factorial design to modelling of Al2O3/SiC particle reinforced al-matrix composites

  • Altinkok, Necat
    • Steel and Composite Structures
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    • v.21 no.6
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    • pp.1327-1345
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    • 2016
  • $Al_2O_3$/SiC particulate reinforced (Metal Matrix Composites) MMCs which were produced by using stir casting process, bending strength and hardening behaviour were obtained using an analysis of variance (ANOVA) technique that uses full factorial design. Factor variables and their ranges were: particle size $2-60{\mu}m$; the stirring speed 450 rpm, 500 rpm and the stirring temperature $620^{\circ}C$, $650^{\circ}C$. An empirical equation was derived from test results to describe the relationship between the test parameters. This model for the tensile strength of the hybrid composite materials with $R^2$ adj = 80% for the bending strength $R^2$ adj = 89% were generated from the data. The regression coefficients of this model quantify the tensile strength and bending strengths of the effects of each of the factors. The interactions of all three factors do not present significant percentage contributions on the tensile strength and bending strengths of hybrid composite materials. Analysis of the residuals versus was predicted the tensile strength and bending strengths show a normalized distribution and thereby confirms the suitability of this model. Particle size was found to have the strongest influence on the tensile strength and bending strength.

PWSCC growth rate model of alloy 690 for head penetration nozzles of Korean PWRs

  • Kim, Sung-Woo;Eom, Ki-Hyun;Lim, Yun-Soo;Kim, Dong-Jin
    • Nuclear Engineering and Technology
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    • v.51 no.4
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    • pp.1060-1068
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    • 2019
  • This work aims to establish a model of a primary water stress corrosion crack growth rate of Alloy 690 material for the head penetration nozzles of Korean pressurized water reactors. The test material had an inhomogeneous microstructure with bands of fine-grains and intragranular carbides in the matrix of coarse-grains, which was similar to the archive materials of the head penetration nozzles. The crack growth rate was measured from the strain-hardened materials as a function of the stress intensity factor in simulated primary water at various temperatures and dissolved hydrogen contents. The effects of strain-hardening, temperature, and dissolved hydrogen on the crack growth rate were analyzed independently, and were then introduced as normalizing factors in the crack growth rate model. The crack growth rate model proposed in this work provides a key element of the tools needed to assess the progress of a stress corrosion crack when detected in thick-wall Alloy 690 components in Korean reactors.

Performance Evaluation of Water Vapour Adsorption & Desorption Properties of Ceramic Panel and Painting Materials for Humidity Control (습도조절용 세라믹패널 및 도료의 흡·방습성능 평가)

  • Jang, Kun-Young;Ryu, Dong-Woo
    • Journal of the Architectural Institute of Korea Structure & Construction
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    • v.34 no.3
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    • pp.43-52
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    • 2018
  • This study is conducted to evaluate the performance of ceramic panels and painting materials for humidity control which are developed in non-plastic room temperature hardening structure as part of a project to improve a residential environment for the low-income class, rather than the performance of high-priced humidity control materials that are produced with the existing plasticity processing. The testing methods included the measurements of absorption & desoprtion of humidity per material; Mock-up Testing; an evaluation method of comparing the absorption & desoprtion performances of Ecocarat, ceramic panels and painting materials through Living Lab. According to the measurements of absorption & desoprtion per material, ceramic panels, E panel, and ceramic painting material showed 73.3g/m2, 96.6g/m2, and 111.1g/m2, respectively. That is, the performance of humidity control of each material was found to be good in the order of: Ceramic Paint > E panel > Ceramic Panel. According to performance evaluation testing with Mock-up test and Living Lab, Ceramic Paint, Ecocarat, and Ceramic Panels showed better absorption & desoprtion performances in the order.

A Study on the Manufacture of Gas Insulated Switchgear Spacer Using APG Molding Process (APG 주형방식을 이용한 가스절연개폐기용 절연 스페이서 제작에 관한 연구)

  • Lee, Chanyong;Bae, Jaesung;Cho, Han-Gu;Lee, Sangmook;Lee, Jaehyeong
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.35 no.4
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    • pp.386-391
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    • 2022
  • The gas insulation switchgear, which is a device for protecting a power system, cannot be supported by the insulation gas itself in a charge unit stored in a metal container. Therefore, molding technology is required to manufacture a gas insulation switch spacer. The APG method injection molding simulation was performed by applying the variables obtained through the physical properties of an epoxy composite used for manufacturing an insulating spacer to a moldflow software. After varying the temperature conditions of heater in the simulation, the thermal characteristics and the degree of hardening of the spacer were analyzed, based on which the optimum process conditions are presented.