• Title/Summary/Keyword: Temperature control curing

Search Result 142, Processing Time 0.029 seconds

FRACTURE TOUGHNESS OF SELF-CURING DENTURE BASE RESINS WITH DIFFERENT POLYMERIZING CONDITIONS (의치상용 자가중합레진의 중합조건에 따른 파괴인성)

  • Jeong Soo-Yang;Kim Ji-Hye;Yang Byung-Deok;Park Ju-Mi;Song Kwang-Yeob
    • The Journal of Korean Academy of Prosthodontics
    • /
    • v.43 no.1
    • /
    • pp.52-60
    • /
    • 2005
  • Purpose. The intent of this study was to evaluate the effects of curing conditions on self-curing denture base resins to find out proper condition in self-curing resin polymerization. Materials and methods, In this study, 3 commercial self-curing denture base resins are used Vertex SC, Tokuso Rebase and Jet Denture Repair Acrylic. After mixing the self curing resin, it was placed in a stainless steel mold(3$\times$6$\times$60mm). The mold containing the resin was placed under the following conditions: in air at 23$^{\circ}C$; or in water at 23$^{\circ}C$; or in water at 23$^{\circ}C$ under pressure(20psi); or in water at 37$^{\circ}C$ under pressure(20psi) or in water at 50$^{\circ}C$ under pressure(20psi) , or in water at 65$^{\circ}C$ under pressure(20psi), respectively. Also heat-curing denture base resin is polymerized according to manufactures' instructions as control. Fracture toughness was measured by a single edge notched beam(SENB) method. Notch about 3mm deep was carved at the center of the long axis of the specimen using a dental diamond disk driven by a dental micro engine. The flexural test was carried out at a crosshead speed 0.5mm/min and fracture surface were observed under measuring microscope. Results and conclusion . The results obtained were summarized as follows : 1. The fracture toughness value of self-curing denture base resins were relatively lower than that of heat-curing denture base resin. 2. In Vertex SC and Jet Denture Repair Acrylic, higher fracture toughness value was observed in the curing environment with pressure but in Tokuso Rebase, low fracture toughness value was observed but there was no statistical difference. 3. Higher fracture toughness value was observed in the curing environment with water than air but there was no statistical difference. 4. Raising the temperature in water showed the increase of fracture toughness.

Thermal cracking assessment for nuclear containment buildings using high-strength concrete

  • Yang, Keun-Hyeok;Mun, Jae-Sung;Kim, Do-Gyeum;Chang, Chun-Ho;Mun, Ju-Hyun
    • Computers and Concrete
    • /
    • v.26 no.5
    • /
    • pp.429-438
    • /
    • 2020
  • To shorten the construction times of nuclear facility structures, three high-strength concrete mixtures were developed with specific consideration given to their curing temperatures, their economic efficiency, and the practicality of their quality control. This study was conducted to examine the temperature rise profiles of these three concrete mixtures and the potential for early-age thermal cracking in the primary containment vessel of a nuclear reactor with a wall thickness of 1200 mm. The one-layer placement height of the concrete for the primary containment vessel was increased from the conventional 3 m to 3.5 m. A nonlinear finite element analysis (FEA) was conducted using the thermal properties of concrete determined from the isothermal hydration and adiabatic hydration tests, and tuned through comparisons made with temperature rise profiles obtained for 1200-mm-thick mock-up wall specimens cured at temperatures of 5, 20, and 35℃. The hydration heat performance of the three concrete mixtures and their potential to produce thermal cracking in nuclear facilities indicate that the mixtures have considerable potential for practical application to the primary containment vessel of a nuclear reactor at various curing temperatures, fulfilling the minimum requirements of the ACI 301 and minimizing the likelihood of the occurrence of thermal cracks.

Effect of Resorcinol as Free Formaldehyde Scavenger for Fabric Finished with Urea-formaldehyde Precondensate. (Urea-Formaldehyde 수지가공포에 있어 Resorcinol의 유리 Formaldehyde 포착효과)

  • Kang, In-Sook;Kim, Sung-Reon
    • Textile Coloration and Finishing
    • /
    • v.9 no.2
    • /
    • pp.41-49
    • /
    • 1997
  • To control free formaldehyde release from fabric finished with N-methylol compounds, resin finished cotton fabric was treated with resorcinol solution, dried and cured. Factors affecting to control formaldehyde release have been investigated. It was shown that the aftertreatment with resorcinol greatly suppressed the free formaldehyde release. Up to concentration of about 5% of resorcinol, the concentration of resorcinol effected on the control of free and evolved formaldehyde. And at high concentration of resorcinol, however, the concentration became rather insensitive to contol formaldehyde release. Addition of some salt catalysts such as ammonium chloride, zinc nitrate, sodium acetate and ammonium acetate, was effective in decreasing formaldehyde release. Considering the effect on the control of formaldehyde and crease recovery, ammonium acetate was concidered to be the best catalyst. It was observed that the optimum curing temperature for the resorcinol treatment was about 15$0^{\circ}C$, and that the curing time did not affected formaldehyde release over three minutes. Although the treatment of resorcinol had a little adverse effect on crease recovery of resin finished fabric, this effect could be negligible.

  • PDF

Effects of Hardener and Extender Contents on Curing Behavior of Urea-Melamine-Formaldehyde Resin

  • Eom, Young-Geun;XU, Guang-Zhu;Lee, Young-Kyu;Kim, Hyun-Joong
    • Journal of the Korean Wood Science and Technology
    • /
    • v.36 no.5
    • /
    • pp.42-48
    • /
    • 2008
  • This study was conducted to discuss the effects of hardener and extender contents on peak temperature, reaction enthalpy (${\Delta}H$), gelation time, viscosity change, and pH value in three types of UMF (urea-melamine- formaldehyde) resin with the help of perpHecT LogR meter, differential scanning calorimetry (DSC), and advanced rheometric expansion system (ARES), The results indicated that the pH value of Control A steeply decreased to 5,2 in the early stage but relatively remained constant thereafter as in Synthesis 1 and Synthesis 2, The peak temperature and time decreased as well, whereas ${\Delta}H$ and viscosity increased with the increase of hardener content. On the other hand, ${\Delta}H$ was not changed up to the extender content of 5% and then decreased with its further addition, And the pH value and peak temperature showed no change with the increase of extender content at the hardener content of 5% in three types of UMF resin, The effect of hardener content in this experiment, however, appeared more conspicuous in Control A than in the other two types of Synthesis 1 and Synthesis 2, These results might be caused by higher molecular weight with longer chains of methylene ($-CH_2-$) and methylene ($-CH_2-O-CH_2-$) ether bridges or much more branched chains in Control A.

Comparative proteome profiling in the storage root of sweet potato during curing-mediated wound healing (큐어링 후 저장에 따른 고구마 저장뿌리 단백질체의 비교분석)

  • Ho Yong Shin;Chang Yoon Ji;Ho Soo Kim;Jung-Sung Chung;Sung Hwan Choi;Sang-Soo Kwak;Yun-Hee Kim;Jeung Joo Lee
    • Journal of Plant Biotechnology
    • /
    • v.50
    • /
    • pp.1-10
    • /
    • 2023
  • Sweet potato (Ipomoea batatas L. Lam) is an economically important root crop and a valuable source of nutrients, processed foods, animal feeds, and pigment materials. However, during post-harvest storage, storage roots of sweet potatoes are susceptible to decay caused by various microorganisms and diseases. Post-harvest curing is the most effective means of healing wounds and preventing spoilage by microorganisms during storage. In this study, we aimed to identify proteins involved in the molecular mechanisms related to curing and study proteomic changes during the post-curing storage period. For this purpose, changes in protein spots were analyzed through 2D-electrophoresis after treatment at 33℃ (curing) and 15℃ (control) for three days, followed by a storage period of eight weeks. As a result, we observed 31 differentially expressed protein spots between curing and control groups, among which 15 were identified. Among the identified proteins, the expression level of 'alpha-amylase (spot 1)' increased only after the curing treatment, whereas the expression levels of 'probable aldo-keto reductase 2-like (spot 3)' and 'hypothetical protein CHGG_01724 (spot 4)' increased in both the curing and control groups. However, the expression level of 'sporamin A (spot 10)' decreased in both the curing and control treatments. In the control treatment, the expression level of 'enolase (spot 14)' increased, but the expression levels of 'chain A of actinidin-E-64 complex+ (spot 19)', 'ascorbate peroxidase (spot 22)', and several 'sporamin proteins (spot 20, 21, 23, 24, 27, 29, 30, and 31)' decreased. These results are expected to help identify proteins related to the curing process in sweet potato storage roots, understand the mechanisms related to disease resistance during post-harvest storage, and derive candidate genes to develop new varieties with improved low-temperature storage capabilities in the future.

Determination of Proper Application Rate of Curing Compound for Cement Concrete Pavement (콘크리트 포장 양생제의 적정살포량 결정 연구)

  • Kim, Jang-Rak;Suh, Young-Chan;Ahn, Sung-Soon
    • International Journal of Highway Engineering
    • /
    • v.7 no.2 s.24
    • /
    • pp.45-55
    • /
    • 2005
  • It is known that the Q/C(Quality Control) in the early age of portland cement concrete(PCC) pavement gives a huge effect on long term pavement performance. Thus, many studies regarding the construction of PCC pavement have focused on how to assure construction quality at the early age stage. Curing is one of the most important factor in Q/C of PCC pavement. Membrane curing that protects the evaporation of moisture by placing an impermeable layer on the slab surface is the most common practice for curing the PCC pavement. In order to improve the membrane curing practice, the rate of curing compound should be optimized. However, the optimum rate of curing compound considering Korean weather and environmental conditions has not been specified in the pavement construction specifications. In this study, a proper application rate was recommended in terms of minimizing evaporation with several full-scale tests where various rates of curing compound have been applied. Four test sites on the expressway were enlisted during the summer of 2002 and 2003. Application rates tested were in the range of $0. The rate of evaporation, the temperature pattern of the slab and the pulse velocity of concrete surface have been monitored at each test construction. The result from this study showed that the rate of current construction was approximately $160ml/m^2$ and that approximately $400ml/m^2$ of curing application was recommended as the proper rate for minimizing the moisture evaporation.

  • PDF

Comparative analysis of strain according to two wavelengths of light source and constant temperature bath deposition in ultraviolet-curing resin for dental three-dimensional printing (치과 3D 프린팅용 자외선 경화 레진에 광원의 두 가지 파장에 따른 경화 및 항온수조 침적에 따른 변형률의 비교 분석)

  • Kim, Dong-Yeon;Lee, Gwang-Young;Kang, Hoo-Won;Yang, Cheon-Seung
    • Journal of Technologic Dentistry
    • /
    • v.42 no.3
    • /
    • pp.208-212
    • /
    • 2020
  • Purpose: This study aimed to analyze the shrinkage and expansion strain of ultraviolet (UV)-cured resin according to the wavelength of the light source and compare the shrinkage and expansion. Methods: We prepared the mold with according to the ISO 4049 specimen. The size of the circle in the mold was prepared with a height of 6.02 mm and a diameter of 4 mm. UV-curable resin for three-dimensional (3D) printing was injected into the circular mold. The control group was irradiated with a wavelength of 400~405 nm using UV-curing equipment (400 group), and the experimental group was irradiated with a wavelength of 460~465 nm (460 group). Both groups were produced ten specimens. The produced specimen was first measured with a digital micrometer. After the first measurement, the specimen was immersed in a constant temperature water bath for 15 days, after which the second measurement was performed, and the third measurement was taken after 30 days. The measured values were analyzed using the independent sample t-test (α=0.05). Results: In the non-immersion water tank, the contraction was 0.9% in the 400 group and 1.3% in the 460 group. In the constant temperature bath, the expansion was high at -0.4% in the 400 group for 15 days, and the smallest expansion was -0.03% for the 400 group for 30 days. There were significant differences between the two groups (p<0.05). Conclusion: The 400 group had a lower UV resin specimen strain than the 460 group. Therefore, it is recommended to use the wavelength required by the UV-curing resin.

Thermo-rheological behaviors of Phenolic Resins Blended with Petroleum-based Pitches for High Temperature Carbon Composites (석유계 피치가 첨가된 고온 탄소복합재용 페놀수지의 열 유변학적 거동 연구)

  • Yang, Jae-Yeon;Kuk, Yun-Su;Seo, Min-Kang;Kim, Byoung-Suhk
    • Composites Research
    • /
    • v.33 no.6
    • /
    • pp.329-335
    • /
    • 2020
  • In this study, the thermo-rheological behaivors of petroleum pitches with different softening points were studied, and a B-stage phenolic resins/petroleum pitches blends were prepared by adding petroleum pitches to the phenolic resins. As a result, the petroleum pitch with different softening points decreased the fluidity of the petroleum pitch as the Quinoline insoluble (QI) content increased and showed the viscous properties of the solid. In addition, the effect of adding petroleum pitches having different softening points on the thermo-rheological properties of phenolic resins was investigated. When petroleum pitch with a high softening point was added, the fluidity of the phenolic resin was reduced, and the hardening behavior was fast. It was possible to control the curing rate and curing behavior of the phenolic resin by adding petroleum pitches of different softening points. Among them, the phenolic resin mixture to which P-Pitch 2 was added has a higher fluidity than other blends under the same curing temperature condition.

The Influence of Walking on Low Back Pain (요통치료에서 보법의 영향)

  • Park, Seohee;Jang, Sang-Cheol;Na, Sam-Sik;An, Hun-Mo
    • Journal of Korean Medical Ki-Gong Academy
    • /
    • v.14 no.1
    • /
    • pp.63-82
    • /
    • 2014
  • This study is aimed to verify effects of Walking in treating hospitalized patients with low back pain in the Korean medicine hospital. The method of this study is choosing patients whose chief complaints were low back pain in the Korean medicine hospital in Gyeonggi Province. People who agreed to take Walking treatment were classified into experimental group and control group. Both experimental group and control group were treated with Korean medicine. In addition, experimental group performed Walking program more often. Changes of temperature difference taken by digital infrared thermal imaging(DITI) were used as measuring tools. The summary of this study's result is as in the following. There was significant difference in the experimental group which performed Walking treatments but not in the control group resulting from examining the change of temperature difference between left and right Yongchon. As known from the results above, Walking program is meaningful in curing the low back pain.

A 3-dimensional Finite Element analysis of the Temperature and Stress Development in Mass Concrete Pier due to Heat of Hydration (매스콘크리트 교각의 수화열에 의한 온도 및 응력 거동에 대한 3차원 유한요소 해석)

  • 주영춘;김은겸;신치범
    • Proceedings of the Korea Concrete Institute Conference
    • /
    • 1998.10b
    • /
    • pp.928-933
    • /
    • 1998
  • The temperature and stress behaviour of mass concrete pier at early ages was analysed based on the finite element method. The pier investigated is a three-dimensional structure of which the cross-sectional shape varies from a circle to an ellipsoid along the longitudinal axis. In order to obtain the transient temperature and stress distributions in the structure, a three dimensional method was adopted, because the structure of this type cannot be modeled accurately by a two-dimensional method. Temperature analysis was performed by taking into consideration of the cement type and content, boundary and environment conditions including the variations of atmospheric temperature and wind velocity. The results of this study may be useful for the temperature control to restrain thermal cracking and the construction management to design the resonable curing method of mass concrete structure.

  • PDF