• Korean Journal of Optics and Photonics
• /
• v.19 no.6
• /
• pp.400-407
• /
• 2008

An Instrument to measure normal spectral emissivity is built using a Fourier Transform-Infrared (FT-IR) spectrometer. The instrument is composed of four main parts, reference blackbody, sample furnace, optics system, and FT-IR spectrometer. Measurement ranges of temperature and wavelength are $200^{\circ}C{\sim}500^{\circ}C$ and $3.5{\mu}m{\sim}20{\mu}m$, respectively. Measured emissivity of the reference blackbody is greater than 0.9993 with combined relative uncertainty less than 0.69%, which can be considered an ideal blackbody. We studied the emissivity of opaque alumina, graphite, anodized aluminum, and steel (IMS 200). It is shown that emissivity increases with the roughness of the steel (IMS 200) surface.

• Journal of the Korean Chemical Society
• /
• v.42 no.1
• /
• pp.28-35
• /
• 1998

Microorganisms such as alga are able to uptake toxic and heavy metal ions. After Cd(Ⅱ) was preconcentrated on the carbon paste electrode constructed by incorporating alga (Anabaena), it was determined with differential pulse anodic stripping voltammetry. A well-defined oxidation peak of Cd(Ⅱ) was obtained at - 0.75 V vs. SCE. We investigated the optimum conditions using the peak, which are the effect of the amount of alga, pH, ionic strength, temperature, and preconcentration time on the preconcentration of Cd(Ⅱ) and that of the reduction time and potential on the reduction of Cd(Ⅱ) preconcentrated. Calibration curve for the determination of Cd(Ⅱ) was linear over the range of $1.0{\times}10^6\;M\;to\;8.0{\times}10^6$\;M (R=0.9978) and the detection limit was $5.0{\times}10^{-7}$\;M. The relative standard deviation was 3.1% (n=6) for $7.0{\times}10^{-6}\;M Cd(Ⅱ). In regeneration of the electrode surface with 0.1 M HCl, the response was reproducible continuously by 10 times.

• Transactions of the Korean Society of Mechanical Engineers A
• /
• v.34 no.1
• /
• pp.43-48
• /
• 2010

The heat sink system for a main board in a network server computer is built on printed circuit board by an anchor structure, mounted by eutectic SnPb solder. The solder creeping is caused by a constant high temperature condition in the computer and it eventually makes fatal failures. The FE model is used to calculate the stress and predict the life of soldered anchor in the computer. In the model, Anand constitutive equation is employed to simulate creep characteristics of solder. The creep test is conducted to verify and calibrate the solder model. A special jig is designed to mitigate the flexure of printed circuit board and to get the creep deformation of solder only in the test. Test results are compared with analysis and calibration is conducted on Anand model's constants. Precise life prediction of soldered anchor in creep condition can be performed by this model.

• Journal of Sensor Science and Technology
• /
• v.16 no.1
• /
• pp.24-32
• /
• 2007

Conductive rubber material was molded in a belt shape to measure respiration. Its resistivity was approximately $0.03{\;}{\Omega}m$ and the resistance-displacement relationship showed a negative exponent. The temperature coefficient was approximately $0.006{\;}k{\Omega}/^{\circ}C$ negligible when practically applied on the abdomen. The conductive rubber belt was applied on a normal male's abdomen with the dimensional change measured during resting breathing. The abdominal signal was differentiated ($F_{m}$) and compared with the accurate standard air flow rate signal ($F_{s}$) obtained by pneumotachometry. $F_{m}$ and $F_{s}$ differed in waveform, but the start and end timings of each breaths were clearly synchronized, demonstrating that the respiratory frequency could be accurately estimated before further processing of $F_{m}$. $F_{m}-F_{s}$ loop showed a nonlinear hysteresis within each breath period, thus 6 piecewise linear approximation was performed, leading to a mean relative error of 14 %. This error level was relatively large for clinical application, though customized calibration seemed feasible for monitoring general variation of ventilation. The present technique would be of convenient and practical application as a new wearable respiratory transducer.

• Transactions of the Korean Society of Mechanical Engineers B
• /
• v.29 no.9 s.240
• /
• pp.1022-1031
• /
• 2005

Temporal behavior of the laser induced incandescence (LII) signal is often used for soot particle sizing, which is possible because the cooling behavior of a laser heated particle is dependent on the particle size. In present study, LII signals of soot particles are modeled using two non-linear coupled differential equations deduced from the energy- and mass-balance of the process. The objective of this study is to obtain an appropriate calibration curve for determining primary particle size by comparing the gated signal ratio and double-exponential curve fitting methods. Not only the effects of laser fluence and gas temperature on the cooling behavior but also heat transfer mechanisms of heated soot particle have been investigated. The second-order exponential curve fitting showed better agreements with the LII signals than the gated signal ratio method which was based on the lust-order exponential curve fit. And the temporal decay rate of the LII signal and primary particle size showed nearly linear relationship, which was little dependent on the laser fluence. And it also could be reconfirmed that vaporization was dominant process of heat loss during first loons after laser pulse, then heat conduction played most important role while thermal radiation had little influence all the time.

• Journal of the Korean Society for Aeronautical & Space Sciences
• /
• v.36 no.12
• /
• pp.1222-1228
• /
• 2008

A small satellite, DubaiSat-1 FM(Flight Model), which is based on SI-200 standard bus platform and scheduled to be launched in 2008, is being developed by Satrec Initiative and EIAST(Emirates Institution for Advanced Science and Technology). The TCS(Thermal Control Subsystem) of DubaiSat-1 FM has been designed to mainly utilize passive thermal control in order to minimize power consumption, but the active control method using heaters has been applied to some critical parts. Also, thermal analysis has been performed for DubaiSat-1's mission orbit using a thermal analysis model. The thermal design is modified and optimized to satisfy the design temperature requirements for all parts according to the analysis result. The thermal control performance of DubaiSat-1 FM is verified by thermal vacuum space simulation, consisting of thermal cycling and thermal balance test. Also, to validate the thermal modeling of DubaiSat-1 FM, comparison of test results with analysis has been performed and model calibration has been completed.

• Korean Journal of Pharmacognosy
• /
• v.41 no.4
• /
• pp.313-318
• /
• 2010

Guibi-tang, a traditional herbal medicine, is used for anti-oxidant, anti-osteoporosis, hemostasis and gastroprotection. To develop an analysis method of simultaneous determination of six compounds, swertisin, decursinol, glycyrrhizin, 6-gingerol, costunolide and decursin in Guibi-tang, a high performance liquid chromatography was used with diode array detector. Six bioactive components were separated on a SHISEIDO $C_{18}$ column ($5\;{\mu}m$, 4.6 mm I.D.${\times}$250 mm) with column temperature $30^{\circ}C$. The gradient elution was composed of water with 0.1% trifluoroacetic acid (TFA) and acetonitrile. UV wavelength was set at 230 nm, 254 nm and 330 nm, respectively. Calibration curve showed good linear regression ($R^2$ > 0.9999). The limits of detection (LOD) and the limits of quantification (LOQ) ranged in 0.03 - 0.23 ${\mu}g/ml$ and 0.08 - $0.70\;{\mu}g/ml$, respectively. The RSD values of intra- and inter-day test were in the range of 0.03 ~ 0.96% and 0.01 ~ 1.46%, respectively. The evaluated results of accuracy test were varied from 92.28% ~ 105.14% with RSD < 1.60%. In conclusion, this developed simultaneous determination method was accuracy and sensitive to the quality evaluation of Guibi-tang.

• Journal of the Korean Institute of Gas
• /
• v.21 no.5
• /
• pp.45-55
• /
• 2017

Release and fire/explosion tests of flammable gas are extremely dangerous. Furthermore, it is difficult to select the site where the experiment can be performed. In these reasons, gas flow analysis(CFD) has been used as much as possible. However, with the opening of the Energy Safety Empirical Research Center in Yeongwol-gun, Gangwon-do in October 2016, it was possible to conduct releases and detection tests of small scale combustible gas as well as large scale / high pressure / ultra low temperature experiments. In this study, LPG leaked after the calibration and placement of the sensor, the sensor detected LPG and the data were visualized as a contour map. And the differences between the actual release(28s, max 3.7[m]) and the analysis were analyzed compared to the FLACS analyzed under the same conditions.

• Natural Product Sciences
• /
• v.17 no.4
• /
• pp.328-336
• /
• 2011

A high-performance liquid chromatography (HPLC) with diode array detector (DAD) method was established for the discrimination of a folk medicine Forsythia suspensa and Forsythia viridissima. Five and three representative metabolites of the lignan and phenolic glycoside classes were selected for the analysis from F. suspensa and F. viridissima, respectively. The optimal chromatographic conditions were obtained on an ODS column (5 ${\mu}m$, $4.6{\times}250$ mm) with the column temperature at $40^{\circ}C$. The mobile phase was composed of methanol and 0.3% acetic acid using an isocratic elution with the flow rate 1 mL/min. Detection wavelength was set at 280 nm. All calibration curves showed good linear regression ($r^2$ > 0.996) within test ranges. Limits of detection (LOD) and limits of quantitation (LOQ) values were lower than 0.096 and 0.291 ${\mu}g/mL$, respectively. The developed method provided satisfactory precision and accuracy with overall intra-day and inter-day variations of 0.07-0.63% and 0.14-0.62%, respectively, and the overall recoveries of 97.79-102.46% for all of the compounds analyzed. In addition, effectiveness of diverse extraction methods was compared to each other for the development of standard analytical method. The verified method was successfully applied to the quantitative determination of representative metabolites in fifty-three commercial F. suspensa samples and fifteen commercial F. viridissima samples from diverse sources. The overall analytical results showed the unequivocal differences in bioactive constituents between F. suspensa and F. viridissima.

• Journal of the Korean Wood Science and Technology
• /
• v.45 no.5
• /
• pp.572-579
• /
• 2017

Determination of the wood content in wood plastic composite (WPC) is crucial to form reliable WPC market. WPC with simple formulation consisting of only two components (wood flour and polypropylene) was examined using thermogravimetric analysis (TGA) and accelerator mass spectrometry (AMS) for determining wood content in the WPC. TGA method using derivative peak temperature (DTp) of polypropylene under low heating rate ($5^{\circ}C/min$) showed more reliable calibration curve and lower error factor compared to method of using the percentage of weight loss of wood flour. In addition, AMS using bio-based carbon content showed greater reliability for the determination of wood content in the WPC in comparison with the TGA method.