• Structural Engineering and Mechanics
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• 제84권6호
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• pp.823-829
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• 2022

This study considered the experimental parameters (Nano-graphene oxide reinforced polycarbonate, GFRP) under low-velocity impact load and vibration analysis. The effect of nano-graphene oxide (NGO) on a polycarbonate-based composite was studied. Two test procedures were adopted to obtain experimental results, vibration analysis. The mechanical tests were performed on damaged and non-damaged specimens to determine the damaging effect on the composite specimens. After the test was carried out, the effect of NGO was measured and damping factors were ascertained experimentally. 0. 2 wt% NGO was determined as the optimum amount that best affected the Vibration Analysis. The experiments revealed that the composite's damping properties were increased by adding the nanoparticles to 0.25 wt% and decreased slightly for the specimens with the highest nanoparticles content. Cyclic sinus loading was applied at a frequency of 3.5 Hz. This paper study the frequency effect of 3.5khz frequency damage on mechanical results. Found that high frequency will worthlessly affect the fatigue life in NGO/polycarbonate composite. In 3.5 Hz frequency, it was chosen to decrease the heat by frequency. Transmission electron microscopy (TEM) micrographs were used to investigate the distribution of NGO on the polycarbonate matrix and revealed a homogeneous mixture of nano-composites and strong bonding between NGO and the polycarbonate which increased the damping properties and decreased vibration. Finally, experimental modal analysis was conducted after the high-velocity impact damage process to investigate the defect on the NGO polycarbonate composites.

• 한국결정성장학회지
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• 제14권2호
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• pp.68-72
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• 2004

Sm 원소가 첨가된 $(Sm/Y)_{1.8}Ba_{2.4}Cu_{3.4}O_{7-x}$[이하 (Sm/Y)1.8] 고온초전도체를 국부용융성장법을 이용해 대기 중에서 용융성장실험을 하였다. 초기 (Sm/Y)1.8 초전도체 시편은 rubber 몰드를 이용해 냉간정수압성형(CIP) 과정을 거쳐 길이 방향 원통형상으로 제조되었다. 이렇게 얻어진 (Sm/Y)1.8 초전도체는 용융온도 및 성장속도에 따라 광학현미경, TEM그리고 SQUID magnetometer를 이용해 미세구조 및 초전도특성을 평가하였다. 이 결과 (Sm/Y)1.8 초전도체의 최적의 용융온도 및 성장속도는 $1085^{\circ}C$에서 3.5mm/hr로 나타났다. 특히 일방향으로 용융성장된 (Sm/Y)1.8 초전도체의 광학현미경 및 TEM에 의하 미세구조 관측 결과, 초전도상인 (Sm/Y)123 matrix내에 비초전도상인 (Sm/Y)211 inclusions이 균질하게 분포되어 있는 것이 관측되었다. 초전도특성을 평가한 결과 용융성장된 (Sm/Y)1.8초전도체는 90K에서 임계온도가 시작되어 77K이상의 온도에서 포화되는 특성을 보였다.

• 대한기계학회:학술대회논문집
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• 대한기계학회 2001년도 춘계학술대회논문집D
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• pp.600-604
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• 2001

The relation between the aerodynamic diameter and some morphological parameters was studied for flame-generated aggregates. $SiO_{2}$ aggregates were generated from $SiCl_{4}$ in premixed methane/air flames. These aggregates were sampled and classified according to their aerodynamic diameter by a cascade impactor; moreover, computer program was developed and tested to find the equivalent area diameter and the fractal dimension of the aggregates. We calculated the parameters from the digitized images of the aggregate TEM micrographs. The aerodynamic diameters of the sampled aggregates were larger than $0.4{\mu}m$ in this experiment. In most cases, fractal dimension of their projection image was very close to 2.0 for these large aggregates. It was found that the equivalent area diameter of these aggregates was approximately three times larger than the Stokes' diameter of them.

• Advanced Composite Materials
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• 제18권4호
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• pp.365-379
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• 2009

Epoxy/S2-glass reinforced composites (SGRPs) infused with Cloisite 30B nanoclays were manufactured using the vacuum assisted resin infusion molding (VARIM) process. Prior to infusion, the matrix and clays were thoroughly mixed using a direct mixing technique (DMT) and a high shear mixing technique (HSMT) to ensure uniform dispersion of the nanoclays. Structures with varying clay contents (1-3 wt%) were manufactured. Both pristine and SGRP nanocomposites were then subjected to mechanical testing. For the specimens manufactured by DMT, the tensile, flexural, and compressive modulus increased with increasing the clay content. Similarly, the tensile, flexural, compressive, interlaminate shear and impact strength increased with the addition of 1 wt% clay: however the trend reversed with further increase in the clay content. Specimens manufactured by HSMT showed superior properties compared to those of nanocomposites containing 1 wt% clay produced by DMT. In order to understand these phenomena a morphological study was conducted. Transmission electron microscopy (TEM) micrographs revealed that HSMT led to better dispersion and changed the nanoclay structure from orderly intercalation to disorderly intercalation giving multi-directional strength.

• 대한용접접합학회:학술대회논문집
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• 대한용접접합학회 2005년도 추계학술발표대회 개요집
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• pp.189-191
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• 2005

Dissimilar joining of AI 6013-T4 alloys and austenite stainless steel was carried out using friction stir welding technique. Microstructures near the weld zone and mechanical properties of the joint have been investigated. Microstructures in the stainless steel side and AI alloy were depended on the thermo-mechanical condition which they received. TEM micrographs revealed that the interface region was composed of the mixed layers of elongated stainless steel and ultra-fine grained AI alloy and intermetallic compound layer which was identified as the $Al_{4}Fe$ with hexagonal close packed structure. Mechanical properties were lower than those of 6013 AI alloy base metal, because tool inserting location was deviated to AI alloy from the butt line, which resulted in the lack of the stirring.

• 한국표면공학회지
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• 제24권3호
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• pp.137-143
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• 1991

The relation between the ion irradiation induced grain growth and the basic parameters sinvolved in ion beam mixing process was studied. TEM micrographs showed that a significant grain growth has been induced by Ar+ irradiation at room temperature. The grain size increases rapidly in low dose region, while it approaches a saturated value in high dose region, and it has close relationship with nuclear energy deposition and thermodynamic properties such as cohesive energy ( Hc) and heat of mixing ( Hm). A model for the grain growth based on the thermal spike induced atomic migration was developed and applied to interpret experimental results.

• 한국전기전자재료학회논문지
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• 제21권2호
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• pp.188-193
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• 2008

Epoxy/Organically Modified Layered Silicate Nanocomposites were prepared by dispersing synthetic layered silicate modified with alkyl ammonium ions. In the dispersing process, the organically modified layered silicate were mixed in epoxy resin with shearing, and aggregation of the silicate were removed by centrifugal separation after mixing epoxy resin and silicates. Micrographs taken by transmission electron microscopy(TEM) indicate that the nanocomposites have a mixed morphology including both parallel silicate layers and exfoliated silicate layers area, As the thermal properties, the glass transition temperature of the nanocomposites was shifted to a higher temperature($+6^{\circ}C$)than pure epoxy. Furthermore, dispersion of OMLS will prevented relative permittivity from increasing at a high temperature above the glass transition temperature.

• Carbon letters
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• 제9권1호
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• pp.17-22
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• 2008

A carbon nanotube (CNT) of diameter ~20 nm has been synthesized by spray pyrolysis of turpentine oil using Ni/Fe catalyst. Pellet of CNTs has been used as a target to produce semiconducting carbon thin film of band gap 1.4 eV. Presence of oxygen pressure in the pulse laser deposition (PLD) chamber helped to control the $sp^3/sp^2$ ratio to achieve the desired band gap. Results are discussed with the help of Raman spectra, SEM TEM micrographs and optical measurements suggest that semiconducting carbon thin film deposited by PLD technique has retained its nanotubes structure except that its diameter has increased from 20 nm to 150 nm.

• 한국재료학회지
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• 제16권10호
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• pp.599-605
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• 2006

N-(3-triethoxysilylpropyl)-1,4-diaminoanthrquinone-2,3-dicarboximide (TESP-DADI), an organic blue pigment, has been prepared and incorporated into silica solid matrix reacting triethyl orthosilicate (TEOS) via sol-gel method. Morphology and microstructure of resulting hybrid pigment were studied employing SEM and TEM. The micrographs and particle size distributions showed that uniform pigment can be obtained employing TEOS-based sol-gel method forming silica core. Particle size distribution of dispersed pigment in water was examined using the technique of dynamic light scattering. The ensuing pigment dispersion ink was subjected to various physicochemical evaluation such as viscosity, surface tension, inkjet stability, storage stability, and color change as inkjet ink using spectrophotometric, and microscopic techniques.

• Bulletin of the Korean Chemical Society
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• 제21권4호
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• pp.383-388
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• 2000

Multiblock copolymers consisting of poly( g-benzyl L-glutamate) (PBLG) as the hydrophobic part and poly(ethylene oxide) (PEO) as the hydrophilic part (GEG) were synthesized and characterized. GEG polymeric micelles were prepared by the dialysis technique. Particle size distributions based on intensity,volume, and number-average were 22.6 $\pm$ 11.9 nm, 23.5 $\pm$ 4.6 nm, and 23.7 $\pm$ 37 nm, respectively. It was observed that par-ticle size and size distribution of GEG polymeric micelles changed significantly with the choice of initial sol-vent. Transmission electron micrographs (TEM) showed the polymeric micelles to be spherically shaped, with sizes ranging from 20 nm to 40 nm in diameter. Fluorescence spectroscopy measurements suggested that GEG block copolymers wereassociated in water to form polymeric micelles, and the critical micelle concentrations (CMC) value of the block copolymers was 0.0094 g/L. Further evidenceof micelle formation of GEG block copolymers and limited mobility of the PBLG chain in the core ohe micelle was obtained with 1 H NMR in D2O.