• The Journal of Korean Institute of Communications and Information Sciences
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• v.21 no.6
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• pp.1576-1586
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• 1996

The subject of this paper is the analysis of a Wire-TEM cell(W-TEM cell) which has an inner wire array rather than a metallic septum;its basic structure is similiar to a NBS TEM cell. To verify improved performances of this W-TEM cell as a standard EM field generator, well-known quasi-static approximations are employed and their resultant ingegral equations are numerically analyzed by moment method. Although the electric field strength of a W-TEM cell is 1.4 dB lower than tht of a NBS TEM cell, the uniformity of EM field patterns in a W-TEM cell is improved. It is also shown that the EM field distortions resulting from loading by the conditing objects under test(loading effects), are decreased considerably. This paper also deals with the investigations about relationship between the EM field distributions and the number of wire composing the inner conductor. Finally, the experimental analysis is performed on the practical model which is built on the basis of the design variables brought out by the theoretical andnumerical analysis.

• Applied Microscopy
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• v.32 no.4
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• pp.311-317
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• 2002

There is great requirement on the TEM specimen preparation method with particle size selectivity as a prerequisite for the quantitative structure analysis on the materials such as gibbsite powder, which generally forms a large agglomerate and shows a variation of transition process depending on their sizes. In this experiment, we made an attempt to give a methodology for the TEM specimen preparation of powder with the size selectivity. After mixing 1 wt% gibbsite powder with ethanol solvent, gibbsite suspension was prepared by application of ball-milling and ultrasonification with addition of 0.25 vol% dispersion agent, Darvan C, which was diluted into distilled water by the ratio 1:19. Appling the static sedimentation method to gibbsite suspension after estimation of the sedimentation time by the measurement of accumulative concentration variation, we acquired TEM specimens with well-dispersed and size selected gibbsite particles in nm scale. Overall picture of each sample was taken by SEM and morphology of each dispersed particle was imaged by TEM. Raw and processed gibbsite powders were also examined by XRD to investigate whether they were suffered from phase change during the process or not.

• Journal of the Korean Institute of Telematics and Electronics A
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• v.33A no.7
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• pp.99-110
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• 1996

In this paper, the analysis o fthe electric field distribution for TEM cell which is matched iwth 50 is performed, and the relations of variables for characteristic impedance are derived. Quasi-static approximations are used to calculate the fiedl strength of the internal field of TEM cell. The results of the improved method for analysis of the electric field is compared with that of R.J. Spigel. and the improved method for characteristic impedance and the results of numerical analysis are shown.

• Bulletin of the Korean Chemical Society
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• v.34 no.3
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• pp.788-792
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• 2013

A shortcoming of using transmission electron microscopy (TEM) for structural analysis via electron diffraction is the relatively large error of the measurements as compared to X-ray diffraction. To reduce these errors, various internal standard methods from earlier studies have been widely used. We developed a new device to facilitate the application of internal standard methods in preparation of TEM grids used for nanopowder analysis. Through the application of a partial mask on the TEM grid, both the internal standards and the research materials can be loaded on the same grid. Through this process, we conducted a TEM analysis that compared synthetic hydroxyapatite (HAp) nanopowder to bone apatite from a bovine femur. We determined that the accuracy of the d-spacing measurements of the HAp and bone powders could be improved to better than 1% after statistical treatments of the experimental data. By applying a quarter mask, we loaded four different nanoparticles on a single TEM grid, with one section designated for the internal standard.

• Applied Microscopy
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• v.46 no.2
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• pp.110-115
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• 2016

Transmission electron microscopy (TEM) is a powerful tool for analyzing a broad range of materials and provides localized information about the microstructure. However, the analysis results are strongly influenced by the quality of the thin foil specimen. Sample preparation for TEM analysis requires considerable skill, especially when the area of interest is small or the material of interest is difficult to thin because of its high hardness and its mechanical instability when thinned. This article selectively reviews recent advances in TEM sample preparation techniques using a tripod polisher. In particular, it introduces two typical types (fl at type and wedge type) of TEM sample preparation and the benefits and drawbacks of each method; finally, a method of making better samples for TEM analysis is suggested.

• The Journal of Korean Institute of Electromagnetic Engineering and Science
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• v.10 no.1
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• pp.63-69
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• 1999

In this paper, we analyze the cutoff frequencies of the TEM Cells by the FDTD, and introduce new boundary condition for the FDTD to identify the modes. Then, we confirm efficiency of the FDTD comparing results in previous papers. We also give our opinion from the results by FDTD to the arguments, which is resulted from different results about cutoff frequencies in the TEM Cells, especially the symmetric TEM Cells.

• Applied Microscopy
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• v.31 no.4
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• pp.315-323
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• 2001

In situ TEM heating experiments utilizing kaolinite powder samples result in the following facts. (1) The water recirculation system adopted in the Gatan's heating holder is required to prevent specimen drift above $500^{\circ}C$. (2) Since the degree of phase changes depends on the thickness of powders below $600^{\circ}C$, examinations of both thin and thick specimens are required. (3) Sample preparation using Mo-grids is required for TEM heating experiments above $900^{\circ}C$. At these temperature ranges the effect of heating rate and holding time on the phase transition process increases drastically, so that a programmed temperature control is required. (4) TEM heating experiments of the embedded powders by epoxy for the cross-sectional view was limited due to the severe epoxy movement during heating above $300^{\circ}C$. Better methods of sample preparation are required to overcome this problem.

• Applied Microscopy
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• v.48 no.2
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• pp.49-53
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• 2018

A successful transmission electron microscope (TEM) analysis is closely related to the preparation of the TEM specimen and should be followed by the suitable TEM specimen preparation depending on the purpose of analysis and the subject materials. In the case of the Si-based anode material, lithium atoms of formed Li silicide were removed due to ion beam and electron beam during TEM specimen preparation and TEM observation. To overcome the problem, we proposed a new technique to make a TEM specimen without the ion beam damage. In this study, two types of test specimens from the Si-based anode material of Li-ion battery were prepared by respectively adopting the only focused ion beam (FIB) method and the new FIB-ultramicrotome method. TEM analyses of two samples were conducted to compare the Ga ion damage of the test specimen.

• The Proceeding of the Korean Institute of Electromagnetic Engineering and Science
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• v.2 no.1
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• pp.37-45
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• 1991

The electromagnetic field distribution within rectangular coaxial transmission lines (RCTL:TEM cells) is calculated using a numerical method. Boundary integral equations(BIE) considering equivalence theorem and extended boundary condition(EBC) in tapered region are used, thereby restricting the operational frequencies (0~130 MHz) below the cell cutoff frequency(130 MHz). The EM fields within NIST TEM cell ($1\times0.6\times2m$) are calculated by this method. The results of the numerical calcuation have a good agreement in the cross-sectional EM field distribution of TEM cell with 2-dimensional analysis results. Based on this method, the first cutoff freque- ncy in high order modes in the cell and the electric field polarization are considered.

• Journal of the Korean Society for Geothermal and Hydrothermal Energy
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• v.16 no.3
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• pp.1-7
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• 2020

To provide a design direction for high efficiency thermoelectric module(TEM) dehumidifiers, the effects of design factors of TEM dehumidifiers on dehumidification energy efficiency and performance were numerically investigated. The design factors considered in this study are the TEM capacity, the performance of heat exchangers on the heating and cooling surfaces of the TEM. The higher capacity of the TEM results the higher dehumidification energy efficiency and performance at some operating voltage. The enhanced performance of the heat exchanger on heating surface increased the dehumidification energy efficiency and performance at all the operating voltage. The enhanced performance of the heat exchanger on cooling surface decreased the dehumidification energy efficiency and performance at all operating voltage.