• Title/Summary/Keyword: TEM Journal

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Design & Fabrication of Ferrite-core Loop Antenna for Portable Radio Receiver (휴대형 무선 단말을 위한 FERRITE-CORE LOOP ATENNA의 설계 제작)

  • 권원현;천경준;허선종;박한규
    • The Journal of Korean Institute of Communications and Information Sciences
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    • v.17 no.9
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    • pp.918-926
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    • 1992
  • In this paper, ferrite-core loop antenna for portable radio receiver is designed and its characteristics are analyzed. Antenna is fabricated by inserting the ferrite core inside the planar conductor loop$(10{\times}6{\times}15mm^3)$. Bandwidth and Q factor of fabricated antenna measure 0.55 MHz and 280, respectively. These results show remarkable enhancement compared to the conventional loop antenna having the same physical dimension(BW=1.9MHz, Q=8.14). Experimental results show that the relative gain of the fabricated antenna is about 11 dB higher than that of the conventional antenna.

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The Vertical Growth of CNTs by DC Bias-Assisted PECVD and Their Field Emission Properties. (플라즈마 화학 기상 증착법에서 DC bias가 인가된 탄소나노튜브의 수직성장과 전계방출 특성)

  • 정성회;김광식;장건익;류호진
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.15 no.4
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    • pp.367-372
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    • 2002
  • The vertically well-aligned carbon nanotubes(CNTs) were successfully grown on Ni coated silicon wafer substrate by DC bias-assisted PECVD(Plasma Enhanced Chemical Vapor Deposition). As a catalyst, Ni thin film of thickness ranging from 15~30nm was prepared by electron beam evaporator method. In order to find the optimum growth condition, the type of gas mixture such as $C_2H_2-NH_3$ was systematically investigated by adjusting the gas mixing ratio at $570^{\circ}C$ under 0.4Torr. The diameter of the grown CNTs was 40~200nm and the diameter of the CNTs increased with increasing the Ni particles size. TEM images clearly showed carbon nanotubes to be multiwalled. The measured turn-on field was $3.9V/\mu\textrm{m}$ and an emission current of $1.4{\times}10^4A/\textrm{cm}^2$ was $7V/\mu\textrm{m}$. The CNTs grown by bias-assisted PECVD was able to demonstrate high quality in terms of vertical alignment, crystallization of graphite and the processing technique at low temperature of $570^{\circ}C$ and this can be applied for the emitter tip of FEDs.

Fast and Efficient FDTD Analysis for Microstrip Structures (마이크로스트립 구조에 대한 빠르고 효율적인 FDTD 해석)

  • 우종우;윤현보
    • The Journal of Korean Institute of Electromagnetic Engineering and Science
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    • v.11 no.8
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    • pp.1297-1304
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    • 2000
  • The full wave method requires a great number of computer memory and lasting long CPU time for the calculation of the discontinuity problems in microstrip structures. While the computation only for the transverse field components at those structures causes the both of time and memory reduction. For the case of the calculating only transverse components for the most of microstrip structures such as low-pass filter, branch coupler and patch antenna the computer memory and running time can be reduced to about 50% and 33%, comparing to the full wave computation. Consequently, the proposed method than that of TEM-mode has an advantages of higher speed and less memory than that of conventional FDTD analysis.

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Preparation and Characteristics of Ceramic Composite Powders Coated with $Al_2O_3$: (III) Composite Powders of $Al_2O_3-ZrO_2$ ($Al_2O_3$로 피복시킨 세라믹 복합분체의 제조 및 특성: (III) $Al_2O_3-ZrO_2$ 복합분체)

  • 현상훈;이지현;송원선
    • Journal of the Korean Ceramic Society
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    • v.29 no.8
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    • pp.667-673
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    • 1992
  • The alumina-zirconia composite powders of core particle ZrO2 coated with Al2O3 were prepared by the hydrolysis-deposition of the mixed aluminum salt solution of Al2(SO4)3-Al(NO3)3-Urea. The effects of hydrolysis reaction and coating parameters on characteristics of coated powders and composites were also investigated. The degree of coating could be estimated from the ratio of tetra-/mono-ZrO2 present at the room temperature after heat-treating coated powders at 120$0^{\circ}C$ and the result of TEM observations. When the content of ZrO2 in the dispersed coating system, the coating time, and the volume ratio of water/solution were 50 mg/g, 180 min, and 5, respectively the coating efficiency was maximum (the ratio of tetra-/mono-ZrO2 was 87/13). The relative densities of coated Al2O3-ZrO2 composites sintered at 1$650^{\circ}C$ for 4 hrs were about 91~98% and the maximum ratio of tetra-/mono-ZrO2 in Al2O3-20wt% ZrO2 composites was 62/38.

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Synthesis and Characterization of Ultrafine $\beta$-SiC Powder by Vapor Phase Reaction (기상합성법에 의한 $\beta$-SiC 초미분말 합성 및 특성)

  • 어경훈;이승호;유용호;소명기
    • Journal of the Korean Ceramic Society
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    • v.35 no.11
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    • pp.1190-1196
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    • 1998
  • Ultrafine ${\beta}$-SiC powders were synthesized by the vapor phase reaction of TMS[Si(CH3)4] in hydrogen The reaction temperature and TMS concentration were varied from 1000 to 1400$^{\circ}C$ and from 1 to 10% respectively. The average particle size and phase of the powders were analyzed by TEM and XRD. Ultrafine ${\beta}$-SiC powders were synthesized above 1000$^{\circ}C$ and the crystallinity of the powders increased with increasing reaction temperature. Shape of the particles were spherical and had average size of about 20 nm which showed no difference as the reaction temperature and TMS concentration increased. From the FT-IR analysis the absorption bands of Si-C of the powders shifted to higher wavenumber as the reaction temperature increased,. Under the condition of total gas flow above 1500cc/min ${\beta}$-SiC and poly-Si powders were obtained simultaneously. The Si-O bond intensity was increased under the condition of total gas flow rate above 1000cc/min which might be due to oxidation formed on poly-Si.

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Microwave Sintering Behavior and Electrical Properties of BaTiO$_3$ Ceramics (BaTiO$_3$ 세라믹의 마이크로파 소성 및 전기적 특성)

  • Bai, Kang;Kim, Ho-Gi
    • Journal of the Korean Ceramic Society
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    • v.35 no.11
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    • pp.1203-1211
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    • 1998
  • The microwave sintered BaTiO3 samples were obtained by using the microwave sintering device which can precisely control the sintering temperature and the sinter time by using IR optical thermometer and PID temperature controller. During microwave sintering the internal temperature of samples were mesur-ed by the optical fiber thermometer to compare the sintering behaviors between microwave- and con-ventionally sintered ones. The former showed the faster rate of grain growth with sintering time and the larger grain size than the latter. Also they showed the similar pattern of dielectric properties with tem-perature changes from 2$0^{\circ}C$ to 16$0^{\circ}C$.

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The Reaction of Internal Electrodes with Bi$_2$O$_3$ in Multilayer ZnO Varistor (적층형 ZnO바리스터의 내부전극과 Bi$_2$O$_3$ 와의 반응)

  • Kim, Young-Jung;Kim, Hwan;Hong, Kook-Sun;Lee, Jong-Kook
    • Journal of the Korean Ceramic Society
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    • v.35 no.11
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    • pp.1121-1129
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    • 1998
  • Reactions between Ag-Pd internal electrode materials and{{{{ { {Bi }_{2 }O }_{3 } }} in multilayer chip varistor were in-vestigated. For more than 1 mol%{{{{ { {Bi }_{2 }O }_{3 } }} in varistor composition internal electrode structure was destroyed due to the reaction between internal electrode and{{{{ { {Bi }_{2 }O }_{3 } }} But for typical varistor compositions (below 1 mol% of{{{{ { {Bi }_{2 }O }_{3 } }} content) microstructural changes around the internal electrode were not observed. However SEM-EDS and TEM-EDS analysis showed the uneven distribution of{{{{ { {Bi }_{2 }O }_{3 } }} in the internal electrode which was due to the migration of{{{{ { {Bi }_{2 }O }_{3 } }} to the electorde during sintering. As a results the nonlinear coefficient of multilayer varistor showed very large distribution as well as the breakdown voltage.

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Properties of Working Electrodes with Diamond Blends in Dye Sensitized Solar Cells

  • Choi, Minkyoung;Noh, Yunyoung;Song, Ohsung
    • Journal of the Korean Ceramic Society
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    • v.52 no.5
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    • pp.384-388
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    • 2015
  • We prepared blocking layers by adding 0.0 ~ 0.6 wt% nano diamond blends (DBs) to $TiO_2$ blocking layers to improve the energy conversion efficiencies (ECEs) of dye sensitized solar cells (DSSCs). TEM and micro-Raman spectroscopy were used to characterize the microstructure and phases of DBs, respectively. Optical microscopy and FE-SEM were used to analyze the microstructure of the $TiO_2$ blocking layer with DBs. UV-VIS-NIR spectroscopy was used to determine the absorbance of the working electrodes. A solar simulator and a potentiostat were used to determine the photovoltaic properties and the impedance of the DSSCs with DBs. From the results of the DBs analysis, we determined a 6.97 nm combination of nano diamonds and graphite. We confirmed that ECE increased from 5.64 to 6.48 % when the added DBs increased from 0.0 to 0.2 wt%. This indicates that the effective surface area and electron mobility increased when DBs were added to the $TiO_2$ blocking layer. Our results indicate that the ECE of DSSCs can be enhanced by adding an appropriate amount of DBs to the $TiO_2$ blocking layers.

Synthesis and Characterization of CoFe2O4/SiO2 using Cobalt Precursors from Recycling Waste Cemented Carbide (폐 초경합금에서 추출된 Co를 이용한 CoFe2O4/SiO2 합성 및 특성평가)

  • Yu, Ri;Pee, Jae-Hwan;Kim, Yoo-Jin
    • Journal of the Korean Ceramic Society
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    • v.48 no.5
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    • pp.454-457
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    • 2011
  • We report the preparation of nanocrystalline cobalt ferrite, $CoFe_2O_4$, particles using recycled $Co_3O_4$ and their surface coating with silica using micro emulsion method. Firstly, the $Co_3O_4$ powders were separated from waste cemented carbide with acid-base chemical treatment. The cobalt ferrite nanoparticles with the size 10 nm are prepared by thermal decomposition method using recycled $Co_3O_4$. $SiO_2$ was coated onto the $CoFe_2O_4$ particles by the micro-emulsion method. The $SiO_2$-coated $CoFe_2O_4$ particles were studied their physical properties and characterized by X-ray diffraction (XRD), high resolution-transmission electron microscopy (TEM) analysis and CIE Lab value.

Synthesis of One-dimensional Spinel LiMn2O4 Nanostructures as a Positive Electrode in Lithium Ion Battery

  • Lee, Hyun-Wook;Muralidharan, P.;Kim, Do-Kyung
    • Journal of the Korean Ceramic Society
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    • v.48 no.5
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    • pp.379-383
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    • 2011
  • This paper presents the synthesis of one-dimensional spinel $LiMn_2O_4$ nanostructures using a facile and scalable two-step process. $LiMn_2O_4$ nanorods with average diameter of 100 nm and length of 1.5 ${\mu}m$ have been prepared by solid-state lithiation of hydrothermally synthesized ${\beta}$-$MnO_2$ nanorods. $LiMn_2O_4$ nanowires with diameter of 10 nm and length of several micrometers have been fabricated via solid-state lithiation of ${\beta}$-$MnO_2$ nanowires. The precursors have been lithiated with LiOH and reaction temperature and pressure have been controlled. The complete structural transformation to cubic phase and the maintenance of 1-D nanostructure morphology have been evaluated by XRD, SEM, and TEM analysis. The size distribution of the spinel $LiMn_2O_4$ nanorods/wires has been similar to the $MnO_2$ precursors. By control of reaction pressure, cubic 1-D spinel $LiMn_2O_4$ nanostructures have been fabricated from tetragonal $MnO_2$ precursors even below $500^{\circ}C$.