• Title/Summary/Keyword: TEM Journal

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Cutting Technique for Biodegradable Rope using a CW CO2 Laser with TEM00 mode

  • Lee, Dong-Gil;Kim, Seong-Hun;Park, Seong-Wook;Yang, Yong-Su;Xu, Guo-Cheng
    • Journal of Electrical Engineering and Technology
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    • v.7 no.4
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    • pp.576-581
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    • 2012
  • A 23 W continuous wavelength $CO_2$ laser system exited by a high-frequency LCC resonant converter is adapted to cut a biodegradable rope fabricated with polybutylene succinate. As the biodegradable rope consists of three twisted strands, the thickness changes relative to the position of the laser beam and we thus propose a method to determine exact cutting depth. In order to obtain the parameters related to the rope cutting, the experimental and theoretical cutting depths are compared and analyzed for a range of laser heat sources. The melted thickness and groove width of the cut biodegradable rope are also examined. The proposed theoretical cutting depth depends on the incident power and target velocity ratio. From these experimental results, the biodegradable rope with a diameter of 22 mm can be cut with a heat source of 50 J/cm resulting in a melted thickness of 1.96 mm and a groove width of 0.65 mm. The laser system is shown to be perfect tool for the processing of biodegradable rope without the occurrence of raveling.

Assessment of Bacteria Removal Using Silver Ion Absorbed Ceramic Filter

  • Kim, Woo-Hang;Smith, James
    • Journal of Environmental Science International
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    • v.21 no.8
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    • pp.901-907
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    • 2012
  • The objective of this study was to evaluate bacteria removal ability of the metallic silver which was baked silver ion impregnated ceramic filter at heating condition. Silver leaking from baked ceramic filter was tested to sustain bacteria removal for a long time. Silver impregnated ceramic filter could remove E. coli completely at $10^{12}$ MPN/100ml to $10^{13}$ MPN/100ml of influent. However, ceramic filter without silver did not remove E. coli completely under the same condition. After baking, the silver impregnated ceramic filter almost didn't leak out the silver ion from filter. Photo of TEM (Transmission Electron Microscopy) showed that absorbed silver ions remained in ceramic filter after baking process and most of silver were less than 10 nm. According to the increase in the amount of silver in the ceramic filter, removal efficiencies of E. coli were increased but turbidity removal was decreased. It can be accounted that increased removal efficiency of E. coli was from disinfection of silver that is in the ceramic filter. Simulated concentrations of bacteria agree well with the observed experimental effluent concentration data. Moreover, first-order decay coefficients increased to 0.0034/min after silver was added in the ceramic filter. Increase of first-order decay coefficient proves that silver-added ceramic filter can remove bacteria easily.

Fault Analysis of Semiconductor Device (반도체 장치의 결함해석)

  • Park, S.J.;Choi, S.B.;Oh, C.S.
    • Journal of Energy Engineering
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    • v.25 no.1
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    • pp.192-197
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    • 2016
  • We have surveyed on technical method of fault analysis of semiconductor device. Fault analysis of semiconductor should first be found the places of fault spots. For this process they are generally used the testers; EB(emission beam tester), EM(emission microscope), OBIRCH(optical beam induced resistance change method) and LVP(laser voltage probing) etc. Therefore we have described about physical interpretation and technical method in using scanning electron microscope, transmission electron microscope, focused ion beam tester and Nano prober.

Novel Bi2S3/TiO2 Heterogeneous Catalyst: Photocatalytic Mechanism for Decolorization of Texbrite Dye and Evaluation of Oxygen Species

  • Zhu, Lei;Oh, Won-Chun
    • Journal of the Korean Ceramic Society
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    • v.53 no.1
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    • pp.56-62
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    • 2016
  • A heterogeneous $Bi_2S_3/TiO_2$ composite catalyst was synthesized via a green ultrasonic-assisted method and characterized by XRD, SEM, EDX, TEM analysis. The results clearly show that the $TiO_2$ particles were homogenously coated with $Bi_2S_3$ particles, indicating that $Bi_2S_3$ particle agglomeration was effectively inhibited after the introduction of anatase $TiO_2$. The Texbrite BA-L (TBA) degradation rate constant for $Bi_2S_3/TiO_2$ composites reached $8.27{\times}10^{-3}min^{-1}$ under visible light, much higher than the corresponding value of $1.04{\times}10^{-3}min^{-1}$ for $TiO_2$. The quantities of generated hydroxyl radicals can be analyzed by DPCI degradation, which shows that under visible light irradiation, more electron-hole pairs can be generated. Finally, the possible mechanism for the generation of reactive oxygen species under visible-light irradiation was proposed as well. Our result shows the significant potential of $Bi_2S_3$-semiconductor-based $TiO_2$ hybrid materials as catalysts under visible light for the degradation of industry dye effluent substances.

A Contribution to the Pollen Morphology of Hippocastanaceae (칠엽수과(科) 화분(花粉)의 형태학적(形態學的) 연구(硏究))

  • Kim, Kae-Hwan;Aravanopoulos, F.A.;Zsuffa, L.
    • Journal of Korean Society of Forest Science
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    • v.86 no.2
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    • pp.251-258
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    • 1997
  • The pollen morphology of 20 species and one variety of the two genera of Hippocastanaceae was investigated by LM, SEM and TEM. The pollen grains of this family are monads, prolate to subprolate, isopolar, radially symmetrical, 3-colporate or 3-colpate and ora is circular or lolongate. Sculpture pattern is distinctly striate or spinulose, Brae in various directions. Based on the aperture types and sculpture patterns three major pollen types of this family are discernible : hippocastanum, indica, and punduana.

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A Study of Antibacterial Paper Packaging Material Coated with Chitosan-Ag Nanocomposite Prepared by Green Synthesis (키토산-은나노 녹색합성 복합물질을 적용한 항균 기능성 포장지 연구)

  • Kyung, Gyusun;Ko, Seonghyuk
    • Journal of Korea Technical Association of The Pulp and Paper Industry
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    • v.46 no.2
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    • pp.8-15
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    • 2014
  • A novel antibacterial paper coated with chitosan-based silver (Ag) nanocomposite prepared by green synthesis has been investigated for a wide range of application in food, agricultural and medical packaging. Green synthesis of Ag nanoparticles (AgNPs) was carried out by a chemical reaction involving a mixture of chitosan-silver nitrate (AgNO3) in an autoclave at 15 psi, $121^{\circ}C$, for 15-120 sec. AgNPs and their formation in chitosan were confirmed by both UV-Vis spectroscopy and transmission electron microscope (TEM). Fourier transform infrared spectroscopy (FTIR) study showed that free amino groups in chitosan act as an effective reductant and AgNPs stabilizer. Antibacterial test of coated paper with as-prepared chitosan-AgNPs was performed qualitatively against E. coli based on the formation of halo zones around coated papers and it was shown to be effective in suppressing the growth of E. coli with increasing Ag contents in coating layer.

Characterization of Electrospun Nanofibers of Cellulose Nanowhisker/Polyvinyl Alcohol Composites

  • Cho, Mi-Jung;Park, Byung-Dae;Kadla, John F.
    • Journal of the Korean Wood Science and Technology
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    • v.40 no.2
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    • pp.71-77
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    • 2012
  • Cellulose nanowhisker (CNW) isolated from hardwood bleached kraft pulp (HW-BKP) using sulfuric acid hydrolysis was suspended in polyvinyl alcohol (PVA) and electrospun into composites nanofibers. Transmission electron microscopy (TEM) revealed the CNW to be rod-like, approximately of $16.1{\pm}4.6$ nm wide and $194{\pm}61$ nm long, providing an aspect ratio of about 12, with a particle size distribution range of $662.2{\pm}301.2$ nm. Uniform and high quality CNW/PVA composite nanofibers were successfully manufactured by the electrospinning method. As the CNW loading increases, the viscosity of CNW/PVA solutions shows a minimum at 1% CNW level which subsequently results in the smallest diameter (193 nm) of electrospun nanofibers. The average diameter of the nanofibers increased up to 284 nm with increasing CNW loading. These results suggest that the electrospinning method provides a great potential of manufacturing consistent and reliable nanofibers from CNW/PVA solution for the formation of scaffolds with potentials in future application.

Recycling Method of Used Indium Tin Oxide Targets (폐 인듐주석산화물 타겟의 재활용 기술)

  • Lee, Young-In;Choa, Yong-Ho
    • Korean Journal of Materials Research
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    • v.22 no.4
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    • pp.174-179
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    • 2012
  • In this study, we demonstrated a simple and eco-friendly method, including mechanical polishing and attrition milling processes, to recycle sputtered indium tin oxide targets to indium tin oxide nanopowders and targets for sputtered transparent conductive films. The utilized indium tin oxide target was first pulverized to a powder of sub- to a few- micrometer size by polishing using a diamond particle coated polishing wheel. The calcination of the crushed indium tin oxide powder was carried out at $1000^{\circ}C$ for 1 h, based on the thermal behavior of the indium tin oxide powder; then, the powders were downsized to nanometer size by attrition milling. The average particle size of the indium tin oxide nanopowder was decreased by increasing attrition milling time and was approximately 30 nm after attrition milling for 15 h. The morphology, chemical composition, and microstructure of the recycled indium tin oxide nanopowder were investigated by FE-SEM, EDX, and TEM. A fully dense indium tin oxide sintered specimen with 97.4% of relative density was fabricated using the recycled indium tin oxide nanopowders under atmospheric pressure at $1500^{\circ}C$ for 4 h. The microstructure, phase, and purity of the indium tin oxide target were examined by FE-SEM, XRD, and ICP-MS.

Prediction of long-term wind speed and capacity factor using Measure-Correlate-Predict method (측정-상관-예측법을 이용한 장기간 풍속 및 설비이용률의 예측)

  • Ko, Kyung-Nam;Huh, Jong-Chul
    • Journal of the Korean Solar Energy Society
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    • v.32 no.6
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    • pp.37-43
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    • 2012
  • Long-term variations in wind speed and capacity factor(CF) on Seongsan wind farm of Jeju Island, South Korea were derived statistically. The selected areas for this study were Subji, having a year wind data at 30m above ground level, Sinsan, having 30-year wind data at 10m above ground level and Seongsan wind farm, where long-term CF was predicted. The Measure-Correlate-Predict module of WindPRO was used to predict long-tem wind characteristics at Seongsan wind farm. Eachyear's CF was derived from the estimated 30-year time series wind data by running WAsP module. As a result, for the 30-year CFs, Seongsan wind farm was estimated to have 8.3% for the coefficien to fvariation, CV, and-16.5% ~ 13.2% for the range of variation, RV. It was predicted that the annual CF at Seongsan wind farm varied within about ${\pm}4%$.

Investigation of Dispersion Stability of Conductive Nano Ink Using 1-Octanethiol Coated Copper Nano Powders (1-Octanethiol이 코팅된 나노 구리 분말을 이용한 나노 잉크의 분산도에 대한 연구)

  • Cho, Danee;Baik, Jong-Hwan;Park, Joong-Hark;Lee, Caroline Sunyong
    • Journal of the Korean Ceramic Society
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    • v.49 no.5
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    • pp.417-422
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    • 2012
  • Copper nano particles have been considered as the materials for conductive ink due to its good thermal, electrical conductivity and low cost. However, copper nanoparticles oxidize easily, decreasing dispersion stability and electrical conductivity. Therefore, it is important to develop a method to minimize oxidation of copper nano particles to improve its dispersion stability property in copper nano ink. In this study, copper nano particles were coated with 1-Octanethiol VSAM(Vaporized Self Assembled Multilayers) to prevent oxidation and coated copper powders were dispersed in conductive ink successfully by studying its relationship of different chain length of solvents to 1-Octanethiol coating layer to fabricate nano ink. Various alcohol solvents, such as 1-Hexanol, 1-Octanol, and 1-Decanol were used. The coating layer was observed using FESEM and TEM. Furthermore, dispersion of copper nano particles in nano inks, was characterized using Turbiscan analyzer, viscometer, and contact angle measurement tool.