• Title/Summary/Keyword: Synthetic method

Search Result 2,107, Processing Time 0.027 seconds

A Facile Synthetic Method of 2-Oxaxolidinones and 1,3-Oxazine-2-ones, Essential Moieties of New Antiulcer Agent

  • Park, Min-Soo;Lee, Jae-Won
    • Archives of Pharmacal Research
    • /
    • v.16 no.2
    • /
    • pp.158-160
    • /
    • 1993
  • 2-Oxazolidinones and 1,3-oxazine-2-ones, key moieties of new antiulcer agents, were prepared successfully by treating corresponding hydroxyamide with N-bromosuccinimide (NBS) and silveracetate in acetonitrile. From the fact that the methods for the preparation of hydoxy amides are versatile and such amides could be converted to the corresponding 2-oxazolid-iones and 1,3-oxazine-2-one under our reaction condition, we think that our method is very practical one for the preparation of such compounds. In addition, the above synthetic example affords a good evidence of the synthetic applicability of our improved Hofmann rearrangement.

  • PDF

Producing synthetic lightweight aggregates by treating waste TFT-LCD glass powder and reservoir sediments

  • Tang, Chao-Wei
    • Computers and Concrete
    • /
    • v.13 no.3
    • /
    • pp.325-342
    • /
    • 2014
  • The use of lightweight aggregate (LWA) instead of ordinary aggregate may make lightweight aggregate concrete, which possesses many advantages such as lightweight, lower thermal conductivity, and better fire and seismic resistance. Recently the developments of LWA have been focused on using industrial wastes as raw materials to reduce the use of limited natural resources. In view of this, the intent of this study was to apply Taguchi optimization technique in determining process condition for producing synthetic LWA by incorporating waste thin film transition liquid crystal displays (TFT-LCD) glass powder with reservoir sediments. In the study the waste TFT-LCD glass cullet was used as an additive. It was incorporated with reservoir sediments to produce LWA. Taguchi method with an orthogonal array L16(45) and five controllable 4-level factors (i.e., cullet content, preheat temperature, preheat time, sintering temperature, and sintering time) was adopted. Then, in order to optimize the selected parameters, the analysis of variance method was used to explore the effects of the experimental factors on the performances (particle density, water absorption, bloating ratio, and loss of ignition) of the produced LWA. The results showed that it is possible to produce high performance LWA by incorporating waste TFT-LCD glass cullet with reservoir sediments. Moreover, Taguchi method is a promising approach for optimizing process condition of synthetic LWA using recycled glass cullet and reservoir sediments and it significantly reduces the number of tests.

Analysis of Ultrasound Synthetic Transmit Focusing Using Plane Waves (평면파를 이용한 초음파 합성 송신 집속 기법의 해석)

  • Lee, Jong Pil;Song, Jae Hee;Song, Tai-Kyong
    • The Journal of the Acoustical Society of Korea
    • /
    • v.33 no.3
    • /
    • pp.200-209
    • /
    • 2014
  • In this paper, we present a general model for synthetic transmit focusing method using plane waves (STF-PW) of which the properties are investigated through mathematical analysis and compared with those of the conventional focusing method. The analysis results show that STF-PW produces non-diffracting beams in the sense that their main lobe widths do not change with depth. We also present a method for synthesis of plane waves to obtain a desired main lobe width while preventing grating lobe generation and a method for broadening the region over which the non-diffracting property is maintained. The proposed model and analysis results were validated through computer simulations.

Analyses on Environment-friendliness of Root Barrier Materials based on Fish Toxicity Test (어독성 실험에 따른 방근재 친환경 특성 분석)

  • Woo, Ji-Keun;Kim, Sung-Kyun
    • Journal of the Korean Society of Environmental Restoration Technology
    • /
    • v.13 no.4
    • /
    • pp.42-51
    • /
    • 2010
  • The purpose of this study is to analyze the characteristics of environment-friendliness of Root Barrier materials based on comprehensive experiments on harmfulness of Root Barrier materials and fish toxicity of Oryzias latipes mortality to verify eco-toxicity of each method of construction and Root Barrier material, which are to be applied by taking eco-toxicity into account when building ecological flows in upper areas on natural and artificial grounds. As a result, the following conclusions have been reached in this study: 1. In regard of the harmfulness analyzed, each material showed a different result of analytical value in each lab tank. Compared to lab tank, pH (la), DO (lb), T-N (VI) and T-coli (la) were in the same grade, but COD, SS, T-P and F-coli were less than that of control, respectively increased or decreased by material were analyzed. 2. In the experiment of fish toxicity, Barrier sheet was found to have 66.7% of fish mortality, indicating strong fish toxicity. Synthetic rubber system root barrier sheet (20.0%) was analyzed to have medium fish toxicity, while Synthetic resin system root barrier-waterproof sheet (3.3%), Synthetic rubber system membrane root barrier sheet (3.3%) and Synthetic resin system root barrier sheet (0.0%) showed relatively lower mortality and fish toxicity. To sum up such results as found in the experiment mentioned so far, the values of harmfulness and root penetration resistance analyzed were different in each lab tank, but there was absolutely little correlation with the mortality gained from the experiment on fish toxicity. In the experiment of fish toxicity, environment-friendly root barrier materials were analyzed, and it was found that Synthetic resin system root barrier sheet, Synthetic resin system root barrier waterproof sheet and Synthetic rubber system membrane root barrier sheet are highly environment-friendly. In contrast, Synthetic rubber system root barrier sheet was found to have medium-level environment-friendliness. Also, Barrier sheet was analyzed to have low environment-friendliness.

Halo CME mass estimated by synthetic CMEs based on a full ice-cream cone model

  • Na, Hyeonock;Moon, Yong-Jae
    • The Bulletin of The Korean Astronomical Society
    • /
    • v.46 no.1
    • /
    • pp.43.1-43.1
    • /
    • 2021
  • In this study, we suggest a new method to estimate the mass of a halo coronal mass ejection (CME) using synthetic CMEs. For this, we generate synthetic CMEs based on two assumptions: (1) the CME structure is a full ice-cream cone, (2) the CME electron density follows a power-law distribution (ρcme0r-n). The power-law exponent n is obtained by minimizing the root mean square error between the electron number density distributions of an observed CME and the corresponding synthetic CME at a position angle of the CME leading edge. By applying this methodology to 57 halo CMEs, we estimate two kinds of synthetic CME mass. One is a synthetic CME mass which considers only the observed CME region (Mcme1), the other is a synthetic CME mass which includes both the observed CME region and the occulted area larger than 4 solar radii (Mcme2). From these two cases, we derive conversion factors which are the ratio of a synthetic CME mass to an observed CME mass. The conversion factor for Mcme1 ranges from 1.4 to 3.0 and its average is 2.0. For Mcme2, the factor ranges from 1.8 to 5.0 with the average of 3.0. These results imply that the observed halo CME mass can be underestimated by about 2 times when we consider the observed CME region, and about 3 times when we consider the region including the occulted area. Interestingly these conversion factors have a very strong negative correlation with angular widths of halo CMEs.We also compare the results with the CME mass estimated from STEREO observations.

  • PDF

Numerical Experiment on Migration using 45° Wave Equation (45°파동 방정식을 이용한 마이그레이숀 실험)

  • Jang, Hyuk-Jun;Yang, Sung-Jin;Shin, Chang-Soo
    • Economic and Environmental Geology
    • /
    • v.23 no.3
    • /
    • pp.353-358
    • /
    • 1990
  • This paper presents numerical experiments on migration of synthetic seismograms using by $45^{\circ}$ wave equation. The seismograms used are zero-offset seismogram (corresponding to stacked section) on point reflectors, dipping plane reflector, faulted and folded layers. The seismograms are constructed by upward continuation of seismic source wavelets, exploading on subsurface reflection interfaces, to the earth surface. The synthetic seismograms are migrated by downward continuation and imaging. The upward and downward continuations are implemented by solving the $45^{\circ}$ wave equation with the finite-difference method. Migration of the synthetic data used in this study results in relatively accurate reposition of subsurface structures while the synthetic sections are quite different from the structures.

  • PDF

A VSSI-CRL Synthetic Control Chart (VSSI-CRL 합성관리도)

  • Lee Jae-Won;Lim Tae-Jin
    • Journal of the Korean Operations Research and Management Science Society
    • /
    • v.30 no.4
    • /
    • pp.1-14
    • /
    • 2005
  • We propose a VSSI-CRL(Variable Sampling Size and Samplina Interval-Conforming Run length) synthetic control chart in order to improve the statistical characteristics of both the VSSI chart and the CRL synthetic chart. The VSSI-CRL chart utilizes VSSI sampling scheme, but it produces a signal only when the CRI is less than a given limit. An algorithm for calculating the ARL(Average Run length) and ATS(Average Time to Signal) of the VSSI-CRL chart is developed by employing Markov chain method. We present some lemmas for describing the statistical characteristics of the VSSI-CRL chart under in-control state. A procedure for designing the VSSI-CRL chart is proposed based on the lemmas. Extensive comparative studios show that the VSSI-CRL chart is superior to the CRL synthetic chart or the VSSI chart in general, and is comparable to the EWMA chart in ATS performance.

Synthesis and Biological Activity of Fungal Metabolite, 4-Hydroxy-3-(3'-Methyl-2'-Butenyl)-Benzoic Acid

  • Kim, Hye-Jin;Kwon, Ho-Jeong
    • Journal of Microbiology and Biotechnology
    • /
    • v.17 no.3
    • /
    • pp.543-545
    • /
    • 2007
  • 4-Hydroxy-3-(3'-methyl-2'-butenyl)-benzoic acid (HMBA) was previously isolated from Curvularia sp. KF119 as a cell-cycle inhibitor. However, the present study used a novel and practical synthetic method to prepare a large quantity of HMBA. The synthetic HMBA was found to inhibit the cell-cycle progression of HeLa cells with a comparable potency to the natural fungal metabolite. The inhibition of the cell-cycle progression by the synthetic HMBA involved both the activation of $p21^{WAF1}$ and the inhibition of cyclin D1 expression in the cells. Consequently, this new synthetic procedure provides an easy and convenient way to produce or manipulate the original fungal metabolite.

High Compression synthetic High Coding Using Edge Sharpening (에지 선명화에 의한 고압축 Synthetic High 부호화)

  • 정성환;김남철
    • Journal of the Korean Institute of Telematics and Electronics
    • /
    • v.26 no.9
    • /
    • pp.1410-1419
    • /
    • 1989
  • In this paper, we present a new synthetic high coding method which gives high image compression ratio. Given an image, only its low-pass component is transmitted by DCT coding` the high-pass component is not transmitted but synthesized using edge sharpening on the reconstructed low-pass image at the receiver. For the DCT coding which is used to encode the low-pass image, we used an improved version of Cox's variance estimator. Also, introduced are new image quality measures called GSNR and EPR which emphasize perceptual aspects of image quality. Experimental results show that the performance of the proposed synthetic high coding is better in various quality measures than that of Cox's adaptive transform coding. Also, it yields acceptable image quality with neither apparent block effect nor visible granular noise even at high compression ratio of about 30:1.

  • PDF

Analysis and optimization of Wiel-Dobke synthetic testing circuit parameters (Weil-Dobke 합성단락 시험회로의 Parameter 분석과 최적화)

  • Kim, Maeng-Hyun;Rhyou, Hyeong-Kee;Park, Jong-Wha;Koh, Hee-Seog
    • Proceedings of the KIEE Conference
    • /
    • 1995.07b
    • /
    • pp.623-627
    • /
    • 1995
  • This paper describes analysis and optimization of Weil-Dobke synthetic testing circuit parameters, which is efficient and economical test method in high capacity AC circuit breaker. In this paper, analysis of synthetic short-circuit test circuit parameter proposed nondimensional factor that is reciprocal comparison value of circuit parameter and is not related to rated of circuit breaker, in particular, this study induce minimization of required energy of critical TRV generation specified in IEC 56 standards and present optimal design of synthetic short circuit testing facilities.

  • PDF