• Title/Summary/Keyword: Surface microstructure

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Effects of Melting and Rolling Condition of Ti-10wt.%Ta-10wt.%Nb Alloy on Microstructure Variation (용해 및 가공조건 변화가 Ti-10wt.%Ta-10wt.%Nb합금의 미세조직에 미치는 영향)

  • Lee, Doh-Jae;Lee, Kwang-Min;Kim, Min-Ki;Lee, Kyung-Ku
    • Journal of Korea Foundry Society
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    • v.22 no.3
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    • pp.114-120
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    • 2002
  • A new titanium based alloy, Ti-10Ta-10Nb, has designed to examine the improved mechanical properties and biocompatibility. A specimen of titanium alloy was melted in a consumable vacuum arc furnace and homogenized at $1050^{\circ}C$ for 24 h. The effect of hot rolling on microstructure was estimated after rolling at $400^{\circ}C$ and $800^{\circ}C$ respectively. Surface of melted alloy by consumable vacuum arc melting was consisted of rough surface and it was changed to sound surface by coating of $ZrO_2$ slurry on copper mold surface. The hardness of Ti-10Ta-10Nb alloy increased with the amount of${\alpha}+{\beta}$ phase. Ti-10Ta-10Nb alloy showed $Widmanst{\"{a}}ten$ structure by hot rolling at $800^{\circ}C$ and in the rolling ${\beta}-region$ was negligible effects on microstructure refining.

Synthesis of WC-CrN superlattice film by cathodic arc ion plating system

  • Lee, Ho. Y.;Han, Jeon. G.;Yang, Se. H.
    • Journal of Surface Science and Engineering
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    • v.34 no.5
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    • pp.421-428
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    • 2001
  • New WC-CrN superlattice film was deposited on Si substrate (500$\mu\textrm{m}$) using cathodic arc ion plating system. The microstructure and mechanical properties of the film depend on the superlattice period (λ). In the X-ray diffraction analysis (XRD), preferred orientation of microstructure was changed according to various superlattice periods(λ). During the Transmission Electron Microscope analysis (TEM), microstructure and superlattice period (λ) of the WC - CrN superlattice film was confirmed. Hardness and adhesion of the deposited film was evaluated by nanoindentation test and scratch test, respectively. As a result of nanoindentation test, the hardness of WC - CrN superlattice film was gained about 40GPa at superlattice period (λ) with 7nm. Also residual stress with various superlattice period (λ) was measured on Si wafer (100$\mu\textrm{m}$) by conventional beam-bending technique. The residual stress of the film was reduced to a value of 0.2 GPa by introducing Ti - WC buffer layers periodically with a thickness ratio ($t_{buffer}$/$t_{buffer+superlattice}$ ). To the end, for the evaluation of oxidation resistance at the elevated temperature, CrN single layer and WC - CrN superlattice films with various superlattice periods on SKD61 substrate was measured and compared with the oxidation resistance.

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Advancements in Polymer-Filler Derived Ceramics

  • Greil, Peter
    • Journal of the Korean Ceramic Society
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    • v.49 no.4
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    • pp.279-286
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    • 2012
  • Microstructure tailoring of filler loaded preceramic polymer systems offers a high potential for property improvement of Si-based ceramics and composites. Advancements in manufacturing of bulk materials by controlling microstructure evolution during thermal induced polymer-ceramic transforma-tion and polymer-filler reactions will be presented. Rate controlled pyrolysis, multilayer gradient laminate design and surface modification by gas solid reaction are demonstrated to yield ceramic components of high fractional density and superior mechanical properties. Emerging fields of applications are presented.

Microstructure of Zn-Ni Alloy Electrodeposir (아연-니켈합금전착층의 조직특성)

  • 예길촌;최성렬;신현준;안덕수
    • Journal of Surface Science and Engineering
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    • v.21 no.1
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    • pp.10-18
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    • 1988
  • The variation of Composition and the microstructure of Zn-Ni alloy electrodespposits were investigated to the electrolysis conditions chloride bath. The codeposition mechanism is of the equilibrium type in the electrolysis condition of the high temperature(6$0^{\circ}C$)and high flow rate (1.2-3.0m/sec). The(411, 330) perferred orienation was mainly developed in the Zn-Ni electrodeposir with ${\gamma}$-phase structure, while the(422.600) orientation was closely related to the commposition and the structure of the alloy electrodeposit.

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The effect of Er:YAG laser irradiation on the surface microstructure and roughness of $TiO_2$ implant (Er:YAG 레이저 조사가 산화 티타늄 블라스팅 임플란트 표면 미세 구조 및 거칠기에 미치는 영향)

  • An, Jang-Hyuk;Kwon, Young-Hyuk;Park, Joon-Bong;Herr, Yeek;Chung, Jong-Hyuk
    • Journal of Periodontal and Implant Science
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    • v.38 no.1
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    • pp.67-74
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    • 2008
  • Purpose: The aim of this study was to evaluate the effect of Er:YAG laser on microstructure and roughness of $TiO_2$ blasting implant surface. Materials and Methods: Ten $TiO_2$ blasting implant were used in this experiment. One implant was control group, and nine $TiO_2$ blasting implant surfaces were irradiated with Er:YAG laser under 100 mJ/pulse, 140 mJ/pulse, and 180 mJ/pulse condition for 1 min, 1.5 min, and 2 min respectively. Optical interferometer and scanning electron microscopy was utilized to measure roughness and microstructure of specimens. Results: The surface roughness was decreased after Er:YAG laser irradiation in all groups, but there was no significant difference. 100 mJ/pulse and 140 mJ/pulse group did not alter the $TiO_2$ blasting implant surface in SEM study while 180 mJ/pulse group altered the $TiO_2$ blasting implant surface. Implant surfaces showed melting, microfracture and smooth surface in 180 mJ/pulse group. Conclusion: Detoxification of implant surface using Er:YAG laser must be irradiated with proper energy output and irradiation time to prevent implant surface alteration.

Wear characteristics of High Carbon 9CrSi Alloy Steel of Laser Surface Cladding (Laser Surface Cladding 고탄소 9CrSi 합금강의 마모 특성)

  • Yu, Neung-Hui;Gang, Seong-Gun
    • Korean Journal of Materials Research
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    • v.11 no.10
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    • pp.813-819
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    • 2001
  • The microstructure and the distribution of hardness of Co and A1 alloy powder cladding layer in high carbon 9CrSi alloy steel for roll materials cladded by laser surface cladding were investigated. And, for the evaluation of soundness as the roll materials, we examined the wear resistance of the cladding materials with the wear appratus of pin on disc type. The experimental results showed that the microstructure of laser cladding layer was constituted with the clad surface layer, the alloy layer, the heat treatment layer with base metal. The wear resistance of Ni alloy Powder cladding material was superior to that of Co alloy powder cladding material both at the low speed (0.46m/s) and the high speed(0.92m/s). It seemed that the behavior of wear showed the abrasive wear at the early stage and the adhesive wear at the late stage.

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The Change in Diffusion Coefficient and Wear Characteristic in Carbonitriding Layer of SCM415 Steel (침탄질화 처리된 SCM415강의 깊이에 따른 확산 및 마모특성 변화)

  • Lee, Su-Yeon;Youn, Kuk-Tea;Huh, Seok-Hwan;Lee, Chan-Gyu
    • Journal of Surface Science and Engineering
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    • v.44 no.5
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    • pp.207-212
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    • 2011
  • In this study, the change in diffusion coefficient and wear characteristic with depth in the carbonitriding layer of SCM415 steel was discussed. To determine the diffusion coefficient, depth profile of carbon was measured from the surface using the Glow Discharge Spectrometer. In otherwise, measurements of carbide fraction, micro vickers hardness of surface and observation of microstructure have been implemented through the SEM image. $Fe_3$(C,N) layer and effective depth were increased as the time for carbonitriding takes longer. According to wear experiment, the results showed that wear resistance was improved by $Fe_3$(C,N) layer and effective depth.

Surface Analysis Techniques for Studying Optical Degradation of Solar Coatings (태양에너지 박막의 광퇴화 연구를 위한 표면분석)

  • Lee, Kil-Dong
    • Journal of the Korean Solar Energy Society
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    • v.29 no.2
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    • pp.55-61
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    • 2009
  • This paper reviews the state-of-the art in surface analysis techniques for solar coatings. For analyzing solar coatings and interfaces, surface properties were very important factor for obtaining the information related to the optical degradation processes and microstructure. Various types of analytical techniques for chemical composition, microstructure and surface topography analysis of solar coatings were discussed. In addition, the examples of solar selective coating analysis results for applications were demonstrated. Development and analysis technique of solar coating for energy conservation was felt to be necessary at this time.

Preferred Orientation, Microstructure, Surface Morphology and Mechanical Properties of Electrodeposited Copper Foils (電解銅薄의 優先方位, 斷面組織, 表面形態 및 機械的 性質)

  • Kim, Yoon-Keun;Lee, Dong-Nyung
    • Journal of Surface Science and Engineering
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    • v.18 no.3
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    • pp.95-104
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    • 1985
  • A study has been made of preferred orientation, crose sectional microstructure, surface morphology and mechanical properties of copper foils fabricated by electrodeposition on 304 stainless steel plate from copper sulfate baths for high speed plating. The preferred orientation of the copper foils changed from the [110] to the [111] to ture with decreasing bath temperature and increasing cathode current density. The foils with the [110] texture had the field oriented texture type structure and the surface of many asperities grooved approximately perpendicular to the subtrate. A specimen with the [111]+[311] texture had the lower strength than one with the [10] texture, if they were obtained under similar electrolysis conditions.

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