• Corrosion Science and Technology
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• v.7 no.5
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• pp.269-273
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• 2008

It is known that the fluoric resin has the most outstanding properties in the extremely acidic environment of high temperature. However, this resin is the thermal hardening type that needs long time heat treatments above $250^{\circ}C$. It's impossible to use in situ in the extremely acidic environment such as a huge FGD ductworks or industrial chemical tanks. Furthermore, even the natural hardening type fluoric coatings which can be hardened less than $120^{\circ}C$ can not be applied to the highly acidic environmental plants because of its chemical resistance. In this study, new fluoric coatings that has excellent thermal resistance, chemical resistance and corrosion resistance has been developed in order to solve above problems and to be applied to the large plant structures in the field. These newly developed coatings are organic and inorganic composite type that have fluoric rubber(100 wt%), fluoric resin(5~50 wt%), oxalates(5~30 wt%), inorganic fillers mixed with plate-type and bulk-type solids(20~150 wt%), hardeners(0.5~5 wt%), and hardening hasteners(0.1~3 wt%). The best chemical and physical properties of these coatings are acquired by variation of adhesive reinforcement agents, dispersants, leveling agents. Mixing ratios of plate-type and bulk-type inorganic fillers influence the thermal properties, abrasive resistance and chemical infiltration properties of coatings. The mixing control is also very important to have homogeneous surface and removing inner voids of coatings.

• Journal of the Korean institute of surface engineering
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• v.44 no.6
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• pp.246-249
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• 2011

Surface modification before coating nickel by coupling agents and/or etchant of glass did not provide enough adhesive strength of electroless nickel deposits on glass. Effect of heat treatments on hardness as well as adhesion of nickel deposits was studied by using tape test for adhesion, nanoindenter for hardness and glancing angle x-ray diffractometer (GAXRD) for phase characterization. Heat treatment improved hardness as well as adhesion. XRD results give that the improvements of adhesion and hardness are due to the formation of $NiSiO_4$ around the interface between the nickel deposits and the glass and the precipitation of $Ni_3P$ causing precipitation hardening, respectively. The details in effects of heat treatment on adhesion and hardness are described here.

• Transactions of the Korean Society of Machine Tool Engineers
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• v.10 no.1
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• pp.127-132
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• 2001

By the use of a similar numerical method as the forming limit strain by coating method of coated sheet metals is investigated, in which the FEM is applied and J2G(J2-Gotohs Corner Theory) is utilized as the plasticity constitutive equa-tion. Circular bonded sheet metals with dissimilar sheets on both surface planes are stretched in a plane -strain state, with various work-hardening exponent n-values and thicknesses of each layer. Processes of shear-band formation in such com-posite sheets are clearly illustrated. It is concluded that, it the bonded state, the higher limiting strain of one layer is reduced due to the lower limiting strain of the other layer and vice versa, and does not necessarily obey the rule of linear combination of the limiting strain of each layer weighed according thickness.

• Proceedings of the Korean Society of Machine Tool Engineers Conference
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• 2003.04a
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• pp.340-345
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• 2003

By the use of a similar numerical method as that in the previous paper, the forming limit strain by coating method of clad sheet metals is investigated, in which the FEM is applied and J2G(J2-Gotoh's corner theory) is utilized as the plasticity constitutive equation. Clad two-layer sheets and sheets bonded with dissimilar sheets on both surface planes are stretched in a plane-strain state, with various work-hardening exponent n-values and thicknesses of each layer. Processes of shear-band formation in such composite sheets are clearly illustrated. It is concluded that, in the clad state, the higher limiting strain of one layer is reduced due to the lower limiting strain of the other layer and vice versa, and does not necessarily obey the rule of linear combination of the limiting strain of each layer weighted according thickness.

• Journal of the Korea Academia-Industrial cooperation Society
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• v.17 no.4
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• pp.448-453
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• 2016

Erosion and abrasion caused by cavitation damage occur in fluid equipment, such as ships or impellers. Similarly, the equipment damage from noise and vibration can shorten its life. This study analyzed the importance of the parameter characteristics of the process optimization of HVOF (High Velocity Oxygen Fuel spraying), which is generally used in a variety of industries for enhancing the resistibility from the cavitation phenomenon. The surface of the ALBC3 substrate was coated with an amorphous powder as a filler metal according to the experimental design using the Taguchi method, and then the characteristics with each parameter were analyzed using a porosity measurement test. The optimal process conditions was a combustion pressure of 80psi, coating distance of 270mm, gun speed of 200mm/s, and powder feed rate of 25g/min as a result of the HVOF coating by applying the experimental design. The combustion pressure, coating distance and powder feed rate were more than 25% and indicated a similar contribution rate, but the contribution rate of the gun speed was 19%, which was slightly less than the others. The contribution rate with each parameter was only slightly significant. On the other hand, all four parameters were found to be important in the contribution rate aspects of the HVOF coating process.

• Proceedings of the Korean Society of Precision Engineering Conference
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• 2005.10a
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• pp.192-196
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• 2005

Key part of main equipment in a gas turbine may be likely to be damaged due to operation under high temperature, high pressure, high-speed rotation, etc. Accordingly, the cost for maintenance increases and the damaged parts may cause generation to stop. The number of parts for maintenance also increases, but diagnostics technology fur the maintenance actually does not catch up with the demand. Blades are made of precipitation hardening Ni superalloy IN738 and the like for keeping hot strength. The surface of a blade is thermal-sprayed, using powder with main compositions such as Ni, Cr, Al, etc. in order to inhibit hot oxidation. Conventional regular maintenance of the coating layer of a blade is made by FPI (Fluorescent Penetrant Inspection) and MTP (Magnetic Particle Testing). Such methods, however, are complicated and take long time and also require much cost. In this study, defect diagnostics were tested for the coating layer of an industrial gas turbine blade, using an infraredthermography camera. Since the infrared thermography method can check a temperature distribution on a wide range of area by means of non-contact, it can advantageously save expenses and time as compared to conventional test methods. For the infrared thermography method, however, thermo-load must be applied onto a tested specimen and it is difficult to quantify the measured data. To solve the problems, this essay includes description about producing a specimen of a gas turbine blade (bucket), applying thermo-load onto the produced specimen, photographing thermography images by an infrared thermography camera, analyzing the thermography images, and pre-testing for analyzing defects on the coating layer of the gas turbine blade.

• Korean Journal of Materials Research
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• v.4 no.2
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• pp.166-176
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• 1994

Ni base superalloys are composed of solid sohltion hardening elements(Co, Cr. Mo. W and so on) and $\gamma '$ precipitation hardening elements(A1, Ti, Nb, Ta and so on). To Improve the mechanical properties and oxidation resistanre of superalloys, rare earth elements(%r, Hf, Y and so on) are added to the inner substrate, or are used as coating materials. Their pffects on the growth rate and adhes~on of oxide are changed according to the kinds of oxides such as $AI_2O_3$ and $Cr_2O_3$. The effect of yttrium on the oxidation rate, grain size of oxide, internal structure, and crack resistance was investigated for two kinds of Ni-base superalloys. One in AF'115 superalloy containing Hf and the other is MA6000 superalloy containing $Y_2O_3$. They werr owid~zed at high temperature after yttrium surface modification using ion coater. Yttrium coating on the AF115 and MA6000 superalloys results in a marked change in the growth of the inner oxide. For AF115 superalloy, the degree of gram boundary segregation of $Cr_2O_3$, and prefer en^ tial oxidation of Hf are decreased, and the shape of inner oxidation layer was changed from triangle to plate type. For MA6000 superalloy, $Cr_2O_3$ oxide scale was transformed as outer oxidation layer of CrZOI and inner oxidation layer of $Cr_2O_3$.

• Journal of the Korean Wood Science and Technology
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• v.41 no.3
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• pp.221-233
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• 2013

This study was performed to identify the effect of end-coating around pith of heavy timbers of Red pine and Korean pine on high temperature and low humidity drying characteristics. Total drying times were 268 hours, and ranges of final moisture content was investigated that Red Pine 9.2% to 10.8% MC for square and round timber, in case of Korean Pine 15.0% to 22.0% MC for square timber, 12.8% to 20.4% MC for round timber. Moisture content distribution of Red Pine was a uniform, but part of high moisture content was found in Korean Pine. In case of Korean pine, the surface checks were occurred more severe than in case of Red pine, and end-coating treatment were investigated to be ineffective on surface check. The internal checks were only formed on the two timbers. The value of the case hardenings was investigated that the ranges 3.7% to 9.1% for Red pine. In case of Korean pine, on the other hand, the case hardenings presence a few as 20.9% to 35.8%.

• Journal of the Korea Academia-Industrial cooperation Society
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• v.19 no.10
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• pp.339-345
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• 2018

We investigated the curing properties of cured coatings for a multi-focal UV-LED. The coatings are for LEDs that operate at multiple UV wavelengths, unlike conventional single-wavelength UV-LEDs. Using UV-LED light sources with wavelengths of 365, 395, 420, and 450 nm, we analyzed the optical characteristics such as the direction of light flux and light source. We also analyzed the curing characteristics at each UV-LED wavelength to optimize the LED for composite wavelengths. The curing performance state was predicted through computer simulation for when the multiple wavelengths of UV light sources are superimposed, and then actual LEDs were designed and fabricated. To improve the internal high-speed curing, a multi-spot module was fabricated, in which each LED is condensed, and multiple wavelengths are synthesized and condensed at the same position. The adhesive strength, surface hardness, and internal hardness of the curing agent were tested by varying the wavelength combination conditions. The surface hardening and internal hardening were compared and analyzed using a hardness tester and FT-IR analyzer. As a result, the characteristics of the surface and internal hardness were improved by a multi-spot method in which four wavelengths were overlapped in a UV-LED rather than a single wavelength.

• Journal of the Korean institute of surface engineering
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• v.54 no.5
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• pp.230-237
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• 2021

In this study, the influence of silicon contents on the microstructure, mechanical and tribological properties of Ti-Al-Si-N coatings were systematically investigated for application of cutting tools. The composition of the Ti-Al-Si-N coatings were controlled by different combinations of TiAl₂ and Ti₄Si composite target powers using an arc ion plating technique in a reactive gas mixture of high purity Ar and N₂ during depositions. Ti-Al-Si-N films were nanocomposite consisting of nanosized (Ti,Al,Si)N crystallites embedded in an amorphous Si₃N₄/SiO₂ matrix. The instrumental analyses revealed that the synthesized Ti-Al-Si-N film with Si content of 5.63 at.% was a nanocomposites consisting of nano-sized crystallites (5-7 nm in dia.) and a three dimensional thin layer of amorphous Si₃N₄ phase. The hardness of the Ti-Al-Si-N coatings also exhibited the maximum hardness value of about 47 GPa at a silicon content of ~5.63 at.% due to the microstructural change to a nanocomposite as well as the solid-solution hardening. The coating has a low friction coefficient of 0.55 at room temperature against an Inconel alloy ball. These excellent mechanical and tribological properties of the Ti-Al-Si-N coatings could help to improve the performance of machining and cutting tool applications.