• Journal of Powder Materials
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• v.16 no.5
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• pp.358-362
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• 2009

Ti$_{50}$Cu$_{20}$Ni$_{20}$Al$_{10}$ quaternary amorphous alloy was prepared by high-energy ball milling process. A complete amorphization was confirmed for the composition of Ti$_{50}$Cu$_{20}$Ni$_{20}$Al$_{10}$ after milling for 30hrs. Differential scanning calorimetry showed a large super-cooled liquid region ($\Delta$T$_x$ = T$_x$ T$_g$, T$_g$ and T$_x$: glass transition and crystallization onset temperatures, respectively) of 80 K. Prepared amorphous powders of Ti$_{50}$Cu$_{20}$Ni$_{20}$Al$_{10}$ were consolidated by spark-plasma sintering. Densification behavior and microstructure changes were investigated. Samples sintered at higher temperature of 713 K had a nearly full density. With increasing the sintering temperature, the compressive strength increased to fracture strength of 756 MPa in the case of sintering at 733 K, which showed a 'transparticle' fracture. The samples sintered at above 693 K showed the elongation maximum above 2%.

• The Journal of Advanced Prosthodontics
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• v.8 no.3
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• pp.224-228
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• 2016

PURPOSE. This study aimed to investigate whether dentin surface preparation with diamond rotary instruments of different grit sizes affects the shear bond strength of resin-bonded restorations. MATERIALS AND METHODS. The buccal enamel of 60 maxillary central incisors was removed with a low speed diamond saw and wet ground with silicon carbide papers. The polished surfaces of the teeth were prepared with four groups of rotary diamond burs with super-coarse (SC), coarse (C), medium (M), and fine (F) grit sizes. Following surface preparation, 60 restorations were casted with nickel-chromium alloy and bonded with Panavia cement. To assess the shear bond strength, the samples were mounted on a universal testing machine and an axial load was applied along the cement-restoration interface at the crosshead speed of 0.5 mm/min. The acquired data was analyzed with one way ANOVA and Tukey post hoc test (${\alpha}=.05$). RESULTS. The $mean{\pm}SD$ shear bond strengths (in MPa) of the study groups were $17.75{\pm}1.41$ for SC, $13.82{\pm}1.13$ for C, $10.40{\pm}1.45$ for M, and $7.13{\pm}1.18$ for F. Statistical analysis revealed the significant difference among the study groups such that the value for group SC was significantly higher than that for group F (P<.001). CONCLUSION. Dentin surface roughness created by diamond burs of different grit sizes considerably influences the shear bond strength of resin bonded restorations.

• Transactions of the Korean Society of Mechanical Engineers A
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• v.34 no.12
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• pp.1909-1915
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• 2010

The material properties of gas turbine components change during the daily start/stop thermal cycle because of exposure to the hot combustion gas. Recently, single-crystal Ni-based superalloys have been used to manufacture many hot-gas components for gas turbines. However, the user needs to depend on the manufacturer for maintenance issues because of the lack of data required for predicting blade life and material degradation. In this study, we investigate the time-dependent degradation of first-stage blades at various operating facilities to collect the basic data for life assessment and damage analysis. The blade material is a single-crystal Ni-based superalloy, CMSX-4, and the EOH (equivalent operating hours) are 25,000 and 52,000, respectively. We prepared the test specimen directly from used blades and carried out mechanical tests and microstructural observations.

• Transactions of the Korean Society of Mechanical Engineers A
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• v.34 no.10
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• pp.1403-1409
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• 2010

For many years, high-strength nickel-base superalloys have been used to manufacture turbine blades because of their excellent performance at high temperatures. The prediction of fatigue life of superalloys is important for improving the efficiency of the turbine blades. In this study, low cycle fatigue tests are performed for different values of total strain and temperature. The relations between strain energy density and number of cycles before failure occurs are examined in order to predict the low cycle fatigue life of IN738LC super alloy. The results of low cycle fatigue lives predicted by strain energy methods are found to coincide with experimental data and with the results obtained by the Coffin-Manson method.

• Steel and Composite Structures
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• v.36 no.2
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• pp.213-228
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• 2020

Shape Memory Alloys (SMAs) are new materials used in various fields of science and engineering, one of which is civil engineering. Owing to their distinguished capabilities such as super elasticity, energy dissipation, and tolerating cyclic deformations, these materials have been of interest to engineers. On the other hand, the connections of a steel structure are of paramount importance because of their vulnerabilities during an earthquake. Therefore, it is indispensable to find approaches to augment the efficiency and safety of the connection. This research investigates the behavior of steel connections with extended end plates equipped hybridly with 8 rows of high strength bolts as well as Nitinol superelastic SMA bolts. The connections are studied using component method in dual form. In this method, the components affecting the connections behavior, such as beam flange, beam web, column web, extended end plate, and bolts are considered as parallel and series springs according to the Euro-Code3. Then, the nonlinear force- displacement response of the connection is presented in the form of moment-rotation curve. The results obtained from this survey demonstrate that the connection has ductility, in addition to its high strength, due to high ductility of SMA bolts.

• Journal of Powder Materials
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• v.16 no.1
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• pp.9-15
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• 2009

Amorphization and crystallization behaviors of $Ti_{50}Cu_{50}Ni_{20}Al_{10}$ powders during high-energy ball milling and subsequent heat treatment were studied. Full amorphization obtained after milling for 30 h was confirmed by X-ray diffraction and transmission electron microscope. The morphology of powders prepared using different milling times was observed by field-emission scanning electron microscope. The powders developed a fine, layered, homogeneous structure with prolonged milling. The crystallization behavior showed that the glass transition, $T_g$, onset crystallization, $T_x$, and super cooled liquid range ${\Delta}T=T_x-T_g$ were 691,771 and 80 K, respectively. The isothermal transformation kinetics was analyzed by the John-Mehn-Avrami equation. The Avrami exponent was close to 2.5, which corresponds to the transformation process with a diffusion-controlled type at nearly constant nucleation rate. The activation energy of crystallization for the alloy in the isothermal annealing process calculated using an Arrhenius plot was 345 kJ/mol.

• Journal of Powder Materials
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• v.18 no.2
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• pp.141-148
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• 2011

Carbon material shows relatively high strength at high temperature in vacuum atmosphere and can be easily removed as CO or $CO_2$ gas in oxidation atmosphere. Using these characteristics, we have investigated the applicability of carbon mold for precision casting of high melting point metal such as nickel. Disc shape carbon mold with cylindrical pores was prepared and Ni-base super alloy (CM247LC) was used as casting material. The effects of electroless Nickel plating on wettability and cast parameters such as temperature and pressure on castability were investigated. Furthermore, the proper condition for removal of carbon mold by evaporation in oxidation atmosphere was also examined. The SEM observation of the interface between carbon mold and casting materials (CM247LC), which was infiltrated at temperature up to $1600^{\circ}C$, revealed that there was no particular product at the interface. Carbon mold was effectively eliminated by exposure in oxygen rich atmosphere at $705^{\circ}C$ for 3 hours and oxidation of casting materials was restrained during raising and lowering the temperature by using inert gas. It means that the carbon can be applicable to precision casting as mold material.

• Journal of Welding and Joining
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• v.20 no.2
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• pp.82-89
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• 2002

In order to clarify hot cracking phenomena occurred in Inconel 690 welds and it's prevention, in this study, the cracking behavior and the influence of welding variables on cracking in Inconel 690 overlay welds on Mn-Ni-Cr-Mo steel(SA 508 cl.3) for pressure vessel were investigated by using mock-up test. The main results are as follows: The cracks in Inconel 690 overlay welds were mainly generated near the start and the end part of welding beads adjacent to STS 309L welded outside of Inconel 690 welds. Most of the cracks showed typical solidification crack, and also it was assumed that there was possibility of liquation cracking in HAZ. The existence of Nb constituents or concentration of Nb was recognized on the fracture facets of the solidification cracks in the welds by SMAW. Therefore Nb was considered to be the main factor of the solidification cracking. As the weld heat input was more increased and the weld bead length was longer, the extent of cracking was more increased. Moreover the extent of cracking was considerably decreased by changing of welding sequence to the start and the end part of welds. Hot cracking in welds by GTAW was considerably decreased as compared with that of SMAW. And cracks were well generated in the Inconel 690 overlay welds adjacent to 575 309L welds. This means that the hot cracking susceptibility of Inconel 690 welds was largely varied by chemical components and/or compositions of filter metals, base metals and neighboring welds.

• Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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• 2004.07b
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• pp.1258-1261
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• 2004

ACSR전력선의 송전용량 증가를 위해 개발된 증용량저이도 송전선인 STACBUAW(Super Thermal-resistant Aluminum alloy Conductors, aluminum-clad Invar-Reinforced)전선은 초내열 Al도체 및 인바강선의 사용으로 비교적 고온에서의 안정적 운전이 가능하다. 그러나 고온 환경에서 장시간 노출된 STACIR/AW전선의 안정적 관리를 위해서는, 열화 된 STACIR/AW 전선의 인장강도, 각 구성소재의 탄성 계수, 비틀림 계수 둥과 같은 기계적 물성이 장기 운전 모의를 위해 설정된 열화온도, 열화시간 등에 대해 종합적으로 평가될 필요가 있다. 또한 크립 등과 같이 고온응력 부하상태에서의 변형거동과 탄성계수 및 선 팽창계수의 온도의존성 등은 전선의 이도관리와 예측을 위해서도 명확히 규명되어야할 중요한 관리 인자이다. 그러나 현재까지는 이들에 대해 수행한 어떠한 연구결과들도 보고 되어 있지 않은 실정이다. 본 연구에서는 STACIR/AW $410mm^2$ 송전선을 장시간 운전의 모의를 위해 가속열화 시키고 가속열화에 따른 STACIR/AW전선 및 그 구성소재의 강도, 비틀림 특성의 변화를 조사하여 장시간 운전에 따른 STACIR/AW전선의 안정성을 평가하여 보고하고자 하였다.

• Transactions of the Korean Society of Mechanical Engineers A
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• v.35 no.7
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• pp.753-758
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• 2011

The Ni-base super-heat-resistant alloy, GTD-111, is employed in gas turbines because of its high temperature strength and oxidation resistance. It is important to predict the fatigue life of this superalloy in order to improve the efficiency of gas turbines. In this study, low-cycle fatigue tests are performed as variables of total strain range and temperature. The relationship between the strain energy density and number of cycles to failure is examined in order to predict the low-cycle fatigue life of the GTD-111 superalloy. The fatigue life predicted by using the strain-energy methods is found to coincide with that obtained from the experimental data and from the Coffin-Manson method.