• 열처리공학회지
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• 제3권4호
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• pp.10-22
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• 1990

A study has been investigated on the effect of mechanical properties (tension strength, rotary bending fatigue strength, wear resistance, hardness) according to the carbide particle size variation by the treatment of 1) quenching tempering, and 2) quenching, subzero treatment and tempering. The material used in this investigation was a typical bearing steel, high C high Cr, AISI E 52100. The result obtained in this study were as follows : (1) Finer the carbide particle size increasing the hardness and retained austenite in same quenching condition. (2) Finer the carbide particle size reduced the tension and rotary bending fatigue which were resulted from austenite grain growth and carbide precipitation on grain boundry that induced by carbide refine heat treatment. (3) Finer the carbide particel size increasing the wear resistance which were resulted by uniform distribution of carbide and increased hardness induced by microstructural uniform hardenability of matrix. (4) When the carbide particles were refinded, subzero treatment is effective only wear resistance and hardness.

• 한국정밀공학회:학술대회논문집
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• 한국정밀공학회 2003년도 추계학술대회 논문요약집
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• pp.63-63
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• 2003

• 열처리공학회지
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• 제37권3호
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• pp.128-137
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• 2024

In this study, the carburizing heat treatment process used in aircraft gear manufacturing was compared with the general carburizing heat treatment process using AISI 9310 steel. The process of carburizing followed by slow cooling, and then quenching after austenitizing(Process A) showed less compressive residual stress and less retained austenite in the surface layer compared to the process of quenching directly after carburizing(Process B). In prpcess B, there was a large amount of retained austenite when quenched immediately after carburization, and when treated with subzero, martensite rapidly increased and the compressive residual stress increased significantly, but at the same time, there is a risk of cracking due to severe expansion in volume. Therefore, in the case of aviation parts, it is believed that a step-by-step heat treatment cycle was adopted to ensure stability against heat treatment cracks. As a result of the final tempering after sub-zero treatment, the A process specimen showed a deeper effective case depth and HV700 depth and a higher hardness value above HV700 than the B process specimen.

• 한국식품과학회지
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• 제20권2호
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• pp.200-204
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• 1988

생체(生體) 마늘의 영하 조건에서의 저장 가능성을 검토하기 위하여 생체 인편에 대한 내한특성(耐寒特性)을 조사한 결과 마늘 인편의 빙점은 $-4^{\circ}C{\sim}-5^{\circ}C$로 산지별로 차이가 크지 않았으나 수확 후 처리 조건 및 저장 기간의 경과에 따라 다소 차이를 보여 예건전(豫乾前) $-3.5^{\circ}C$, 예건후(豫乾後) $-4.5^{\circ}C$, 저장 5개월 후 $-5.5^{\circ}C$로 나타났다. 그러나 동결치사한 마늘 인편의 빙점(氷點)은 $-2.5^{\circ}C$로 생체조직(生體組織)에 비하여 높았다. 생체(生體)마늘을 $-4^{\circ}C{\sim}-15^{\circ}C$사이의 5개 저장고(貯藏庫)에서 동결치사율(凍結致死率)을 조사(調査)하였던 바 $-4^{\circ}C$구에서는 0%, $-6.5^{\circ}C$구에서는 건전율(率) 80% 치사율(致死率) 20%였으며 $-15^{\circ}C$구에서는 70%의 치사율(致死率)을 나타내고 있어 생체(生體)마늘의 동결치사(凍結致死) 임계온도는 $-6.0^{\circ}C$ 정도로 판단되었다. 저장온도(貯藏溫度) 조건(條件)에 따른 호흡률의 변화는 온도(溫度) 하강($-4^{\circ}C$까지)에 따라 감소하는 경향을 보였고$Q_{10}$값은 $-4.0^{\circ}C{\sim}5.0^{\circ}C$ 범위에서 2, $5^{\circ}C{\sim}15^{\circ}C$에서 3, $15^{\circ}C{\sim}37^{\circ}C$에서 1.2를 보였다. 기존의 저온 저장 조건으로 제시된 ASHRAE의 $0^{\circ}C$, 75% RH, 빙점 $0.8^{\circ}C$는 한국산 마늘의 경우 재검토되어야 할 것으로 사료된다.

• 열처리공학회지
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• 제2권2호
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• pp.33-37
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• 1989

In order to improve hardness uniformity of standard-hardness blocks. experimental procedure was designed using Taguchi Method. For this purpose the following factors were studied: austenitizing temperature, tempering condition, grinding condition, subzero treatment, lapping time, $15{\mu}m$ polishing time, final polishing time. These factors were processed and then ten hardness values were measured on each specimen. SN (signal to noise) ratio for each condition was calculated with standard variations of these values. Finally, from the calculated value of ANOVA on SN ratios, the lapping time was found to be the main factor Better uniformity with longer lapping time implies that residual stress that was formed after quenching is a dominent parameter that affects on the uniformity of hardness. Therefore, step-quenching method was adapted to minimize the residual stress. By this modification of quenching procedure, the hardness uniformity was improved remarkably and the yield ratio was increased from 55% to 88%.

• 한국산학기술학회:학술대회논문집
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• 한국산학기술학회 2003년도 춘계학술발표논문집
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• pp.83-86
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• 2003

SKD11은 자이로 펌프의 로타와 붓싱 재질로 사용되는데, 자이로펌프는 임펠러의 회전이 없고 원판의 기울기 운동으로 흡입과 토출을 반복하는 고압용적식 펌프이다. 이 펌프의 내구성을 향상시키기 위하여 우수한 내압성과 내마모성을 갖는 재질선정이 요구한다. 따라서 현재 가장 널리 사용되고있는 SKD11에 심냉처리를 통하여 미세조직의 개선을 수행하였고, 가스질화처리에 의한 표면경화로 내압성과 내마모성을 증가시키고자 하였다. SKD11의 미세조직 변화를 조사하기 위하여 광학현미경과 X-선 회절기를 사용하여 미세조직 관찰과 상변화를 조사하였으며, Rockwell 경도기틀 사용하여 각 변수에 따른 경도변화를 조사하였다. 연구 결과 기지조직은 모두 마르텐사이트로 나타났으며, 이 이외에 각각의 조건에 따라 크롬탄화물, PFZ, 잔류오스테나이트가 확인되었다. SKD11을 액화질소로 냉각한 후 500℃에서의 템퍼링으로 가장 큰 경도값을 얻을 수 있었다. 또한 가스질화처리에 의하여 표면경도를 크게 증가시킬 수 있었다.

• 열처리공학회지
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• 제9권1호
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• pp.12-18
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• 1996

Austenite(${\gamma}$) grain size, ${\varepsilon}$ martensite volume fraction and damping capacity of Fe-17%Mn alloy have been investigated as a function of solution treatment temperature of $600^{\circ}C$ to $1100^{\circ}C$. With increasing the solution temperature, ${\gamma}$ grain size, ${\varepsilon}$ martensite content and damping capacity are increased, while the hardness is decreased. When ${\gamma}$ grains are small, ${\varepsilon}$ plates grow in only one direction in each ${\gamma}$ grain. However, if the ${\gamma}$ grains are large in accordance with high solution treating temperature, several ${\varepsilon}$ variants with different orientations are formed and intersected each other in each ${\gamma}$ grain. In spite of small ${\varepsilon}$ martensite content, the damping capacity of the specimen which was annealed at $700^{\circ}C$, followed by subzero treatment at $-196^{\circ}C$, is almost equal to that of the specimen annealed at $1000^{\circ}C$ and subsequently quenched to room temperature. From this result it is suggested that the damping capacity of Fe-17%Mn alloy having fine ${\gamma}$ grains is mainly attributed to the movement of ${\gamma}/{\varepsilon}$ interface without the operation of other damping sources such as ${\varepsilon}/{\varepsilon}$ boundaries and stacking faults in ${\varepsilon}$ reported previously.

• 한국주조공학회지
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• 제22권6호
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• pp.281-287
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• 2002

In order to investigate the variation of microstructure and property of the Electro-slag Remelted M2 steel, microstructure observation, hardness, and bending test were performed by using optical microscope. SEM/EDS, rockwell hardness tester, charpy impact tester and bending tester, respectively. It was revealed that the number of inclusions and content of gas elements(S, O, N) in M2 steel fabricated by ESR process decreased markedly compared to those of AIM. It seems to be due to refining effect of ESR process. The volume fraction of carbides in quenched and tempered specimens after austenitizing at 1150$^{\circ}C$ and 1240$^{\circ}C$ was measured. The volume fraction of grain boundary carbides were found to be similar for both specimens. However, The volume fraction of carbides in grain decreased with an increase of austenitizing temperature. When specimen was austenitized at 1150$^{\circ}C$, grain boundary carbides showed needle like morphology. But, the carbides were broken with an increase of austenitizing temperature. The specimen austenitized at 1240$^{\circ}C$ showed higher hardness and lower bending strength compared to that of 1150$^{\circ}C$. As expected, toughness increased with sub-zero quenching treatment.