• Biotechnology and Bioprocess Engineering:BBE
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• 제10권3호
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• pp.212-217
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• 2005

Desorption/ionization on silicon mass spectrometry (DIOS-MS) is a relatively new laser desorption/ionization technique for mass spectrometry without employing an organic matrix. This present study was carried to survey the experimental factors to improve the efficiency of DIOS-MS through electrochemical etching condition in structure and morphological properties of the porous silicon. The porous structure of silicon structure and its properties are crucial for the better performance of DIOS-MS and they can be controlled by the suitable selection of electrochemical conditions. The fabrication of porous silicon and ion signals on DIOS-MS were examined as a function of silicon orientation, etching time, etchant, current flux, irradiation, pore size, and pore depth. We have also examined the effect of pre- and post-etching conditions for their effect on DIOS-MS. Finally, we could optimize the electrochemical conditions for the efficient performance of DIOS-MS in the analysis of small molecule such as amino acid, drug and peptides without any unknown noise or fragmentation.

• 신재생에너지
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• 제2권2호
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• pp.94-101
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• 2006

[ $1m^3$ ] solid hydrate contains up to $200m^3$ of natural gas, depending on pressure and temperature. Such large volume of natural gas hydrate can be utilized to store and transport large quantity of natural gas in a stable condition. So, in the present investigation, experiments carried out for the formation of natural gas hydrate governed by pressure, temperature, and gas compositions, etc.. The results show that the equilibrium pressure of structure II natural gas hydrate) is approximately 65% lower and the solubility is approximately three times higher than structure I methane hydrate). Also, the subcooling conditions of the structure I and II must be above 9K and 11K in order to form hydrate rapidly regardless of gas components, but the pressure increase is more advantageous than the temperature decrease in order to increase the gas consumption. And utilizing nozzles for spraying water in the form of droplets into the natural gas dramatically reduces the hydrate formation time and increases its solubility at the same time.

• 한국전기전자재료학회논문지
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• 제23권9호
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• pp.741-746
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• 2010

Three-dimensionally ordered macro-porous Sn-C composites were prepared by using polystyrene microsphere as a template. The Sn-C composites were composed of well-interconnected pore with circular shape and wall structure with wall thickness of a few tens of nano-meters. This porous three-dimensional structure is readily and uniformly accessible to the electrolyte, which facilitates lithium ion diffusion during charge-discharge reactions. The wall thickness of the composites was increased as the increase of Sn content of the composite. From EDS analysis, it is confirmed that the Sn was dispersed uniformly in Sn-C composites. The capacity was increased as the Sn content increased, which is due to Sn anode with high capacity. The Sn-C composites with high Sn content showed superior cyclic performances. Such enhancement is ascribed to the thick wall thickness and small pore size of the sample with high Sn content. The Sn-C composite with Sn 30 wt% showed relatively high capacity and stable cycle life, however, the stability of the 3-dimensional structure should be enhanced by further work.

• 대한전기학회:학술대회논문집
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• 대한전기학회 1992년도 하계학술대회 논문집 B
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• pp.1218-1220
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• 1992

This paper presents the three section sliding mode control algorithm based on variable structure current controller design in a synchronous frame and indirect field oriented control method, and applies it to the position control of induction motor. This control scheme solves the problem of robustness loss during the reaching phase that occurs in a conventional VSC strategy, and ensures the stable sliding mode and robustness enhancement throughout an entire response. As the performance of a VSI fed induction motor drives depends on the characteristics of inner loop current controller, it is desired that the current controller have the fast tracking and robust nature. Therefore, we introduced the voltage mapping table based on the concept of voltage space vector for variable structure current control, and implemented fully digital control system using 16-bit microcontroller with on-chip peripherals without additional processing circuits. Simulation and experimental results confirm the validity of this control scheme for robust AC servo drive system of VSI fed induction motor.

• Structural Engineering and Mechanics
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• 제63권1호
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• pp.115-124
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• 2017

In this paper, a different technique to predict the effects of soil-structure interaction (SSI) on seismic response of building systems is investigated. The technique use a machine learning algorithm called Support Vector Regression (SVR) with technical and analytical results as input features. Normally, the effects of SSI on seismic response of existing building systems can be identified by different types of large data sets. Therefore, predicting and estimating the seismic response of building is a difficult task. It is possible to approximate a real valued function of the seismic response and make accurate investing choices regarding the design of building system and reduce the risk involved, by giving the right experimental and/or numerical data to a machine learning regression, such as SVR. The seismic response of both single-degree-of-freedom system and six-storey RC frame which can be represent of a broad range of existing structures, is estimated using proposed SVR model, while allowing flexibility of the soil-foundation system and SSI effects. The seismic response of both single-degree-of-freedom system and six-storey RC frame which can be represent of a broad range of existing structures, is estimated using proposed SVR model, while allowing flexibility of the soil-foundation system and SSI effects. The results show that the performance of the technique can be predicted by reducing the number of real data input features. Further, performance enhancement was achieved by optimizing the RBF kernel and SVR parameters through grid search.

• Macromolecular Research
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• 제10권2호
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• pp.60-66
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• 2002

The morphology, dynamic mechanical behavior and fracture behavior of polyetherimide (PEI)/dicyanate semi-interpenetrating polymer networks (semi-IPNs) with a morphology spectrum were analyzed. To obtain the morphology spectrum, we disported PEI particles in the procured dicyanate resin containing 300 ppm of zinc stearate catalyst. The semi-IPNs exhibited a morphology spectrum, which consisted of nodular spinodal structure, dual-phase morphology, and sea-island type morphology, in the radial direction of each dispersed PEI particle due to the concentration gradient developed by restricted dissolution and diffusion of the PEI particles during the curing process of the dicyanate resin. Analysis of the dynamic mechanical data obtained by the semi-IPNs demonstrated that the transition of the PEI-rich phase was shifted toward higher temperature as well as becoming broader because of the gradient structure. The semi-IPNs with the morphology spectrum showed improved fracture energy of 0.3 kJ/$m^2$, which was 1.4 times that of the IPNS having sea-island type morphology. It was found that the partially introduced nodular structure played a crucial role in the enhancement of the fracture resistance of the semi-IPNs.

• 한국세라믹학회지
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• 제28권9호
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• pp.721-729
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• 1991

SnO2-TiO2(Pt or Pd), as raw material for hydrocarbon gas sensors, was prepared by a coprecipitation method. The SnO2-TiO2-based thick film gas sensors were made by screen printing technique. The titanium dioxide synthesized was shown to be anatase structure from XRD peaks and was transformed to rutile structure between 700$^{\circ}C$ and 1000$^{\circ}C$. Titanium dioxide in SnO2-TiO2 thick films devices plays a very important role in the enhancement of the sensitivity to CH4 and C4H10. In the case of SnO2-TiO2(Pt) sensors, titanium dioxide that was rutile structure enhanced the sensitivity of the thick film to CH4. Platinum added to the raw powder at coprecipitation (as chloroplatinic acid VI hydrate) improved the gas sensitivity to hydrocarbon gases. Therefore, it is expected that the SnO2-TiO2(Pt) thick film sensors fabricated in this experiment could be put into practical use as LPG (primary component : C4H10 and C3H8) and LNG (primary component : CH4) sensors.

• 대한전자공학회논문지TC
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• 제41권4호
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• pp.51-58
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• 2004

본 논문에서는 발룬(Balun) 임피던스 트랜스포머(transformer)를 이용한 새로운 구조의 도허티 증폭기를 설계하였다. 도허티 증폭기의 보조 증폭기는 부하변조를 위해 낮은 출력 영역에서 동작이 되지 않도록 설계되며, 일반적으로 보조 증폭기가 동작하지 않는 경우 증폭기의 출력 임피던스는 개방이 된다고 가정한다. 그러나 실제로 구현된 보조 증폭기의 출력 일피던스는 출력단 정합회로의 임피던스 변환 효과에 의해 개방이 아닌 낮은 임피던스 값을 갖게 된다. 본 논문에서는 상기와 같은 보조 증폭기의 특성을 이용하여 새로운 방식의 푸쉬풀 구조 도허티 증폭기를 설계하였다. 제작된 도허티 증폭기는 2개 반송파의 WCDMA 입력 신호에 대하여 출력전력 40㏈m에서 5㎒ 오프셋 주파수 인접채널 누설전력 비율 －37.3㏈c와 23.7%의 효율 특성을 나타내었다.

• Journal of Mechanical Science and Technology
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• 제17권12호
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• pp.2107-2115
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• 2003

A supersonic dual coaxial jet has been employed popularly for various industrial purposes, such as gasdynamic laser, supersonic ejector, noise control and enhancement of mixing. Detailed characteristics of supersonic dual coaxial jets issuing from an inner supersonic nozzle and outer sonic nozzles with various ejection angles are experimentally investigated. Three important parameters, such as pressure ratios of the inner and outer nozzles, and outer nozzle ejection angle, are chosen for a better understanding of jet structures in the present study. The results obtained from the present experimental study show that the Mach disk diameter becomes smaller, and the Mach disk moves toward the nozzle exit, and the length of the first shock cell decreases with the pressure ratio of the outer nozzle. It was also found that the highly underexpanded outer jet produces a new oblique shock wave, which makes jet structure much more complicated. On the other hand the outer jet ejection angle affects the structure of the inner jet structure less than the pressure ratio of the outer nozzle, relatively.

• Nuclear Engineering and Technology
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• 제38권2호
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• pp.139-146
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• 2006

An experimental study was performed to evaluate the effects of surface coating and an enhanced insulation structure on the downward facing boiling process and the critical heat flux on the outer surface of a hemispherical vessel. Steady-state boiling tests were conducted in the Subscale Boundary Layer Boiling (SBLB) facility using an enhanced vessel/insulation design for the cases with and without vessel coatings. Based on the boiling data, CHF correlations were obtained for both plain and coated vessels. It was found that the nucleate boiling rates and the local CHF limits for the case with micro-porous layer coating were consistently higher than those values for a plain vessel at the same angular location. The enhancement in the local CHF limits and nucleate boiling rates was mainly due to the micro-porous layer coating that increased the local liquid supply rate toward the vaporization sites on the vessel surface. For the case with thermal insulation, the local CHF limit tended to increase from the bottom center at first, then decrease toward the minimum gap location, and finally increase toward the equator. This non-monotonic behavior, which differed significantly from the case without thermal insulation, was evidently due to the local variation of the two-phase motions in the annular channel between the test vessel and the insulation structure.