• Proceedings of the Computational Structural Engineering Institute Conference
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• 1998.04a
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• pp.60-67
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• 1998

This paper deals with the development of a variable-node element and its application to the adaptive h-version mesh refinement-recovery for the incompressible viscous flow analysis. The element which has variable mid-side nodes can be used in generating the transition zone between the refined and unrefined elements and efficiently used for construction of a refined mesh without generating distorted elements. A modified Gaussian quadrature is needed to evaluate the element matrices due to the discontinuity of derivatives of the shape functions used for the element. The penalty function method which can reduce the number of independent variables is adopted for the purpose of computational efficiency and the selective reduced integration is carried out for the convection and pressure terms to preserve the stability of solution. For the economical analysis of transient problems, not only the mesh refinement but also the mesh recovery is needed. The numerical examples show that the optimal mesh for the finite element analysis of a wind around the structures can be obtained automatically by the proposed scheme.

• Journal of the Korean Vacuum Society
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• v.8 no.2
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• pp.111-115
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• 1999

The structural characteristics of an epitaxial $BaTiO_3$ film on MgO(001) grown by sputtering were studied as a function of temperature using in-situ, real time synchrotron x-ray scattering experiments. We found that the as-grown film was single c-domain but strained at room temperature and tetragonally distorted with the c-axis normal to the film surface. Interestingly, its lattice parameters were found to be expanded in both the in-plane and the out-of -plane directions, i.e. biaxially, comparing with those of a bulk $BaTiO_3$ . More importantly, as it was heated up to $600^{\circ}C$, the tetragonal structure was kept up through without and any phase transition, which is usually observed in other epitaxial ferroelectric thin films.

• Structural Engineering and Mechanics
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• v.4 no.6
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• pp.601-612
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• 1996

To simulate the large-scale failure evolution with current computational facilities, a simple approach, that catches the essential feature of failure mechanisms, must be available so that the routine use of failure analysis is feasible. Based on the previous research results, a simple analysis procedure is described in this paper for failure simulation. In this procedure, the evolution of localization is represented by a moving surface of discontinuity, and the transition between continuous and discontinuous failure modes are described via the moving jump forms of conservation laws. As a result, local plasticity and damage models, that are formulated based on thermodynamic restrictions, are still valid without invoking higher order terms, and simple integration schemes can be designed for the rate forms of constitutive models. To resolve localized large deformations and subsequent cracking, an efficient structural solution scheme is given for Static and dynamic problems.

• Proceedings of the Computational Structural Engineering Institute Conference
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• 2010.04a
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• pp.314-317
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• 2010

본 논문에서는 p-수렴 천이요소의 층별이론을 사용하여 균열을 갖는 적층판의 팻취보강 효과에 대해 알아보았다. 이 모델의 면내 변위는 각 구간별로 연속인 선형변화로 가정하였고, 두께방향으로의 면외 변위는 일정한 상수로 가정하여 적용하였다. 변위장의 정의는 적분형 르장드로 다항식을 적용하였다. 또한 에너지 방출률법과 VCCT 방법을 사용하여 응력확대계수를 산출하였다. 수치적분은 별도의 외삽법 없이 각층별의 절점에서 방생하는 적분 값을 바로 얻을 수 있는 가우스-로바토 적분법을 사용하여 계산하였으며, 수치예제를 통해 제안된 모델의 정확도와 기존의 3차원 고체요소를 사용한 것보다 동일한 정확도를 얻기 위해 휠씬 적은 요소 및 자유도가 사용됨을 알 수 있었다.

• Transactions on Electrical and Electronic Materials
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• v.13 no.3
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• pp.136-138
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• 2012

The electrical characteristics of complex films composed of poly(ethylene oxide) (PEO) and urea as a function of the urea concentration were examined in this study. Moreover, their structural characteristics were also compared. Depending on the urea concentration, the structural phases were classified as PEO+${\beta}$-phase composite, ${\beta}$-phase+${\alpha}$-phase composites, or ${\alpha}$-phase composite+urea. At urea concentrations below ~0.064 M, the ${\beta}$-phase was dominant in the complex film. Moreover, the conductance increased rapidly with an increase in the urea concentration. For urea concentrations ranging from ~0.064 to ~0.25 M, the ${\beta}$-phase was gradually substituted by the ${\alpha}$-phase. As the film was composed entirely of the ${\alpha}$-phase at urea concentrations greater than ~0.25 M, its conductance was decreased. In this study, the electrical characteristics observed for the different phases are analyzed and discussed.

• Transactions of Materials Processing
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• v.13 no.6 s.70
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• pp.535-539
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• 2004

Although magnesium has high potential for structural material due to the lightweight and high specific strength, the structural application has been limited by the low ductility at room temperature. The reason of the poor ductility is few activated slip systems of magnesium (HCP structure) during deformation. As temperature increases, however, additional non-basal slip systems are incorporated to exhibit higher ductility comparable to aluminum. In the present study, a series of tensile tests of Mg-Al alloy has been carried out to study deformation behavior with temperature variation. Analysis of load relaxation test results based on internal variable approach gave information about relationship between the micromechanical character and corresponding deformation behavior of magnesium. Especially, the material parameter, p representing dislocation permeability through barriers was altered from 0.1 to 0.15 as the non-basal slip systems were activated at high temperature.

• Bulletin of the Korean Chemical Society
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• v.15 no.1
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• pp.64-74
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• 1994

The nonstoichiometric chalcogenides with NaCl-type structure were prepared and the physical and structural properties were studied. The homogeneous range and the structural change were studied based on X-ray powder diffractions using Rietveld-type full-profile fitting technique. Wide homogeneous ranges were observed in Y-S and Y-Se systems, and relatively narrow homogeneous ranges were observed in Yb-S and Yb-Se systems. Both in $Yb_{1-x}S\;and\;Yb_{1-x}Se$, a vacancy ordering transition occurred in (111) plane direction. The ordered superstructure had cubic symmetry(Fm$\bar{3}m) with doubled unit cell "a" parameter compared to the original NaCl-type. The superlattice developed in a continuous second-order transitiion was characterized by the reduced waved vector k= $(a^*+b^*+c^*)/2$. Y-S system had metallic, and YSe, YbSe system had semiconducting properties in their homogeneous ranges. It was observed that the change of electronic transport properties in extended homogeneous range did not depend on the relativeratio of metal to nonmetal, but on the quantities of vacancies.

• Advances in materials Research
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• v.9 no.4
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• pp.311-321
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• 2020

In this study, Mangifera Indica tree sawdust reinforced bisphenol-A aniline based benzoxazine composites were prepared by varying the sawdust from 20 wt% to 45 wt%. Thermogravimetric analysis of composites revealed excellent compatibility between polybenzoxazine and sawdust from the remarkable growth in char yield from 22% (neat resin) to 36% (for highly filled) and glass transition temperature from 151 to 165℃. Ultimate weight loss of the composites evaluated from the Derivatives of TG plots. Limiting oxygen index values of the composites reported considerable growth i.e.,from 28 to 32 along with the increase in filler content. Differential scanning calorimetry results showed that sawdust particles have an insignificant effect on curing temperature (219℃) for the raise in sawdust content. Structure of the sawdust, benzoxazine monomer, polybenzoxazine and composites were studied using Fourier transformation infrared spectroscopy. Overall, polybenzoxazine composites with sawdust as filler showed improved thermal properties when compared with pure polybenzoxazine.

• Journal of the Korean Magnetic Resonance Society
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• v.27 no.1
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• pp.1-4
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• 2023

Transthyretin (TTR) is an indispensable transporter protein of thyroxine and a retinol molecule in humans. TTR has a stable homo-tetrameric structure in its native state, while upon dissociation into monomers, it becomes aggregation-prone and can form an amyloid fibril. Although the amyloidogenic propensity of TTR has been known and investigated since the late 1990s, the structural information regarding TTR's amyloidogenic species is still elusive. Here, we employed high-pressure nuclear magnetic resonance (HP-NMR) approaches on the monomeric variant of TTR (TTR[F87M/L110M]; M-TTR) and observed that it experiences a two-step transition in response to the pressurized condition. Our study demonstrated that M-TTR in an ambient condition has heterogeneous structural features, which is likely related to the amyloidogenic propensity of TTR.

• Progress in Superconductivity and Cryogenics
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• v.25 no.4
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• pp.1-4
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• 2023

Recently, a claim of material, named LK-99 (a lead apatite-based compound), exhibiting a superconducting transition temperature of over 400 K under standard atmospheric pressure, was reported [1, 2]. This claim has generated considerable attention from scientists worldwide. Here, we synthesized five LK-99 samples following the method detailed in the original papers [1, 2], and measured structural and resistivity data for each of these samples. The structure of the synthesized samples (P6₃/m, a=9.82 Å , c=7.34 Å ) was very close to the reported one. Contrary to the report, however, no hint of room-temperature superconductivity was noted from any of the samples. The results of Energy-dispersive X-ray spectroscopy (EDXS) measurements demonstrate that the atomic distribution in the sample was inhomogenous, and unreacted precursors were included in the samples. To investigate the intrinsic superconducting properties of LK-99, we propose to synthesize samples having high structural purity and chemical uniformity.