• Title/Summary/Keyword: Stirring Temperature

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Application of the full factorial design to modelling of Al2O3/SiC particle reinforced al-matrix composites

  • Altinkok, Necat
    • Steel and Composite Structures
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    • v.21 no.6
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    • pp.1327-1345
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    • 2016
  • $Al_2O_3$/SiC particulate reinforced (Metal Matrix Composites) MMCs which were produced by using stir casting process, bending strength and hardening behaviour were obtained using an analysis of variance (ANOVA) technique that uses full factorial design. Factor variables and their ranges were: particle size $2-60{\mu}m$; the stirring speed 450 rpm, 500 rpm and the stirring temperature $620^{\circ}C$, $650^{\circ}C$. An empirical equation was derived from test results to describe the relationship between the test parameters. This model for the tensile strength of the hybrid composite materials with $R^2$ adj = 80% for the bending strength $R^2$ adj = 89% were generated from the data. The regression coefficients of this model quantify the tensile strength and bending strengths of the effects of each of the factors. The interactions of all three factors do not present significant percentage contributions on the tensile strength and bending strengths of hybrid composite materials. Analysis of the residuals versus was predicted the tensile strength and bending strengths show a normalized distribution and thereby confirms the suitability of this model. Particle size was found to have the strongest influence on the tensile strength and bending strength.

A Study on the Effects of Salinity and Washing in on Aerobic Composting of Food Wastes

  • Park, Seok-Hwan
    • Proceedings of the Korean Environmental Health Society Conference
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    • 2004.06a
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    • pp.207-209
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    • 2004
  • This study was performed to estimate the effects of salinity and washing of food wastes on temperature, pH, and salinity in aerobic composting of food wastes. Weight ratios of food wastes to water in washing were 1:0(Control), 1:1(W-1), 1:2(W-2), 1:3(W-3) and 1:4(W-4), respectively. Ratios of food wastes to wood chips in reactor of Control, W-1, W-2, W-3 and W-4 were 5kg:5L, respectively. Reactors were operated for 24 days with 1 hour stirring by 1 rpm and 2 hours aeration per day. The increase in the ratio of food wastes to water used in washing resulted in the decrease of the highest reaction temperature and the elongation of the high temperature reaction period. The lowering of the ratio of food wastes to water used in washing resulted in faster pH increase The final salinities of Control, W-1, W-2, W-3 and W-4 were 0.95%, 0.73%, 0.65%, 0.57% and 0.41%, respectively.

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Effects of Washing of Food Wastes on Aerobic Composting (음식물쓰레기의 세척이 호기성 퇴비화에 미치는 영향)

  • 박석환
    • Journal of Environmental Health Sciences
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    • v.30 no.1
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    • pp.1-6
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    • 2004
  • This study was performed to estimate the effects of washing of food wastes on temperature, pH, weight and volume reduction and salinity in aerobic composting of food wastes. Weight ratios of food wastes to water in washing were 1:0(Control), 1:1 (W-1), 1:2(W-2), 1:3(W-3) and :4(W-4), respectively. Ratios of food wastes to wood chips in reactor of Control, W-1, W-2, W-3 and W-4 were 5 kg:5 1, respectively. Reactors were operated for 24 days with 1 hour stirring by 1 rpm and 2 hours aeration per day. The increase in the ratio of food wastes to water used in washing resulted in the decrease of the highest reaction temperature and the elongation of the high temperature reaction period. The lowering of the ratio of food wastes to water used in washing resulted in faster pH increase and the steady state in the weight reduction rate and the volume reduction rate of composts. The final salinities of Control, W-1, W-2, W-3 and W-4 were 0.95%, 0.73%, 0.65%, 0.57% and 0.41%, respectively.

Effect of variation of Nitrogen Content by Cattle Feces on Aerobic Composting of Food Wastes (우분에 의한 질소함량의 변화가 음식물폐기물의 호기성 퇴비화에 미치는 영향)

  • 박석환;김종오
    • Journal of Environmental Health Sciences
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    • v.26 no.3
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    • pp.38-42
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    • 2000
  • This study was performed to define the effects of the cattle feces on aerobic composting of food wastes in vessel system. Weights of cattle feces added to food wastes of 3kg were 0.25, 0.50, 1.00 and 1.50kg, respectively. Reactors were operated with stirring for 1 hour per day by 1rpm and aeration for 2 hours per day. When the weight of cattle feces was increased, the highest temperature of sample was increased, the duration period of higher temperature was elongated, and the fluctuatio of pH was severs. When the weight of cattle feces was decreased, the final density was increased. The more cattle feces were added, the more porosity was increased, C/N ratio, salinity and conductivity were decreased. There facts denotes that the addition of cattle feces increases the efficiency of composting process and the final product of composting, namely compost.

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Induction Heating of Aluminum Alloys for Thixoforging (Thixoforging 공정을 위한 알루미늄 재료의 유도 가열)

  • 정홍규;강충길
    • Proceedings of the Korean Society for Technology of Plasticity Conference
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    • 1998.03a
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    • pp.107-112
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    • 1998
  • The semi-solid materials(SSMs) fabricated under electric-magnetic stirring condition are necessary to be applicated in the thixoforging process. The optimal reheating conditions to thixoforging process were investigated with changing the reheating time, holding time, reheating temperatures, capacity, and adiabatic material size. In the case of solid fraction fs=50%, the microstructure of SSM (specimen size:d76X 190) at the condition of the first reheating time 4min, holding time lrnin and reheating temperature 350%, the second reheating time 3min, holding time 3min and reheating temperature 575C, the thlrd reheating time lmin, holding time 2min and reheating temperature 584'C, capacity Q=8.398KW, and adiabatic material size 53mm is obtained with globular microstructure and finest.

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Phase Changes of Calcium Carbonate by Temperature and RPM in Continuous Crystallizer (연속식 결정화기에서 온도와 교반속도에 의한 탄산칼슘 결정의 형상변화)

  • Shin, Yuonjeong;Han, Hyunkak
    • Korean Chemical Engineering Research
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    • v.57 no.5
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    • pp.666-671
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    • 2019
  • Calcium carbonate involves three phases such as calcite, vaterite, and aragonite. Calcite and aragonite were more thermodynamically stable than vaterite. The synthesis of aragonite crystals by the reaction with sodium carbonate and calcium chloride solutions was investigated focusing on the effect of temperature and rpm in continuous crystallizer. In the batch crystallization test, calcite was synthesized by a relatively low temperature (under $40^{\circ}C$), but aragonite was formed at high temperature. In the continuous process with 100 rpm, no aragonite was found regardless of reaction temperature. But as increasing the stirring rate to 300 rpm and 500 rpm, the ratio of aragonite to calcite increased as increasing the temperature.

The Effect of Wind (Typhoon), Tide and Solar Radiation for the Water Stratification at Deukryang Bay in Summer , 1992 (하계 득량만의 연직혼합과 관련된 바람 (태풍), 조석, 태양에너지의 영향)

  • Lee, Byung-Gul;Cho, Kyu-Dae;Hong, Chol-Hoon
    • Journal of the Korean Society of Fisheries and Ocean Technology
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    • v.31 no.3
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    • pp.256-263
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    • 1995
  • This paper presents the evidence on the considerably strong stratification - destratification(SD) phenomena during spring - neap tidal cycle in summer of 1992 based on the observed temperature, salinity and density data. To find out the main factors causing SD in the bay, we computed the rate of potential energy balance of the surface heat flux, tidal and wind stirring proposed by Simpson and Hunter (1974) and Simpson and Bowders (1981) using observed data. It was found that the energy of the wind stirring was one - order smaller than those of the heat flux and the tidal stirring. It means that the variation of stratification phenomena in the bay mainly depend on tidal stirring and sea surface heating in summer if there was no exceptionally strong wind event like a typhoon. Finally, we tested the effects of typhoon on the mixing characteristics of the bay using the example of a empirical typhoon model. It was found that when wind speed is larger than 15m/sec in Deukryang Bay, the wind energy was always larger than the average heating energy based on empirical typhoon model test. Particularly, typhoon passed on the left side of the bay, strong wind energy happened, which is almost the same as tidal energy of spring tide.

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Effect of reaction factors on the characteristics of Ni-coating layer onto graphite (흑연표면의 니켈코팅층 특성에 미치는 반응인자의 영향)

  • Dong Jin Kim;Hun Saeong Chung;Myung Kyu Jung;Ki Byoung Youn
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.4 no.4
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    • pp.395-404
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    • 1994
  • Ni-graphite composite powders were prepared by reduction of $Ni^{++}$ from ammoniacal nickel sulfate solution on graphite core by hydrogen gas. Effect of reaction factors on the reduction rate and the properties of nickel layer were investigated by SEM, Optical Microscopy, size and chemical analysis. Induction period, a time lag between the injection of hydrogen gas and the start of the reduction, was 20~110 mins and affected by the reaction temperature and stirring speed. The reduction rate of $Ni^{++}$ was $4.5g/{\ell}/min$ at optimum condition and increased with increasing reaction temperature and stirring speed.

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Determination of Non-Steroidal Anti-Inflammatory Drugs in Human Urine Sample using HPLC/UV and Three Phase Hollow Fiber-Liquid Phase Microextraction (HF-LPME)

  • Cha, Yong Byoung;Myung, Seung-Woon
    • Bulletin of the Korean Chemical Society
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    • v.34 no.11
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    • pp.3444-3450
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    • 2013
  • Three phase hollow fiber-liquid phase microextraction (HF-LPME), which is faster, simpler and uses a more environmentally friendly sample-preparation technique, was developed for the analysis of Non-Steroidal Anti-Inflammatory Drugs (NSAIDs) in human urine. For the effective simultaneous extraction/concentration of NSAIDs by three phase HF-LPME, parameters (such as extraction organic solvent, pH of donor/acceptor phase, stirring speed, salting-out effect, sample temperature, and extraction time) which influence the extraction efficiency were optimized. NSAIDs were extracted and concentrated from 4 mL of aqueous solution at pH 3 (donor phase) into dihexyl ether immobilized in the wall pores of a porous hollow fiber, and then extracted into the acceptor phase at pH 13 located in the lumen of the hollow fiber. After the extraction, 5 ${\mu}L$ of the acceptor phase was directly injected into the HPLC/UV system. Simultaneous chromatographic separation of seven NSAIDs was achieved on an Eclipse XDB-C18 (4.6 mm i.d. ${\times}$ 150 mm length, 5 ${\mu}m$ particle size) column using isocratic elution with 0.1% formic acid and methanol (30:70) at a HPLC-UV/Vis system. Under optimized conditions (extraction solvent, dihexyl ether; $pH_{donor}$, 3; $pH_{acceptor}$, 13; stirring speed, 1500 rpm; NaCl salt, 10%; sample temperature, $60^{\circ}C$; and extraction time, 45 min), enrichment factors (EF) were between 59 and 260. The limit of detection (LOD) and limit of quantitation (LOQ) in the spiked urine matrix were in the concentration range of 5-15 ng/mL and 15-45 ng/mL, respectively. The relative recovery and precision obtained were between 58 and 136% and below 15.7% RSD, respectively. The calibration curve was linear within the range of 0.015-0.96 ng/mL with the square of the correlation coefficient being more than 0.997. The established method can be used to analyse of NSAIDs of low concentration (ng/mL) in urine.

Preparation of Spherical Energetic Composites by Crystallization/Agglomeration and their Thermal Decomposition Characteristics (결정화/응집 기법에 의한 구형 에너지 복합체 제조 및 그 열분해 특성)

  • Lee, Eun-Ae;Shim, Hong-Min;Kim, Jae-Kyeong;Kim, Hyoun-Soo;Koo, Kee-Kahb
    • Applied Chemistry for Engineering
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    • v.27 no.2
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    • pp.158-164
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    • 2016
  • Spherical DADNE/AP (1,1-diamino-2,2-dinitroethylen/ammonium perchlorate) energetic composites were produced by drowning-out/agglomeration (D/A). The agglomeration of DADNE with AP particles was found to be affected by the amount of the bridging liquid, stirring velocity and residence time. The composites appeared to grow dramatically with the amount of bridging liquid which triggers agglomeration. As the stirring velocity and the residence time increased, the size of composites increased and then tended to decrease. Thermal gravimetric analysis showed that the addition of DADNE activates the low temperature decomposition (LTD) of AP. For the neat AP, the only about 30 wt% of AP was found to decompose at the LTD. On the other hand, it was found that 70 wt% of AP decomposed when DADNE was added by physical mixing and 90 wt% of AP decomposed when the DADNE/AP composites were prepared by the D/A method.