• Title/Summary/Keyword: Stirring Temperature

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Fabrication of a Joint Node for an Aluminum Frame for a Low Speed Electric Vehicle using Thixoforming Technology (저속 전기자동차용 알루미늄 차체 조인트 노드의 반응고 성형)

  • Lee, S.Y.
    • Transactions of Materials Processing
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    • v.23 no.4
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    • pp.244-249
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    • 2014
  • The thixoforming process has been applied to forming of a joint node for the aluminum frame of a low speed electric vehicle. A joint node should connect three aluminum extruded chassis showing different profiles. The MHS(magnetohydrodynamic stirring) A357 billet was selected because homogeneous globular grains are necessary as the billet materials for thixoforming. A careful design of joint node has been performed by the considerations of structural demands and the simulation results for the thixoforming process using the MAGMAsoft. Optimum heating temperature for the A357 billet was between 580 and $585^{\circ}C$ corresponding to the semi-solid temperatures showing 20-30% of liquid fraction. An injection speed of around 100mm/s and preheating of die at temperatures of $200^{\circ}C$ were also necessary conditions to obtain reasonable thixoformed parts.

Adsorption of heavy metals Cu(II), Pb(II) and Cd(II) on Cichory (치커리에 의한 중금속 Cu(II), Pb(II), Cd(II)의 흡착능)

  • 박문숙;양미경
    • Journal of environmental and Sanitary engineering
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    • v.12 no.1
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    • pp.97-100
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    • 1997
  • The adsorption of the Chchory particles on Cu(II), Pb(II) and Cd(II) ions were examined by measurements of the adsorption percentage under various condition of temperature, pH, times, heavy metal concentration. Each of 100ml sample solution of Cu(II), Pb(II) and Cd(II) ions mixed with 2g of the Cichory under stirring in shaking water bath for minutes. The solutions were then filtered and pretreatmented according to water pollution official test methods. The concentrations of Cu(II), Pb(II) and Cd(II) ions in the solution were determined by the atomic adsorption spectrophotometer. As a results, the most effective pH of the adsorption of Cu(II), Pb(II) and Cd(II) was 9. With increasing the concentration of heavy metals the amount of adsorption on Cichory was increased. The adsorption equilibrium of Pb(II) and Cd(II) ions were reached to equilibrium by shaking for about 40 minutes. The absorptivities were 85%, 75% respectively.

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The Study of Synthesis and Reactivity of Metal Complexes With Amino Acidic Ligands(I) (아미노산을 리간드로 갖는 금속착화합물의 합성 및 반응성에 관한 연구(I))

  • Han, Je-Hong;Chung, Pyung-Jin
    • Journal of the Korean Applied Science and Technology
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    • v.11 no.2
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    • pp.75-87
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    • 1994
  • The metal complexes containing amino acidic ligands were prepared by using 11 kinds of amino acids as ligands and Ni, Cu, Co, Zn, Fe as a central metal. The starting was continued for 4hrs at room temperature. But Bis(D,L-Serine)Ni (II), and (D,L-Serine)Co (II) were prepared by heating method($80^{\circ}C$). In order to investigated reaction activity of Bis(D,L-Aspartato) Metal(II), stirring time was varied and Bis(D,L-Tyrosine ) Metal(II) used different divalent metal salts. We anticipate getting a great value from these prepared complexes as a monomer and a catalyst of polymerization which has peculier characteristics.

Formation of Medium Chain Fatty Acid by Wine Yeasts (포도주 효모에 의한 중간크기의 지방산 생성)

  • Lee, Soo-O
    • Korean Journal of Food Science and Technology
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    • v.21 no.6
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    • pp.832-837
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    • 1989
  • It has been suggested that medium chain fatty acid(MCFA) may be toxic to yeast and bacteria and thus play a role in the inhibition of alcoholic and malolactic fermentations and also important contributors to wine flavour We measured, by the use of GLC, the concentrations of octanoic, decanoic and dodecanoic acids produced by 12 wine yeast strains during the alcoholic fermentation of a grape juice-like medium. In general, there was a high production of MCFA at first, dropping dramatically later. The formation of MCFA is largely dependent on yeast strain but it also depends upon temperature, sugar concentration, stirring and carbon dioxide sparging.

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Synthesis of Pentasil Zeolites (펜타실 제올라이트의 합성에 관한 연구)

  • Ahn, Byung-Joon;Chon, Hak-Ze
    • Journal of the Korean Chemical Society
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    • v.32 no.2
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    • pp.149-155
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    • 1988
  • Pentasil zeolites, including ZSM-5, ZSM-8, ZSM-11 and silicalites, were synthesized using various organic cations. Synthesis run was carried out in a Parr pressure reactor of $2{\ell}$ capacity and a self-constructed reactor with a magnetic stirring system. The reactant materials used are colloidal silica (Snowtex), sodium aluminate, sodium chloride, TEA, TPA, TBA, Choline and water. The composition of starting materials and the reaction temperature were found to be important factors for the synthesis of uniform pentasil zeolites.

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Synthesis of $(ZrSiO_4)$ Powders by the Sol-Gel Process -Effect of the Milling- (졸-겔법에 의한 지르콘$(ZrSiO_4)$ 분말 합성 -재분쇄(Milling)에 대한 효과-)

  • 신용철;신대용;한상목;남인탁
    • Journal of the Korean Ceramic Society
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    • v.32 no.7
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    • pp.853-857
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    • 1995
  • ZrSiO4 powders were prepared from partially hydrolyzed solution of Si(OC2H5)4 and ZrOCl2.8H2O solution by the sol-gel method and formation rate of ZrSiO4 on the reaction parameter was investigated. In order to prepare homogeneous ZrSiO4 precursor gels, the H2O/Si(OC2H5)4 molar ratio of about 2, the pH of the ZrOCl2.8H2O solution fo about 4 and stirring time of the mixed solutions of about 2 hrs were appropriate. Formation of temperature of ZrSiO4 reduced about 15$0^{\circ}C$ by milling and formation of ZrSiO4 at 1300~135$0^{\circ}C$ showed an accelerative increase through the hedvall effect by silica.

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Preparation of Copper-coated Graphite Composite Powder by Hydrometallurgical Process (습식법에 의한 동-흑연 복합분말 제조)

  • 김동진;정헌생;윤기병
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.3 no.1
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    • pp.75-84
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    • 1993
  • Copper coating on graphite powders was carried out by cementation process from copper sulfate solution. Effects of operation variables such as copper ion concentration, stirring speed, reaction time and temperature were investigated to obtain optimum conditions for continuous and uniform copper coating on graphite powders. The activation energy of the copper coating process was found to be 3. 59kcal/mole.

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The Optimal Analytical Method for the Determination of PCE and TCE by GC/FID with SPME technieque (고체상미량분석법(SPME)을 이용한 GC/FID에서 PCE 및 TCE 최적 분석법)

  • Ahn Sang-Woo;Lee Si-Jin;Chang Soon-Woong
    • Journal of Environmental Science International
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    • v.13 no.10
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    • pp.903-909
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    • 2004
  • A new method based on solid phase microextraction(SPME), coupled with GC/FID, has been developed for the determination of PCE and TCE in water samples. The experimental parameters affecting the SPME process (i.e, kinds of fibers, extraction time, desorption time, extraction temperature, volume ratio of sample to headspace, salt addition, and magnetic stirring) were optimized. The coefficients of determination ($R^2$) for PCE and TCE were 0.9951 and 0.9831, respectively when analytes concentration ranges from 10 to 300$\mu$g/L. The relative standard deviations were 3.4 and $2.1\%$ for concentration of 10$\mu$g/L(n=5), respectively. The detection limits of PCE and TCE were 0.5 and l.3$\mu$g/L, respectively.

천연 점토를 이용한 Pb(II)의 흡착에 관한연구

  • 김강우;이한섭
    • Journal of Environmental Health Sciences
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    • v.27 no.2
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    • pp.138-144
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    • 2001
  • This study was carried out to investigate characteristics and Pb(II) removal effect of natural clays in the batch mode test. The effect of parameters such as temperature, adsorption time and coexisting cations on the sorption ability and characteristics was investigated to find out whether the clays could be used as adsorbents. Several natural clays from domestic have been investigated to have high specific surface area and have minerals such as SiO$_2$ and $Al_2$O$_3$. As a result, removal effects of Pb(II) on clays were reached at equilibrium in aqueous solutions by stirring about 20 minutes. The removal effect of Pb(II) was best for Kang Jin clay than other clays in terms of fixed time. Adsorption efficiency was not influenced by the possibility of continuous treatment system of wastewater which contain heavy metals by using natural clays from domestic.

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Hydrothermal Synthesis of Rod-like Copper Oxide Crystals

  • Pee, Jae-Hwan;Lee, Dong-Wook;Kim, Ung-Soo;Choi, Eui-Seok
    • Proceedings of the Korean Powder Metallurgy Institute Conference
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    • 2006.09a
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    • pp.167-168
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    • 2006
  • A hyrdrothermal synthesis has been developd to prepare rod-like crystals of copper oxide using copper nitrate trihydrate as a function of synthesis temperature, stirring speed and solution pH value. The properties of the fabricated crystals were studied using scanning electron microscopy, X-ray diffraction and particle size analysis. The morphology of the synthesized CuO was dependent on both the pH value of the solution and the morphology of the seed materials. Synthesized particles have regular morphologies and a uniform size distribution.

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