• Title/Summary/Keyword: Standard solution

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A STUDY ON THE ELIMINATION OF FLUORIDE IN A HOT SPRING WATER

  • Lee, Hyeon-Ki;Kim, Hwan-Gi
    • Environmental Engineering Research
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    • v.11 no.2
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    • pp.77-83
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    • 2006
  • The hot spring water of the north Jeonla province such as Wanggung, Jookrim, Seokjung, and Hwasim, has fluoride concentration of 3.9 mg/L, 12.7 mg/L, 1.9 mg/L, and 6.3 mg/L, respectively. These figures fairly exceed the Korean and WHO standard for potable water, which is 1.5 mg/L. Therefore, in this study, research on elimination of fluoride in a hot spring water of Jookrim region, which has the highest level of fluoride concentration level in the north Jeonla province, was carried out. In analysis of Jookrim hot spring water according to the water quality standard for potable water, pH was very high at 9.25 and the concentration of fluoride was 10 times higher than the standard at 18.2 mg/L. Other measurements were within the standard or not detected. After injecting 10g of activated carbon for elimination of fluoride, the fluoride concentration was measured at 13.5 mg/L, and when 70mL or more of alum 10 g/L solution was injected, the concentration was measured at 2.8 mg/L, and injecting 3g of lime was measured at 9 mg/L. Alum showed the best elimination performance among all individual injections. Injection of 25 mL of activated carbon and 100 mL of alum solution together reduced the fluoride concentration down to 1.3 mg/L, which is under the potable standard. Injection of lime 1g and 75 mL of alum 10 g/L solution together reduced fluoride concentration to 4.1 mg/L. From the modifying HRT, by using ion exchange resin column, the pH was stabilized when HRT was Imin and showed range of $6.7{\sim}7.8$. The fluoride concentration reduced gradually as the HRT increased, and satisfied the potable standard when HRT passed 6 min, and after 30 min HRT, the concentration of fluoride was 0.05 mg/L: almost eliminated.

HEAT EQUATION WITH A GEOMETRIC ROUGH PATH POTENTIAL IN ONE SPACE DIMENSION: EXISTENCE AND REGULARITY OF SOLUTION

  • Kim, Hyun-Jung;Lototsky, Sergey V.
    • Communications of the Korean Mathematical Society
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    • v.34 no.3
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    • pp.757-769
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    • 2019
  • A solution of the heat equation with a distribution-valued potential is constructed by regularization. When the potential is the generalized derivative of a $H{\ddot{o}}lder$ continuous function, regularity of the resulting solution is in line with the standard parabolic theory.

Comparison of Dioxin Analytical Results Between SP-2331 and DB-5MS Capillary Columns in the HRGC/HRMS Analysis (HRGC/HRMS에 SP-2331 및 DB-5MS 컬럼 사용시 다이옥신 결과의 비교)

  • Hong, Jongki;Yang, Jeong-Soo;Shin, Jung-Hwa;Ahn, Yun-Gyong;Lee, Dai-Woon
    • Analytical Science and Technology
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    • v.17 no.2
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    • pp.184-191
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    • 2004
  • In this study, the separation of toxic dioxin 2,3,7,8-congeners by DB-5MS and SP-2331 GC columns which are widely used in HRGC/HRMS analysis was examined. Through the dioxin analysis of column performance check standard solution and fly ash sample, the isomer specific separation of 2,3,7,8-substituted dioxins from tetra to hexa-isomers on DB-5MS and SP-2331 columns were studied. The effect of I-TEQ value by these columns was also studied. The total concentrations of toxic dioxins for the column performance check standard solution were 508.4 ng/mL analyzed by DB-5MS and 515.8 ng/mL analyzed by SP-2331, respectively. The I-TEQ value obtained by both columns was shown to be almost equivalent for the column performance check standard solution and fly ash sample.

Uncertainty Evaluation of Ammonia Determination in Burley Tobacco (버어리종 담배중 암모니아성 질소에 대한 불확도 측정)

  • Lee Jeong-Min;Lee Kyoung-Ku;Han Sang-Bin
    • Journal of the Korean Society of Tobacco Science
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    • v.27 no.1 s.53
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    • pp.107-114
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    • 2005
  • The uncertainty of measurement in quantitative analysis of ammonia by continuous-flow analysis method was evaluated following internationally accepted guidelines. The sources of uncertainty associated with the analysis of ammonia were the weighing of sample, the preparation of extracting solution, the addition of extracting solution into the sample, the reproducibility of analysis and the determination of water content in tobacco, etc. In calculating uncertainties, Type A of uncertainty was evaluated by the statistical analysis of a series of observation, and Type B by the information based on supplier's catalogue and/or certificated of calibration. It was shown that the main source of uncertainty was caused by the volume measurement of 1 mL and 2 mL, the purity of ammonia reference material in the preparation of standard solution, the reproducibility of analysis and the determination of water content of tobacco. The uncertainty in the addition of extraction solution, the sample weighing, the volume measurement of 50 mL and 100 mL, and the calibration curve of standard solution contributed relatively little to the overall uncertainty. The expanded uncertainty of ammonia determination in burley tobacco at $95\%$ level of confidence was $0.00997\%$.

Modified electrical conductivity test method for evaluation concrete permeability

  • Pilvar, Amirreza;Ramezanianpour, Ali Akbar;Rajaie, Hosein
    • Computers and Concrete
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    • v.16 no.6
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    • pp.865-880
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    • 2015
  • Standard test method for bulk electrical conductivity (ASTM C1760) provides a rapid indication of the concrete's resistance to the penetration of chloride ions by diffusion. In this paper a new approach for assessing the bulk electrical conductivity of saturated specimens of hardened concrete is presented. The test involves saturating concrete specimens with a 5 M NaCl solution before measuring the conductivity of the samples. By saturating specimens with a highly conductive solution, they showed virtually the same pore solution conductivity. Different concrete samples yield different conductivity primarily due to differences in their pore structure. The feasibility of the method has been demonstrated by testing different concrete mixtures consisting ordinary and blended cement of silica fume (SF) and calcined perlite powder (CPP). Two standard test methods of RCPT (ASTM C1202) and Bulk Conductivity (ASTM C1760) were also applied to all of the samples. The results show that for concretes containing SF and CPP, the proposed method is less sensitive towards the variations in the pore solution conductivity in comparison with RCPT and Bulk Conductivity tests. It seems that this method is suitable for the assessment of the performance and durability of different concretes containing supplementary cementitious materials.

Improvement of the Ammonia Analysis by the Phenate Method in Water and Wastewater

  • Park, Ga-Eun;Oh, Ha-Na;Ahn, Sam-Young
    • Bulletin of the Korean Chemical Society
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    • v.30 no.9
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    • pp.2032-2038
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    • 2009
  • The amount of phenol and NaOH for the colorimetric determination of ammonia in Korean standard methods (KSM) is found to be highly excessive compared to the standard methods of several other countries. The absorbance of indophenol formed by the Berthelot reaction for ammonia analysis was measured under the various reaction conditions classified in experiment groups 1, 2, 3, 4 and KSM and American standards methods (ASM), and the relationships between the absorbance of indophenol and concentration of ammonia were compared. The amount of phenol can be reduced to 10 g (current 25 g in KSM) and NaOH can be reduced to 1.76 g (current 11 g in KSM) for the preparation of 200 mL phenate solution, and the absorbance sensitivity increased. The concentration of the phenol and NaOH correlatively affect the pH of the solution, which is a critical variable in achieving the maximum sensitivity and rapid and stable color development.

A Turbidimetric Determination of Protein by Trichloroacetic Acid

  • Choi, Wahn-Soo;Chung, Kae-Jong;Chang, Man-Sik;Chun, Jae-Kwang;Lee, Hyang-Woo;Hong, Sung-Youl
    • Archives of Pharmacal Research
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    • v.16 no.1
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    • pp.57-61
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    • 1993
  • Based on the turbidimetric response of protein with 50% trichloroacetic acid (TCA), this study aims to introduce an assay method for protein in solution. The standard procedure consists of mixing equal volume of sample solution (standard or unknown) with 50%-TCA solution and measuring the absorbance at 450 nm after 20 min. The absorbances of the solutions were almost stable over 120 min at room temperature. This assy method is simple, reproducible, and tolerant to many interfering substances. It can detect less amount than $10\mu$g/ml of bovin serum albumin. The assay method has low protein-to-protein variability over wide range of molecular weight.

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Uncertainty in Potentiodynamic Polarization Resistance Measurement (동전위 분극저항 측정에서의 불확도)

  • Kim, Jong Jip
    • Corrosion Science and Technology
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    • v.8 no.5
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    • pp.193-196
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    • 2009
  • For the estimation of uncertainty in potentiodynamic polarization resistance measurement, the type A uncertainty was measured using type 316 stainless steel in an acidified NaCl solution. Sensitivity coefficients were determined for measurand such as scan rate of potential, temperature of solution, concentration of NaCl, concentration of HCl, surface roughness of specimen and flow rate of purging gas. Sensitivity coefficients were large for the measurand such as the scan rate of potential, temperature of solution and roughness of specimen. However, the sensitivity coefficients were not the major factors influencing the combined standard uncertainty of polarization resistance due to the low values of uncertainty in measurements of the measurands. A major influencing factor was the concentration of NaCl. The value of type A uncertainty was 1.1 times the value of type B uncertainty, and the combined standard uncertainty was 10.5 % of the average value of polarization resistance.

SIF AND FINITE ELEMENT SOLUTIONS FOR CORNER SINGULARITIES

  • Woo, Gyungsoo;Kim, Seokchan
    • East Asian mathematical journal
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    • v.34 no.5
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    • pp.623-632
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    • 2018
  • In [7, 8] they introduced a new finite element method for accurate numerical solutions of Poisson equations with corner singularities. They consider the Poisson equations with homogeneous boundary conditions, compute the finite element solutions using standard FEM and use the extraction formula to compute the stress intensity factor(s), then they posed new PDE with a regular solution by imposing the nonhomogeneous boundary condition using the computed stress intensity factor(s), which converges with optimal speed. From the solution they could get an accurate solution just by adding the singular part. Their algorithm involves an iteration and the iteration number depends on the acuracy of stress intensity factors, which is usually obtained by extraction formula which use the finite element solutions computed by standard Finite Element Method. In this paper we investigate the dependence of the iteration number on the convergence of stress intensity factors and give a way to reduce the iteration number, together with some numerical experiments.

A NEW ALTERNATIVE ELLIPTIC PDE IN EIT IMAGING

  • Kim, Sungwhan
    • Bulletin of the Korean Mathematical Society
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    • v.49 no.6
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    • pp.1291-1302
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    • 2012
  • In this paper, we introduce a new elliptic PDE: $$\{{\nabla}{\cdot}\(\frac{|{\gamma}^{\omega}(r)|^2}{\sigma}{\nabla}v_{\omega}(r)\)=0,\;r{\in}{\Omega},\\v_{\omega}(r)=f(r),\;r{\in}{\partial}{\Omega},$$ where ${\gamma}^{\omega}={\sigma}+i{\omega}{\epsilon}$ is the admittivity distribution of the conducting material ${\Omega}$ and it is shown that the introduced elliptic PDE can replace the standard elliptic PDE with conductivity coefficient in EIT imaging. Indeed, letting $v_0$ be the solution to the standard elliptic PDE with conductivity coefficient, the solution $v_{\omega}$ is quite close to the solution $v_0$ and can show spectroscopic properties of the conducting object ${\Omega}$ unlike $v_0$. In particular, the potential $v_{\omega}$ can be used in detecting a thin low-conducting anomaly located in ${\Omega}$ since the spectroscopic change of the Neumann data of $v_{\omega}$ is inversely proportional to thickness of the thin anomaly.