• Title/Summary/Keyword: Sr-89

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Simultaneous analysis method of 89Sr and 90Sr in liquid sample using automated separation system (자동핵종분리장치를 이용한 액체시료 중 89Sr, 90Sr 동시분석법 연구)

  • Kim, Heewon;Lee, Yong-Jin;Kim, Sun-Ha;Lee, Jin-Hong;Lim, Jong-Myoung;Kim, Hyuncheol
    • Analytical Science and Technology
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    • v.33 no.6
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    • pp.274-284
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    • 2020
  • This study described the analytical method for simultaneous determination of 89Sr and 90Sr in liquid sample using automated separation system. Radiostrontium in 0.5 kg of liquid sample was concentrated as SrCO3 to reduce the volume of sample, and purified from the sample using Sr-resin 2 mL (BV, Bed volume). The behavior of Sr and interferences such as Ba, Ca and Y were estimated with various flow rate ranging from 1 to 4 mL min-1. The detailed procedure for the purification of Sr on Sr-resin was presented. The purified radiostronitum was measured in Cerenkov mode and then measured in Scintillation mode by mixing scintillation cocktail. The measured value in both modes were used to calculate the activity of 89Sr and 90Sr. The performance tests were carried out the lab-control-sample having various activity ratio of between 89Sr and 90Sr. The recovery of Sr was ranged from 68 to 94 %. The relative bias of 89Sr activity was ranged from -5 to 20 %, and it was ranged from -10 to 10 % for 90Sr.

A Study on the Analysis of 89Sr and 90Sr with Cerenkov Radiation and Liquid Scintillation Counting Method (첼렌코프광과 액체섬광계수법을 이용한 89Sr 및 90Sr 분석에 대한 연구)

  • Lee, Myung-Ho;Chung, Geun-Ho;Cho, Young-Hyun;Choi, Geun-Sik;Lee, Chang-Woo
    • Analytical Science and Technology
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    • v.15 no.1
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    • pp.20-25
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    • 2002
  • An accurate and simple analytical technique for $^{89}Sr$ and $^{90}Sr$, overcoming the demerits of the conventional method, has been developed with extraction chromatography and liquid scintillation counting. The Sr fraction was separated from hindrance elements with oxalate coprecipitation or cation exchange resin and purified with Sr-Spec column. With liquid scintillation counter, $^{89}Sr$ was measured by Cerenkov radiation method, and $^{90}Sr$ was measured by spectrum unfolding method. The developed radioactive strontium separation method was validated by application to the IAEA-reference material (IAEA-375, Soil) and radioactive waste samples.

Analysis of $^{89}Sr,\;^{90}Sr$ in Soil Sample Using Crown Ether/Chloroform Solvent Extraction Method (Crown Ether/Chloroform 용매추출법을 이용한 토양시료중의 $^{89}Sr,\;^{90}Sr$ 분석)

  • Hong, Kwang-Hee;Choi, Yong-Ho;Kim, Sang-Bog;Lee, Myong-Ho;Park, Hyo-Guk;Choi, Kun-Sik;Kim, Sam-Rang;Lee, Chang-Woo
    • Journal of Radiation Protection and Research
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    • v.21 no.1
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    • pp.9-16
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    • 1996
  • For the determination of radiostrontium, $^{89}Sr\;and\;^{90}Sr$ in environmental soil sample, a solvent extraction method for the separation of Ca and Sr from matrix using crown ether was investigated. In comparison with the existing fuming nitric acid method, the extraction method showed high chemical yield of strontium and provided simple and rapid analytical steps. The new analytical method applied to the determination of radiostrontium in some soil sample around a nuclear power station to show that the analytical procedure is readily applicable to the practical radioactivity monitoring.

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Sr Isotopic Composition of Apatite from the Yeongju and Andong Granites: Isotopic Distinction between the Two Granites and Location of the Boundary (영주화강암과 안동 화강암의 인회석 Sr 동위원소 조성: 두 암체의 동위원소적 구분과 경계의 위치)

  • Yoon, Rina;Lee, Seung-Gu;Park, Kye-Hun;Song, Yong-Sun
    • The Journal of the Petrological Society of Korea
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    • v.25 no.1
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    • pp.89-93
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    • 2016
  • Yeongju and Andong granites, located in the northeastern Yeongnam massif, reveal very similar emplacement ages but distinct initial isotopic compositions of strontium. However, previous studies used different boundaries to distinguish these batholiths. In this study, we determined Sr isotopic compositions of apatite separated from the granites of the area to find out the proper boundary and propose the location of such boundary based upon analysis.

Grain boundary structure and electrical characteristics of alkaline metallic cation-diffused $(SrCa)TiO_3$ ceramics (알칼리 금속 이온의 입계확산에 따른 $(SrCa)TiO_3$ 소결체의 입계구조 및 전기적 특성)

  • Heo, Hyeon;Cho, Nam-Hui
    • Journal of the Korea Institute of Military Science and Technology
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    • v.2 no.1
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    • pp.183-193
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    • 1999
  • Semiconducting (Sr0.85Ca0.15)TiO3 ceramics were prepared by conventional powder synthesis techniques, and then alkaline metallic cations were diffused into the ceramic bodies. The threshold voltage of the ceramics increases with increasing diffusion time and the amount of diffused materials. The ceramics had boundary potential heights of 0.01 ~ 2.89 eV, while their boundary resistance ranged from 2.2 $M{\Omega}$ to 120.4 $M{\Omega}$. Such electrical characteristics of the boundaries were correlated with the boundary structure of the ceramics obtained by transmission electron microscopy.

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A Study on the Decontamination of Cs-137 and Sr-90 Contained in the Liquid Radioactive Waste Discharged from the Spent Fuel Storage Tank Using Microalgae (미세조류를 이용한 사용후핵연료 저장조에서 배출되는 방사성 폐액에 함유된 Cs-137 및 Sr-90 제염에 관한 연구)

  • Kim, Tae Young;Park, Hye Min;Song, Yang Soo;Lee, Un Jang
    • Resources Recycling
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    • v.31 no.5
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    • pp.20-25
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    • 2022
  • In this study, the applicability of microalgae was evaluated for eco-friendly decontamination of cesium-137 (Cs-137) and strontium-90 (Sr-90), which are radioactive nuclides contained in radioactive waste. The monolithic radioactive solution used in the experiment was manufactured at a concentration of 1.5 Bq/mL Cs-137 and 1.0 Bq/mL Sr-90 by diluting a standard radioactive solution and distilled water. This experiment used two types of microalgae, Chlorella Vulgaris was used for Sr-90 decontamination and Hematococcus pluvialis for Cs-137 decontamination. The experimental method is to put the microalgae cultured for 2 weeks into a bottle with a semi-permeable membrane, and then put the bottle in which the microalgae was put into the manufactured radioactive solution, so that the microalgae and the radioactive solution react through the semi-permeable membrane for 48 hours. For the radioactivity concentration analysis of each sample, a gamma-ray nuclide analyzer was used for Cs-137, a γ-ray isotope, and a Liquid Scintillation Count(LSC) was used f or Sr-90, a β-ray isotope. As a result of the experiment, it was confirmed that about 88.0 % of Cs-137 and about 89.7 % of Sr-90 could be decontaminated, and about 98.6 % of Sr-90 was finally able to be decontaminated by the two-stage decontamination method.

Study on (n, α) reactions for the production of 51Cr, 89Sr, 99Tc, 131I, 133Xe, 137Cs and 153Sm radioisotopes used in nuclear medicine

  • Hallo M. Abdullah;Ali H. Ahmed
    • Nuclear Engineering and Technology
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    • v.55 no.9
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    • pp.3352-3358
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    • 2023
  • Nuclear medicine seems to be a decent choice of medicine in the recent decade. The radioactive isotopes 51Cr, 89Sr, 99Tc, 131I, 133Xe, 137Cs and 153Sm are extremely essential in nuclear medicine. The excitation functions of the 54Fe (n, α) 51Cr, 92Zr (n, α) 89Sr, 102Rh (n, α) 99Tc, 134Cs (n, α) 131I, 136Ba (n, α) 133Xe, 140La (n, α) 137Cs and 156Gd (n, α) 153Sm reactions were calculated in this study using the EMPIRE 3.2.3 and TALYS 1.95 nuclear codes. Additionally, the cross sections at 14-15 MeV were calculated using empirical formulae and the experimental data. The computer codes were compared to the experimental data and Empirical formulas as well as the evaluated data (TENDL 2021, JENDL 3.3, JENDL 5, JEFF 3.3, EAF 2010, CENDL 3.1, CENDL 3.2, ROSFOND 2010, FENDL 3.2 b, and BROND 3.1).