• Title/Summary/Keyword: Solidification Process

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Magneto-impedance effect of CoFeSiBNi amorphous magnetic films (CoFeSiBNi 아몰퍼스 합금의 자기-임피던스 효과)

  • Lee, Seung-Hun;Park, Byung-Kyu;Hwang, Sung-Woo;Moon, Sung
    • Journal of Sensor Science and Technology
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    • v.16 no.5
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    • pp.389-393
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    • 2007
  • Soft ferromagnetic materials are very useful for many sensors using magnetic materials demanding high permeability, low coercivity and low hysteresis loss. Among them, FeCoSiBNi amorphous magnetic films show a good impedance change (about 5.01 %/Oe, at 10 MHz) by the exterinal magnetic field in this experiment. The magnetic films are produced by melt-spun method, one of the rapid solidification process. Ribbon shape wires were made from the films, and let them annealed in DC magnetic field to increase the maximum Giant Magneto Impedance ratio. Field annealing decreases the stress and changes the effective anisotropy. Thus, we can find that the impedance change (200.47 %) is improved and the fabricated magnetic wire has characteristics of good sensor element.

The Reliability of Optical Fiber Assembly Using Glass Solder

  • Lee, Jong-Jing;Kang, Hyun-Seo;Koh, Jai-Sang
    • Proceedings of the Korean Reliability Society Conference
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    • 2004.07a
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    • pp.147-151
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    • 2004
  • In this study, an optical fiber assembly directly coupled with a laser diode or a photo diode is designed to confirm high reliable optical coupling efficiency of optical transmitter(Tx) and receiver(Rx). The optical fiber assembly is fabricated by soldering an optical fiber and a Kovar ferrule using a glass solder after inserting an optical fiber through a Kovar ferrule. The Kovar which has good welding characteristics is applied to introduce laser welding technique. The glass solder has excellent thermal characteristics such as thermal shift delamination compared with PbSn, AuSn solder previously used usually. Furthermore, the glass solder doesn't need fiber metalization and this enables low cost fabrication. However, the glass soldering is high temperature process over 35$0^{\circ}C$ and the convex shape after solidification due to surface tension causes the stress concentration on optical fiber. The stress concentration on the optical fiber increases the optical insertion loss and possibility of crack formation. The shape of glass solder was designed referring to 2-D Axi-symmetric FEM simulation. To test the mechanical reliability, mechanical vibration test and shock test were done according to Telcorida GR-468-Core protocol. After each test, the optical loss of the stress distributed fiber assembly didn't exceed 0.5 dB, which passes the test.

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Mechanical Properties of SiC Particulate Reinforced Mg Matrix Composites Fabricated by Melt Stirring Method (용탕교반법에 의한 SiC 입자강화 Mg기 복합재료의 기계적 특성)

  • Lim, Suk-Won;Choh, Takao;Park, Young-Jin
    • Journal of Korea Foundry Society
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    • v.13 no.5
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    • pp.441-449
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    • 1993
  • SiC particulate reinforced magnesium matrix composites were fabricated by melt stirring method. The effet of several factors on mechanical properties and the efficiency of melt stirring method from the viewpoint of these properties were investigated. The tensile strength increased and the elongation decreased with decrease of the particle size or the increase of the paticulate volume fraction for pure magnesium matrix and Mg-5%Zn alloy matrix composites. A longer stirring time improved the tensile strength of these composites. The tensile strength of Mg-5%Ca alloy matrix composites which shows no uniform paticulate distribution was a little lower than that of matrix alloy. Rapid solidification rate is preferred for the improved tensile strength of these composites. The pure magnesium matrix and Mg-5%Zn alloy matrix composites have tensile strength of about 400MPa. This value agrees with the tensile strength of some magnesium matrix composites fabricated by liquid infiltration method or powder metallurgy method at the same volume fraction of reinforcements of whisker or particle. Therefore, the melt stirring method which has the advantages of simple process is considered to be efficient in fabricating magnesium matrix composites.

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Shape Memory Characteristics and Mechanical Properties of Rapidly Solidified $Ti_{50}Ni_{20}Cu_{30}$ Alloy Strips (급냉응고된 $Ti_{50}Ni_{20}Cu_{30}$ 합금 스트립의 형상기억특성과 기계적특성)

  • Kim, Yoen-Wook
    • Journal of Korea Foundry Society
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    • v.29 no.5
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    • pp.187-191
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    • 2009
  • Microstructures and shape memory characteristics of $Ti_{50}Ni_{20}Cu_{30}$ alloy strips fabricated by arc melt overflow have been investigated by means of XRD, optical microscopy and DSC. The microstructure of as-cast strips exhibited columnar grains normal to the strip surface. X-ray diffraction analysis showed that one-step martensitic transformation of B2-B19 occurred in the alloy strips. According to the DSC analysis, it was known that the martensitic transformation temperature ($M_s$) of B2 $\rightarrow$ B19 in $Ti_{50}Ni_{20}Cu_{30}$ strip is $57^{\circ}C$. During thermal cyclic deformation with the applied stress of 60 MPa, transformation hysteresis and elongation associated with the B2-B19 transformation were observed to be $3.7^{\circ}C$ and 1.6%, respectively. The as-cast strip of $Ti_{50}Ni_{20}Cu_{30}$ alloy also showed a superelasticity and its stress hysteresis was as small as 14 MPa. These mechanical properties and shape memory characteristics of the alloy strips were ascribed to B2-B19 transformation and the controlled microstructures produced by rapid solidification of the arc melt overflow process.

Morphology of Membrane of Acrylic Polymers by Wet Phase Inversion Method (습식 상 역전 방법으로 제조한 아크릴계 고분자 막의 모폴로지)

  • Choi Seung-Eun;Park Han-Soo;Lee Kwang-Hee
    • Polymer(Korea)
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    • v.30 no.2
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    • pp.108-111
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    • 2006
  • In this work, the effect of the hydrophobicity of acrylic polymers on the membrane morphology was investigated. The membranes were prepared with poly(methyl methacrylate) (PMMA), poly(ethyl methacrylate) (PEMA), poly (butyl methacrylate) (PBMA), poly(isobutyl methacrylate), and their blends using the wet phase inversion method. PMMA and PEMA having a relatively less hydrophobicity formed the channel-like structure, whereas PBMA and PIBMA having more hydrophobic units formed the finger-like structure. These morphological changes were attributed to differences in the solidification process of the polymer-rich phase determine d by the polymer/solvent/nonsolvent ternary phase diagram. The membrane structures of the blends were controlled by the main component of their blends.

Measurement of Peltier Heat at the Solid/Liquid Interface and Its Application to Crystal Growth I : Theoretical Approach (고/액 계면에서의 Peltier 열 측정 및 결정성장에의 응용 I : 이론적 접근)

  • Kim, Il-Ho;Jang, Gyeong-Uk;Lee, Dong-Hui
    • Korean Journal of Materials Research
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    • v.9 no.11
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    • pp.1108-1111
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    • 1999
  • The Peltier heat absorbed or evolved at the solidiliquid interface in the unidirectional solidification process could contribute to the increase of temperature gradient in liquid and growth velocity, and the enhancement of crystal orientation. In this study, in order to measure the Peltier heat generated at the solidiliquid interface as a way of application to crystal growth, the thermoelectric effects were investigated on the temperature changes at the solid- and liquid-phase of the same material and its interface. Through the theoretical consideration, it was possible to separate sole Peltier. Thomson or Joule heat from the temperature changes due to current density, polarity, and temperature gradient. Thomson coefficient of solid- and liquid-phase as well as Peltier coefficient at the solid/liquid interface could be obtained.

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Formation of Poly(ethylene glycol)-Poly($\varepsilon$-caprolactone) Nanoparticles via Nanoprecipitation

  • Lee, Jae-Sung;Hwang, Su-Jong;Lee, Doo-Sung;Kim, Sung-Chul;Kim, Duk-Joon
    • Macromolecular Research
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    • v.17 no.2
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    • pp.72-78
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    • 2009
  • Size control of therapeutic carriers in drug delivery systems has become important due to its relevance to biodistribution in the human body and therapeutic efficacy. To understand the dependence of particle size on the formation condition during nanoprecipitation method, we prepared nanoparticles from biodegradable, amphiphilic block copolymers and investigated the particle size and structure of the resultant nanoparticles according to various process parameters. We synthesized monomethoxy poly(ethylene glycol)-poly($\varepsilon$-caprolactone) block copolymer, MPEG-PCL, with different MPEG/PCL ratios via ring opening polymerization initiated from the hydroxyl end group of MPEG. Using various formulations with systematic change of the block ratio of MPEG and PCL, solvent choice, and concentration of organic phase, MPEG-PCL nanoparticles were prepared through nanoprecipitation technique. The results indicated that (i) the nanoparticles have a dual structure with an MPEG shell and a PCL core, originating from self-assembly of MPEG-PCL copolymer in aqueous condition, and (ii) the size of nanoparticles is dependent upon two sequential processes: diffusion between the organic and aqueous phases and solidification of the polymer.

Characteristics of the Hard-Overlayers by WC-12%Co Powder Addition in MIG Welding of Al Alloy (Al 합금의 MIG 용접에서 WC-12%Co 분말에 첨가에 의한 경화육성층의 특성)

  • 박정식;양병모;박경채
    • Journal of Welding and Joining
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    • v.18 no.6
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    • pp.102-107
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    • 2000
  • It was attempted to improve the wear resistance of Al alloy under the load condition by making a formation of the thick surface hardening alloy layers. The thick surface hardening alloy layers were formed on 6061 Al alloys overlayed by MIG welding process with WC-12%Co powder addition. Effects of the dispersion of WE-12%Co powders on hardness and wear characteristics of alloys were investigated. The following results were obtained. Most of WE-12%Co powders are dispersed nearly uniform as unmelted particles in the matrix alloy. A part of WC-12%Co powders are melted in the molten pool, and during solidification {TEX}$Al_{9}Co_{2}${/TEX} appeared. With increasing addition of WC-12%Co powders, the hardness and specific wear resistance of the overlay weld alloys increased and reached Hv450 at WC-12%Co powder addition rate of 54g/min. It is considered that excellent wear resistance of the overlayed alloys was due to dispersed WC-12%Co powders and increased 10 times at WC-12%Co powder addition rate of 54 g/min than that of the WC-free overlaying layers.

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Micro-macroscopic analysis on the directional casting of a metal alloy (합금의 방향성 주조에 대한 미시적-거시적 해석)

  • Yu, Ho-Seon
    • Transactions of the Korean Society of Mechanical Engineers B
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    • v.21 no.10
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    • pp.1303-1313
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    • 1997
  • A micro-macroscopic analysis on the conduction-controlled directional casting of Al-Cu alloys is performed, in which emphases are placed on the microstructural features. In order to facilitate the solution procedure, an iterative micro-macroscopic coupling algorithm is developed. The predicted results show that the effect of finite back diffusion on the transient solidification process in comparison with the lever rule depends essentially on the initial concentration of an alloy. In the final casting, the eutectic fraction is distributed in an increasing-decreasing-increasing pattern, each mode of which is named the chill, interior and end zones. This nonuniformity per se suffices to justify the necessity of this work because it originates from the combined effects of finite back diffusion and cooling path-dependent nature of the eutectic formation. As the cooling rate is enhanced, not only the influence depths of boundaries narrow, but also the eutectic fractions in the chill and interior zones increase. In addition, it is revealed for the first time that the micro segregation band is formed in response to a sudden change in cooling rate during the directional casting. An increasing change creates an overshooting band in the eutectic fraction distribution, and vice versa.

Mechanical Properties of 316L manufactured by Selective Laser Melting (SLM) 3D printing (Selective Laser Melting (SLM) 방식 3D Printing으로 제조한 스테인레스 316L 기계적 물성 분석)

  • Park, Sun Hong;Jang, Jin Young;Noh, Yong Oh;Bae, Byung Hyun;Rhee, Byong Ho;Eo, Du Rim;Cho, Jung Wook
    • Proceedings of the Korean Society of Propulsion Engineers Conference
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    • 2017.05a
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    • pp.872-876
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    • 2017
  • Laser Based 3D Printing is an recently advance manufacturing technology for making complex shape comopnent such as automobile and aerospace. So in this article, stainless steel 316L was manufactured by Selective Laser Melting (SLM) and Laser Melting Deposition (LMD) method. SLM is an additive manufacturing process that allow for the manufacture of small and complex component by laser melting and solidification of powder in bed using a high intensity laser beam. The results showed that the laser scanning speed and laser power affects the defect, microstructure and the hardness of the components.

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