• 한국결정성장학회지
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• 제2권2호
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• pp.77-82
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• 1992

FZ법에 의한 결정성장에 있어서 용융대는 고액 계면의 장력에 의해 유지되고 상.하부의 고체봉 사이에 위치하고 있다. 따라서, 용융대의 표면에서는 온도와 농도 차이에 의해 표면장력의 구배가 발생하고 있는 marangoni 대류의 구동력으로 작용한다. 본 연구에서 정상상태의 결정성장시는 결정의 가장자리 영역에서의 Solute 농도는 결정내부 보다도 높아지게 되고 전위의 분포도 불규칙하여 지며, void나 기포 침투, Secondary phase의 생성 및 미소균열등의 결함 발생 확률이 계면부근에서 높아지는 결과를 알 수 있었다. 이는 고액성장 계면이 marangoni 대류에 의하여 이 영역에서 온도의 국부적인 변동에 의해 불규칙하여 지게 되기 때문이라 사료된다.

• 비파괴검사학회지
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• 제28권6호
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• pp.504-511
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• 2008

This paper proposes an ultrasonic measurement method for measurement of linear interfacial stiffness of contacting surface between two steel plates subjected to nominal compression pressures. Interfacial stiffness was evaluated by using shear waves reflected at contact interface of two identical solid plates. Three consecutive reflection waves from solid-solid surface are captured by pulse-echo method to evaluate the state of contact interface. A non-dimensional parameter defined as the ratio of their peak-to-peak amplitudes are formulated and used to calculate the quantitative stiffness of interface. Mathematical model for 1-D wave propagation across interfaces is developed to formulate the reflection and transmission waves across the interface and to determine the interfacial stiffness. Two identical plates are fabricated and assembled to form contacting surface and to measure interfacial stiffness at different states of contact pressure by means of bolt fastening. It is found from experiment that the amplitude of interfacial stiffness is dependent on the pressure and successfully determined by employing pulse-echo ultrasonic method without measuring through-transmission waves.

• 한국초전도ㆍ저온공학회논문지
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• 제3권2호
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• pp.77-83
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• 2001

The thermal characteristics of solid nitrogen are investigated by experiment and analysis for the purpose of evaluating its feasibility as a cooling medium for HTS (high T$_{c}$ superconductor) magnets. A cryostat to refrigerate a liquid-nitrogen container well below its freezing temperature with a 2-stage GM cryocooler is designed and constructed. The spatial distribution of temperature is measure as a function of time during the freezing and melting processes. from which the thermal diffusivity of solid nitrogen can be approximately calculated. the freezing process is formulated and solved by the integral method with an assumption of phase equilibrium at the solid-liquid interface and experimental observation. It may be concluded that the thermal diffusion in solid phase is much slower than in liquid and the degree of super-saturation is quite severe in the solidification of nitrogen.n.

• Journal of the Korean Wood Science and Technology
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• 제51권6호
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• pp.481-492
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• 2023

The ecofriendly lifestyle has attracted considerable support for sustainable development. Natural dyes, as sustainable products, have become a research focus and development area for many scientists. Ecofriendly processing also supports circular sustainable development. This study effectively obtained tannins as a natural dye from merbau (Intsia bijuga) sawdust using water as an ecofriendly solvent. Merbau sawdust is an underutilized industrial waste. Temperature and solid-solvent ratio variations were performed to extract tannins from merbau sawdust. Temperature and solid-solvent ratio positively affected solution yield and tannin concentration. The optimal condition was identified using response surface methodology and experimental observations. A yield of 0.2217 g tannins/g merbau was obtained under the conditions of 333.15 K and 0.125 solid-solvent ratio. Extraction was controlled by convective mass transfer at the interface of solid particles.

• 한국전기전자재료학회:학술대회논문집
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• 한국전기전자재료학회 1997년도 춘계학술대회 논문집
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• pp.111-115
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• 1997

There exists a interface among the different kinds of materials in the solid insulating ones, which effects on the insulating capability heavily. The insulating construction has been developed for each usages and take themselves into several sorts. The conjunction between CV cables have the electrical weakness of solidity and solid interface, so they were focused at the long distance-line. To this background, it is very important to get the information on the interface influencing on the insulating capability of cable and to observe its procedure. In this paper, the interface was made artificially to research the effect owing to the toughness of interface, which results in the aging and treeing proceeding was observed. The polyethylen, as is generally using for the cable, was taken in this research.

• 한국생산제조학회지
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• 제19권6호
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• pp.841-846
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• 2010

The present study examined the mechanical properties of the friction welding with hollow and solid shaft of SM45, of which the diameter is 25.2mm and 33mm. Friction welding was conducted at welding conditions of 2,000rpm, friction pressure of 50MPa, upset pressure of 70MPa, friction time of 0.4sec to 1.4sec by increasing 0.2sec, upset time of 2.0 sec including variable such as friction time are following. Under these conditions, a tensile test, a hardness test and a microstructure of weld interface were studied. The results were as follows : When the friction time was 1.0 seconds under the conditions, the maximum tensile strength of the friction weld happened to be 1,094MPa, which is 120% compared with the tensile strength of SM45C base metal. The upset length linearly increased as friction time increased. According to the hardness test, the hardness distribution of the weld interface was formed from 475Hv to 739Hv. HAZ(Heat Affected Zone) was formed from the weld interface to 2mm of SM45C.

• 한국세라믹학회지
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• 제25권1호
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• pp.78-82
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• 1988

Good quality LiNbO3 single crystals which can be applied to SAW devices, were grown by Czochralski method. It was observed that the gas-bubbles were concentrated in ring shape at the outer part of grown crystals, and this anomaly was illustrated by modeling the mechanism of gas-bubble entrapment according to the melt flow pattern in the crucible. And this mechanism was also encertained by observation of solid-liquid interface shape of grown crystals. The optimal condition for good quality crystals was known that the solid-liquid interface shape was slightly concave.

• Journal of Welding and Joining
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• 제20권5호
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• pp.93-98
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• 2002

The effect of bonding misfit on single crystallization of transient liquid phase (TLP) bonded joints of single crystal superalloy CMSX-2 was investigated using MBF-80 insert metal. The bonding misfit was defined by (100) twist angle (rotating angle) at bonded interface. TLP bonding of specimens was carried out at 1523K for 1.8ks in vacuum. The post-bond heat treatment consisted of the solution and sequential two step aging treatment was conducted in the Ar atmosphere. The crystallographic orientation analysis across the TLP bonded joints was conducted three dimensionally using the electron back scattering pattern (EBSP) method. EBSP analyses f3r the bonded and post bonded heat treated specimens were conducted. All bonded joints had misorientation centering around the bonded interface for as-bonded and post-bond heat treated specimens with rotating angle. The average misorientation angle between both solid phases in bonded interlayer was almost identical to the rotating angle at bonded interface. HRTEM observation revealed that the atom arrangement of both solid phases in bonded interlayer was quite different across the bonded interface. It followed that grain boundary was formed in bonded interface. It was confirmed that epitaxial growth of the solid phase occurred from the base metal substrates during TLP bonding and single crystallization could not be achieved in joints with rotating angle.

• 한국지반공학회논문집
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• 제18권1호
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• pp.79-89
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• 2002

폐기물 매립지에는 차수 및 보호기능을 하는 다양한 토목섬유가 사용된다. 토목섬유 사이의 접촉(interface) 전단강도는 사면에 설치되는 차수 및 최종 덮개시설의 안전한 설계를 위해 곡 필요한 물성치로서, 본 연구에서는 대형 직접전단 시험기를 사용하여 지오멤브레인(GM)과 지오텍스타일(GT) 사이의 접촉 전단강도를 측정하였다. 본 논문에서는 Mohr-Coulomb 파괴 포락선을 이용하여 전단강도를 평가하였으며, 연직하중, 수팀상태, 지오멤브레인(GM)의 표면상태-texturing 유무 - 등이 전단강도에 미치는 영향을 알아보았다. 분석 결과 연직하중이나 수침상태가 전단강도에 미치는 영향은 각각 하중의 크기와 토목섬유의 종류에 따라 정도가 다르게 나타났다. 사면에 설치되는 토목섬유의 경우, 다양한 현장조건-상재하중, 수침상태, 사용되는 토목섬유의 종류을 고려한 시험 결과를 통해 얻은 물성치를 이용하여야 안전한 설계가 될 수 있을 것이다.

• 비파괴검사학회지
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• 제32권4호
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• pp.401-409
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• 2012

초음파 시험은 접착계면에서 발생하는 미접착 결함을 검출할 수 있는 다른 비파괴 시험보다 미접착 검출 능력이 월등히 뛰어나다. 하지만, 스틸 연소관, 내열 고무, 라이너 및 추진제로 구성된 고체 추진기관은 각 재질의 음향 임피던스의 큰 차이와 반사파의 중첩 때문에 초음파 신호를 분석하기에는 많은 어려움 있다. 그러므로 고체 추진기관의 미접착 결함을 검출하기 위한 초음파 시험은 자동화된 C-Scan 시스템을 이용하여 스틸 연소관과 내열 고무 계면의 극히 제한된 영역에서 적용되어 왔다. 기존의 초음파 시험은 대부분의 초음파가 음향 임피던스가 낮은 고무 재질에서 흡수되므로 고체 추진기관의 라이너와 추진제 사이의 미접착 결함을 검출할 수 없었고, 이런 문제점을 해결하기 위하여 초음파 공진법을 사용하여 주파수 스펙트럼으로부터 공진 주파수를 분석하였다. 본 논문은 초음파 공진 특성을 이용하여 라이너와 추진제 사이의 미접착 결함을 검출할 수 있는 기법에 대해 자세히 기술하였다.