• Corrosion Science and Technology
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• v.6 no.4
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• pp.159-163
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• 2007

Micron size Co-alloy 800 (T800) powder is coated on the high temperature, oxidation and corrosion resistant super alloy Inconel 718 substrate by the optimal high velocity oxy-fuel (HVOF) thermal spray coating process developed by this laboratory. For the study of durability improvement of high speed spindle operating without lubricants, friction and sliding wear behaviors of the coatings are investigated both at room and at an elevated temperature of $1000^{\circ}F(538^{\circ}C)$. Friction coefficients, wear traces and wear debris of coatings are drastically reduced compared to those of non-coated surface of Inconel 718 substrate both at room temperature and at $538^{\circ}C$. Friction coefficients and wear traces of both coated and non-coated surfaces are drastically reduced at higher temperature of $538^{\circ}C$ compared with those at room temperature. At high temperature, the brittle oxides such as CoO, $Co_{3}O_{4}$, $MoO_2$ and $MoO_3$ are formed rapidly on the sliding surfaces, and the brittle oxide phases are easily attrited by reciprocating slides at high temperature through oxidation and abrasive wear mechanisms. The brittle solid oxide particles, softens, melts and partial-melts play roles as solid and liquid lubricants reducing friction coefficient and wear. These show that the coating is highly recommendable for the durability improvement coating on the machine component surfaces vulnerable to frictional heat and wear.

• Journal of the Korean institute of surface engineering
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• v.39 no.2
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• pp.70-75
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• 2006

As technology advances, there is a demand for development of hard, solid lubricant coating. (Ti,Cr)N-$MoS_2$, films were deposited on SKD 11 tool steel substrate by co-deposition of $MoS_2$, with (Ti,Cr)N using a D.C. magnetron sputtering process. The influence of the $N_2/Ar$ gas ratio, the deposition temperature, the amount of $MoS_2$ in the films, and the bias voltage on the mechanical and the structural properties of the films were investigated. Wear tests were performed on the films deposited in various conditions.

• Tribology and Lubricants
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• v.40 no.3
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• pp.103-110
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• 2024

Gas foil thrust bearings (GFTBs) are oil-free self-acting hydrodynamic bearings that support axial loads with a low friction during airborne operation. They need solid lubricants to reduce dry-friction between the runner and top foil and minimize local wears on their surfaces during start-up and shutdown processes. In this study, we evaluate the lift-off speeds and load capacity performance of a GFTB with Polytetrafluoroethylene (PTFE) surface coating by measuring drag torques during a series of experimental tests at increasing ambient temperatures of 25, 75 and 110℃. An electric heat gun provides hot air to the test GFTB operating in the closed booth to increase the ambient temperature. Test results show that the increasing ambient temperature delays the lift-off speed and decreases the load capacity of the test GFTB. An early developed prediction tool well predicts the measured drag torques at 60 krpm. After all tests, post inspections of the surface coating of the top foil are conducted. Scanning electron microscope (SEM) images imply that abrasive wear and oxidation wear are dominant during the tests at 25℃ and 110℃, respectively. A quantitative energy dispersive spectroscopy (EDS) microanalysis reveals that the weight percentages of carbon, oxygen, and nitrogen decrease, while that of fluorine increases significantly during the highest-temperature tests. The study demonstrates that the increasing ambient temperature noticeably deteriorates the static performances and degrades the surface coating of the test GFTB.

• Journal of the Korea Academia-Industrial cooperation Society
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• v.16 no.3
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• pp.2308-2313
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• 2015

In order to produce an optimal performance solid lubricant used in the refractory slates, various compositions of starch, graphite and water were evaluated by testing their viscosity, coefficient of friction and wear performance. At 15% starch content, the degree of viscosity increment rose in proportional to graphite content and the lowest coefficient of friction was observed when the graphite content was at 30 wt%. Our results demonstrate that, as the water content decrease, the ratio of solid content increases, which compromises the surface coating resulting in increase of coefficient of friction. The best wear test result was obtained when the starch content was at 15 wt% with graphite content at either 25 wt% or 30 wt%.

• Journal of the Korean Crystal Growth and Crystal Technology
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• v.16 no.6
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• pp.273-277
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• 2006

High velocity of oxy-fuel (HVOF) thermal spray coating is progressively replacing the other classical hard coatings such as chrome plating and ceramic coating by the classical methods, since the very toxic $Cr^{6+}$ ion is well known as carcinogen causing lung cancer, and the ceramic coatings are brittle. Co-alloy T800 powder is coated on the Inconel 718 substrates by the HVOF coating procesess developed by this laboratory. For the study of the possibility of replacing of chrome plating, the wear properties of HVOF Co-alloy T800 coatings are investigated using the reciprocating sliding tester with a counter sliding SUS 304 ball both at room and at an elevated temperature of $1000^{\circ}F\;(538^{\circ}C)$. The possibility as durability improvement coating is studied for the application to the high speed spindles vulnerable to frictional heat and wear. Wear mechanisms at the reciprocating sliding wear test are studied far the application to the systems similar to the sliding test such as high speed spindles. Wear debris and frictional coefficients of T800 coatings both at room and at an elevated temperature of $538^{\circ}C$ are drastically reduced compared to those of non-coated surface of Inconel 718 substrates. Wear traces and friction coefficients of both coated and non-coated surfaces are drastically reduced at a high temperature of $538^{\circ}C$ compared with those at room temperature. These show that the coating is highly recommendable far the durability Improvement coating on the surfaces vulnerable to frictional heat and wear.

• Journal of the Korean Society of Manufacturing Process Engineers
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• v.19 no.12
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• pp.56-61
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• 2020

Fuel economy has always been a major issue in the automobile industry, especially owing to the associated environmental concerns. It is widely known that only 5-20% of the energy generated by automobiles running on internal combustion engine engines is used as power, while the rest is consumed because of friction between components. The main components of the reciprocating piston type compressor used in vehicles, such as the shaft, swash plate, piston, and cylinder, cause severe energy loss owing to frictional contact between each other. The wear contact between the main shaft and the other components is particularly severe. Most quality issues arise owing to the sticking phenomenon that occurs between these parts. In this study, a coating solution to reduce friction is prepared by mixing adhesive solid lubricant, organic binder-polyadimide, inorganic binder (Binder), and graphite in four different ratios, and the best combination is determined.

• Korean Journal of Metals and Materials
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• v.50 no.8
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• pp.549-556
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• 2012

The tribological behavior of CrMoN films with respect to surface chemistry was investigated by using X-ray photoelectron spectroscopy (XPS). All of the films were prepared from a hybrid PVD system consisting of DC unbalanced magnetron (UBM) sputtering and arc ion plating (AIP) sources. The tribological property of the films was evaluated by a friction coefficient using a Ball-on-disk type tribometer. The chemistry of wear track was analyzed by energy dispersive spectroscopy (EDS) and XPS. The friction coefficient was measured to be 0.4 for the CrMoN film, which is lower than that of a monolithic CrN film. EDS and XPS results imply the formation of an oxide layer on the coating surface, which was identified as molybdenum oxide phases, known to be a solid lubricant during the wear test.

• Journal of the Korean Society of Visualization
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• v.17 no.3
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• pp.39-45
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• 2019

A study on the sloshing flow of highly-viscous fluid in a rectangular box was made by both of theoretical approach and experimental visualization method. Assuming a smallness of external forcing to oscillate the container, it was investigated a linear sloshing flow of highly-viscous fluid utilizing asymptotic analysis by Taylor-series expansion as a small parameter R_e (≪1) in which R_e denotes Reynolds number. The theory predict that, during all cycles of sloshing, a linear shape of free surface will prevail in a bulk zone and it has confirmed in experiment. The relevance of perfect slip boundary condition, adopted in theoretical approach, to the bulk zone flow at the container wall was tested in experiment. It is found that quasi-steady coated thin film, which makes a lubricant layer between bulk flow and solid wall, is generated on the wall and the film makes a role to perfect slip boundary condition.

• Journal of the Korean institute of surface engineering
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• v.44 no.6
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• pp.269-276
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• 2011

Phase evolution and tribological behavior of Cr-Mo-N multi compositional films with different interlayer were investigated. The films were deposited by hybrid PVD (Physical Vapor Deposition) system consisted of dc unbalanced magnetron (UBM) sputtering and arc ion plating (AIP) sources. A pure molybdenum (Mo) was used as sputtering target and also a pure Cr was used as AIP target to form the Cr-Mo-N films. Various growth planes were found, no textured surface, in all of the multi composition films. Maximum value of microhardness was measured in Cr-Mo-N film with Mo interlayer as 29 GPa. Composition film was mainly showed the aspect of the adhesive wear than CrN film. The friction coefficient was decreased from 0.6 for pure CrN coating to 0.35 for Cr-Mo-N film with Mo interlayer. This result may come from the formation of metal oxide tribo-layer which is known as solid lubricant during the wear test.