• 제목/요약/키워드: Soda glass

검색결과 257건 처리시간 0.024초

SEM-EDS를 이용한 경남 김해 양동리 출토 유리구슬의 분석 고찰 (SEM-EDS Microanalysis of Glass Beads Excavated from Yangdong-ri Remains, Kimhae)

  • 김규호;허우영;김동원
    • 보존과학회지
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    • 제7권1호
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    • pp.23-30
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    • 1998
  • 고대 유리제품에 대한 과학적 분석 조사는 다양한 정보를 제공한다. 이 중에서 조성 분석을 통하여 사용 원료, 제작 방법, 시대, 그리고 지역으로 그룹화하여 문화 수준과 유입 경로등을 이해하는 자료로 활용할 수 있다. 본 연구에서는 유리나 도자기의 유약 등으로 이루어진 문화재 시료에 대한 SEM-EDS의 정량분석 조건들을 설정하였고, 경남 김해 양동리에서 출토된 유리 구슬 조각 62점을 정량분석하였다. 분석 결과, 이 지역의 유리구슬은 알칼리계 유리로써 칼리계 유리는 AD 1세기, 소다계 유리는 AD 2세기 말~3세기 초부터 나타난 것으로 추정되었다. 유리의 색상은 전이금속 구리, 철, 그리고 망간의 함유량과 밀접한 관계가 있음을 보인다. 이 분석결과는 고대 유리구슬의 성분 함유량이 원료, 색상, 유구편년, 그리고 지역에 따라 그룹이 형성될 수 있음을 확인하였다.

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SOFC용 유리-세라믹섬유 복합기밀재의 고온 기체누설 거동 (High Temperature Gas Leak Behavior of Glass-Ceramic Fiber Composite Seals for SOFC Applications)

  • 이재춘;권혁천;권영필;박성;장진식;이종호;김주선;이해원
    • 한국세라믹학회지
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    • 제42권12호
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    • pp.842-845
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    • 2005
  • Glass composites containing ceramic fiber have been developed for Solid Oxide Fuel Cell (SOFC) seals. Effect of glass type, loading pressure and thermal cycle the leak rates of composite seals was investigated. Seal performance of two commercial glasses was compared with that of $SiO_2BaO-B_2O_3$ glass synthesized in this work. The leak rate for seals made of pyrex(R) increases from $\~0.0005\;to\;\~0.004sccm/cm$ as the gas pressure increases from 10 to 50 kPa. The soda lime silicate glass seal shows the leak rate two times higher than the one made of pyrex(R) or $SiO_2BaO-B_2O_3$ glass. The viscosity of glass at the seal test temperature is presumed to affect the leak rate of the glass seal. As the applied loading pressure increases from 0.4 to 0.8 MPa at $750^{\circ}C$, the leak rate decreases from 0.038 to 0.024 sccm/cm for composite seals. It has been found that during 50 thermal cycles between $450^{\circ}C\;to\;700^{\circ}C$ leak rates remained almost constant, ranging from 0.025 to 0.03sccm/cm. The results showed an excellent thermal cycle stability as well as sealability of the glass matrix ceramic fiber composite seals.

High Xe-content PDP

  • Oversluizen, G.;Dekker, T.
    • 한국정보디스플레이학회:학술대회논문집
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    • 한국정보디스플레이학회 2004년도 Asia Display / IMID 04
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    • pp.55-58
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    • 2004
  • High Xe-content PDP characteristics are discussed. A high efficacy, up to 5 lm/W for a 50% Xe in Ne gas mixture, is realized in 4-inch color PDP test panel designs with low cost stripe-type barrier rib structures, that are powder blasted in soda lime glass. Furthermore, for a high Xe-content a high luminance can be obtained with a relatively small electrode area. Therefore the inter cell gap and the driving margin can be increased in a stripe-type barrier rib structure. Finally, for a high Xe-content the panel lifetime increases, due to increasing luminance and firing voltage stability. Clearly, these findings may direct the design development for next generation PDPs towards a high Xe-content

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열충격하에 있는 균열체의 파괴시간 (Fracture time of cracked body under thermal shock)

  • 이강용;박정수
    • 오토저널
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    • 제14권6호
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    • pp.91-98
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    • 1992
  • In the research on the fracture time of soda lime silicate glass under thermal shock, it is shown that the theoretical and experimental fracture times are in good agreement, the suggested method to measure critical stress intensity factor for small three-point bending specimen is useful and the edge temperature before thermal shock on cracked side vs. crack length and fracture time are inversely proportional.

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Chirped 회절격자를 이용한 집적형 파장분할 다중화기 제작 및 특성 측정 (Fabrication and characterization of integrated optic wavelength demultiplexer using a chirped grating)

  • 서만수
    • 한국광학회:학술대회논문집
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    • 한국광학회 1990년도 제5회 파동 및 레이저 학술발표회 5th Conference on Waves and lasers 논문집 - 한국광학회
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    • pp.232-236
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    • 1990
  • Optical waveguide was fabricated in the soda lime glass substrate using rapid thermal method. A chirped grating having period variation of 0.41 - 0.51${\mu}{\textrm}{m}$ on this waveguide for WDM was made. And then, arranging input and output optical fiber, wavelength division multiplexer with 5 channels in short wavelength region was realized. Experiment result of this WDM showed that wavelength spacing, 3 dB bandwidth, insertion loss and crosstalk were 5nm, 4nm, 40dB and less than -10dB, respectively.

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MIXED-MODE CRACK PROPAGATION BY MOVABLE CELLULAR AUTOMATA METHOD

  • Pak, Mik-Hail;Lee, Choon-Yeol;Chai, Young-Suck
    • 대한기계학회:학술대회논문집
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    • 대한기계학회 2007년도 춘계학술대회A
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    • pp.1754-1759
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    • 2007
  • Propagation of a mixed-mode crack in Soda-Lime silica glass using Movable Cellular Automata (MCA) method is demonstrated in this study. In MCA method, special fracture criterion is used to describe the process of crack initiation and propagation. Comparison between MCA and other crack initiation criteria results are made. The crack resistance curves and bifurcation angles under different loading angles are found. In comparisons with results of maximum circumferential tensile stress criterion, MCA result showed the sufficient agreement.

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유리표면에 진공증착된 금박막의 전기전도도의 습도 의존성 (Humidity Dependence of Electrical Conductivity of Vacuum Evaporated Au Films on Glass)

  • 이동영;박현수
    • 한국세라믹학회지
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    • 제24권6호
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    • pp.572-578
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    • 1987
  • The vacuum evaporated Au films on soda-lime glasses were measured by the electrical conductivity with the variation of the annealing time, relative humidity, and temperature. Au films structures were observed by scanning Electron Microscope and X-ray Diffractometer. As the annealing time and temperature increased, the electrical conductivity was increased due to the migration or annihilation of defects, but the electrical conductivity was decreased as with the relative humidity increased. Au films by XRD and SEM examination showed the negligible effect of chemical reactions.

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$Eu^{3+}$가 첨가된 광변환 유리의 특성과 효과연구 1(유리의 제조와 특성) (Characteristics of Photo-conversion Glass with $Eu^{3+}$ and Its Use 1 (Glass Production and Photo-conversion Characteristics))

  • 정헌생;안양규;길대섭
    • 한국태양에너지학회 논문집
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    • 제22권4호
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    • pp.44-50
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    • 2002
  • Photosynthesis of plants is effective in the range of 550 to 700 nm of the wavelength of solar irradiation. If the conversion of ultraviolet to the above mentioned region is possible, the photosynthesizing ability is expected to be enhanced. $Eu^{3+}$ doped soda-lime bulk and $TiO_2-SiO_2$ sol-gel coated glasses were prepared and their spectroscopic properties were studied. The absorption and emission spectra for the specimens were measured with the changes of wavelength and Eu ion concentration in the range of the wavelength of 300 to 700nm. The transmittance intensity of visible light through the bulk glass and the coated one was unchanged with the addition of Eu element. The emission spectrum intensity of $Eu^{3+}$ was found to be the maximum at 618 nm which is a transition of $^5DO{\rightarrow}^7F_2$. Additionally, it was shown that the intensity was linearly increased up to 10% of the Eu concentration.

저온실링용 ZnO-V2O5-P2O5계 봉착재의 물성에 미치는 TiO2 의 영향 (Effect of TiO2 on the Properties of ZnO-V2O5-P2O5 Low Temperature Sealing Glasses)

  • 이헌석;황종희;임태영;김진호;이석화;김일원;김남석;김형순
    • 한국재료학회지
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    • 제19권11호
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    • pp.613-618
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    • 2009
  • We designed new compositions for lead free and low temperature sealing glass frit of $ZnO-V_2O_5-P_2O_5$ system, which can be used for PDP (Plasma Display Panel) or other electronic devices. The $ZnO-V_2O_5-P_2O_5$ system can be used as a sealing material at temperatures even lower than 430$^{\circ}C$. This system, however, showed lower bonding strength with glass substrate compared to commercialized Pb based sealing materials. So, we added $TiO_2$ as a promoter for bonding strength. We examined the effect of $TiO_2$ addition on sealing behaviors of $ZnO-V_2O_5-P_2O_5$ glasses with the data for flow button, wetting angle, temporary & permanent residual stress of glass substrate, EPMA analysis of interface between sealing materials and glass substrate, and bonding strength. As a result, sealing characteristics of $ZnO-V_2O_5-P_2O_5$ system glasses were improved with $TiO_2$ addition, but showed a maximum value at 5 mol% $TiO_2$ addition. The reason for improved bonding characteristics was considered to be the chemical interaction between glass substrate and sealing glass, and structural densification of sealing glass itself.

라만분광분석법을 이용한 한국 고대 유리의 조성 분류 (Composition Classification of Korea Ancient Glasses by Using Raman Spectroscopy)

  • 심우석;김은아;임수영;김형민;김규호
    • 보존과학회지
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    • 제38권2호
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    • pp.117-123
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    • 2022
  • 본 연구는 한국의 고대 유리에서 납바륨유리 3점, 납유리 3점, 포타쉬유리 10점 그리고 소다유리 10점을 중심으로 라만분광분석법을 이용하여 고대 유리의 융제 분류와 납유리에서 납의 정량 분석에 대한 가능성을 분석하였다. 분석 결과, 신축 진동 영역에서 납바륨유리가 1040 cm-1, 납유리가 1000 cm-1으로 라만 피크 에너지의 차이를 보이며 포타쉬유리와 소다유리는 굽힘 진동 영역에서 Na과 K 양이온의 차이에 따라 포타쉬유리는 490 cm-1에서, 소다유리는 560 cm-1에서 라만 피크의 차이를 보인다. 이외에 납유리는 PbO 함량에 따라 라만 스펙트럼의 적색 편이가 비례하므로 이를 통하여 납유리의 주성분인 PbO의 함량을 정량적으로 분석할 수 있다. 즉, 라만분광분석법으로 납바륨, 납, 포타쉬 그리고 소다유리에 대한 분류와 납유리에서 PbO 함량을 측정할 수 있는 가능성이 확인된다.