• 제목/요약/키워드: Soaking process

검색결과 169건 처리시간 0.02초

담배 주맥 바이오매스의 압착추출특성 연구 (Study on the Mechanical Extraction Properties of Tobacco Stem Biomass)

  • 성용주;한영림;이문수
    • 펄프종이기술
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    • 제40권2호
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    • pp.65-72
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    • 2008
  • This work evaluated the extractability of tobacco stem biomass for the papermaking type Reconstituted Tobacco Sheet(RTS). The effects of the soaking conditions on the hydration of stem biomass and the effects of the hydrated state on the mechanical extraction were investigated. In order to simulate the mechanical expression process of a papermaking type RTS mill, for example, the screw press process, the novel mechanical pressing analyzer was developed for this study. The hydration of stem biomass by soaking process was greatly affected by the soaking time and the soaking temperature. The longer soaking time and the higher soaking temperature resulted in the higher hydrated stem biomass. Since the higher hydrated stem had more combined water in the inner structure and resulted in the more flexible structure, the higher hydrated stem leaded to the more compressed filter cake and the higher water contents in the filter cake after the mechanical pressing. The pilot pulping experiments showed the difference in hydration and extractability between burley and bright tobacco stem. The bulkier structure of the burley stem resulted in the faster hydration by pilot pulping and leaded to the larger reduction in water soluble components. And the hydration process showed the major influence on the separation efficiency of water soluble components.

침지공정에서의 탈수 및 용질 침투현상에 관한 고찰 (Study on Dewatering and Impregnation Soaking Process)

  • 최동원;신해헌;최형택
    • 한국식품영양학회지
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    • 제10권4호
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    • pp.462-467
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    • 1997
  • 최근 건조 및 탈수공정으로 사용되고 있는 침지(soaking)에 의한 방법인 DIS 공정(dewatering and impregnation soaking process)은 상온에서 침지용액에 식품시료를 담금으로서 시료내의 수분이 탈수되는 현상을 이용한 공정으로서 이 때 용액 속의 용질들이 시료 속의 세포 내로 침투하는 확산현상도 동시에 발생한다. 따라서 영양분의 손실과 관능적 품질저하를 억제할 수 있으며, 건조시의 에너지를 절감하는 등의 특성을 갖는다. DIS 공정에서는 용질의 크기에 따라 원형질막 분리현상과 세포벽 붕괴현상이 발생하며, 시료의 조직상태와 운전조건에 의하여 그 탈수 정도는 차이가 나타난다. DIS 공정을 제어하기 위한 모형화는 주로 비정상상태에서의 Fick의 법칙과 물질수지를 기초로 한 여러 가지 모델들이 제안되어 등온상태에서 시간에 따른 탈수량과 용질 침투량을 정확히 예측하고자 하고 있다.

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Combinational Effect of Moist Heating and Gamma Irradiation on The Inactivation of Trypsin Inhibitory Activity in Soybean

  • Felipe, Penelope;Yang, Yun-Hyoung;Lee, Jeong-Hee;Sok, Dai-Eun;Kim, Hyoung-Chin;Yoon, Won-Kee;Kim, Hwan-Mook;Kim, Mee-Ree
    • Food Science and Biotechnology
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    • 제14권6호
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    • pp.732-737
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    • 2005
  • The combinational effect of gamma irradiation and moist heating on the trypsin inhibitor activity (TIA) in soaked and dried soybeans was evaluated by measuring the inhibition using N-benzoyl-DL-arginine-p-nitroanilide (BAPNA) as substrate. Gamma irradiation significantly decreased the TIA level in soybean at doses above 5 kGy, and the $ID_{50}$ (the gamma irradiation dose required to reach 50% inhibition) value for TIA was 13.53 kGy. Soaking prior to gamma irradiation significantly lowered the $ID_{50}$ to 8.44 kGy, and the soaking process enhanced the efficiency to inactivate TIA by as much as 48%. When soaking prior to gamma irradiation was followed by subsequent mild heating ($60^{\circ}C$) process, the $IT_{50}$ (heating time required to reach the 50% inhibition of TIA) value at even 1 kGy (5.28 min) was greatly reduced by over 50% compared to the level for the no-soaking process. In addition, the activation energy of soaking prior to gamma irradiation at 1 kGy was 2.45 kcal/mole, which was also about 50% lower than the 5.10 kcal/mole of dried soybean gamma-irradiated. Based on these results, soaking prior to gamma irradiation is an effective method for TIA inhibition. Furthermore, a combination of two or more processing methods such as soaking, heating and gamma irradiation is much more effective than any single processing method.

콩의 수화 공정에서 수화 온도에 따른 콩(Glycine max)의 수화 및 단백질 용출 특성 (Effect of soaking temperature on soaking characteristics of soybean (Glycine max) during rehydration process)

  • 박현우;한원영;윤원병
    • Journal of Applied Biological Chemistry
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    • 제62권3호
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    • pp.251-255
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    • 2019
  • 콩의 수화 공정에서 수화 온도에 따른 수분함량의 변화 및 단백질 용출을 분석하기 위하여 콩의 수화 특성 및 단백질 용출특성을 확인하였다. 수화 온도가 증가함에 따라 콩의 수화 속도는 증가하는 경향을 나타내었으며, 이러한 수화 특성이 Peleg 모델을 통해 분석되었다($R^2>991$). 초기수분함량으로부터 목표수분함량(130%)까지 수화시키기 위해 25, 35 그리고 $45^{\circ}C$ 수화에서 필요한 수화시간은 각각 12.6, 3.11, 그리고 2.31시간을 나타내어 수화 온도가 증가함에 따라 목표함량에 도달하기 위한 수화시간이 급격히 짧아지는 것을 확인할 수 있었다. 수화공정에 따른 콩의 품질을 분석하기 위해 수화에 따른 단백질 용출량 또한 확인하였으며, 이 또한 Peleg 모델을 이용하여 분석하였다($R^2>0.941$). 단백질 용출 속도는 수화 온도가 증가함에 따라 증가하는 경향을 나타내었으며, 수화 온도가 증가함에 따라 수화에 필요한 시간도 줄어들지만 그에 따른 단백질 용출량 또한 증가하는 것을 확인할 수 있었다. 수분함량과 단백질 용출을 분석하기 위해 개발된 두 모델을 이용하여 목표수분함량까지 수화하였을 때의 콩의 단백질 용출량을 분석하였으며, 25, 35 그리고 $45^{\circ}C$에서 각각 35.2, 93.1 그리고 103.0 mg/g을 나타내어, $25^{\circ}C$의 수화온도에서 12.6시간의 수화시간이 콩의 품질을 고려한 최적 수화공정임을 확인하였다.

억새 바이오매스 전처리에서 압출 처리가 액상 암모니아 침지 처리에 미치는 영향 (The Effect of Extrusion Treatment on Aqueous Ammonia Soaking Method in Miscanthus Biomass Pretreatment)

  • 박선태;구본철;최용환;문윤호;안승현;차영록;김중곤;안기홍;서세정;박돈희
    • 신재생에너지
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    • 제6권4호
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    • pp.6-14
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    • 2010
  • Pretreatment of cellulosic biomass is necessary before enzymatic saccharification and fermentation. Extrusion is a well established process in food industries and it can be used as a physicochemical treatment method for cellulosic biomass. Aqueous ammonia soaking treatment at mild temperatures ranging from 60 to $80^{\circ}C$ for longer reaction times has been used to preserve most of the cellulose and hemicellulose in the biomass. The objective of this study was to evaluate the effect of extrusion treatment on aqueous ammonia soaking method. Extrusion was performed with miscanthus sample conditioned to 2mm of particle size and 20% of moisture content at $200^{\circ}C$ of barrel temperature and 175rpm of screw speed. And then aqueous ammonia soaking was performed with 15%(w/w) ammonia solution at $60^{\circ}C$ for 1, 2, 4, 8, 12 hours on the extruded and raw miscanthus samples respectively. In the combined extrusion-soaking treatment, most compositions removal occurred within 1~2 hours and on a basis of 1 hour soaking treatment values, cellulose was recovered about 85% and other compositions, including hemicellulose, are removed about 50% from extruded miscanthus sample. The combined extrusion-soaking treated and soaking only treated samples were subjected to enzymatic hydrolysis using cellulase and ${\beta}$-glucosidase. The enzymatic digestibility value of combined extrusion-2 hours soaking treated sample was comparable to 12 hours soaking only treated sample. It means that extrusion treatment can shorten the conventional long reaction time of aqueous ammonia soaking. The findings suggest that the combination of extrusion and soaking is a promising pretreatment method to solve both problems for no lignin removal of extrusion and long reaction time of aqueous ammonia soaking.

HEMT 소자 공정 연구 (Part 1. 금속박막 형성을 위한 Lift-off 공정연구) (A Study on HEMT Device Process (Part I. Lift-off Process for the Metallization))

  • 이종람;박성호;김진섭;마동성
    • 대한전자공학회논문지
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    • 제26권10호
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    • pp.1535-1544
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    • 1989
  • The overhang structure of photoresist in optical lithography was studied for the metallization of GaAs-related devices throughout lift-off method. Optical contact aligner with a dose of 8.5 m J/cm\ulcornerand with a wavelength of 300mm was used for ultraviolet exposure of single layer of S1400-27 photoresist. The overhang thickness shows a linear relationship with the soaking time in monochlorobenzene, which its magnitude becomes high at elevated softbake temperature. Such process conditions as a low softbake temperature, a long monochlorohbenzene soaking time and a little exposed energy make the development rate of photoresist lower. The optimum process conditions to obtain a target line-width, which include an appropriate overhang structure such as complete separation between the sidewall of photoresist pattern and the deposited metal edge, are determined as the softbake temperature of 64-74\ulcornerC, the monochlorobenzene soaking time of 10-15min, the ultraviolet exposure time of 70-100sec and the development time of 50-80sec.

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보조용매로 변형된 초임계 이산화탄소에 의한 감초의 triterpenoid saponin(glycyrrhizin)의 추출 (Extraction of Triterpenoid Saponin (glycyrrhizin) from Liquorice by Co-solvent Modified Supercritical Carbon Dioxide)

  • 김현석;김병용;임교빈
    • 한국식품과학회지
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    • 제34권6호
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    • pp.1057-1061
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    • 2002
  • 초임계 유체 추출법에 의해 감초의 triterpenoid saponin(glycyrrhizin)을 추출하기 위해 50 MPa, $60^{\circ}C$와 3mL/min의 조건에서 보조용매와 soaking의 효과를 알아보았다. 순수한 초임계 이산화탄소만을 이용하여 추출한 결과 감초의 glycyrrhizin은 거의 추출되지 않았다. 99.9% methanol, ethanol과 isopropanol을 보조용매로 초임계 이산화탄소에 첨가하여 추출한 경우, 추출수율의 상승에는 큰 영향을 미치지 아니하였다. 시료를 물로 soaking하여 90% methanol을 보조용매로 사용하여 초임계 이산화탄소에 의해 추출한 경우, soaking 용매의 사용량이 증가할수록 추출수율은 증가하였고, 최고 21.68mg/g(회수율 53.25%)의 수율을 보여주었다. 한편 시료의 soaking 없이 70% methanol을 보조용매로 사용하였을 때는 유기용매추출법에 의한 수율보다 더 높은 수율을 나타내었고, 시료를 물로 soaking하여 70% ethanol을 보조용매로 초임계 이산화탄소에 첨가하여 추출하였을 때, 추출수율과 추출속도는 상승하였고, 시료의 90%(w/w)에 해당하는 물로 시료를 soaking한 경우 70% methanol을 보조용매로 사용하였을 때와 거의 동일한 추출수율을 얻을 수 있었다.

Effects of Soaking pH and Extracting Temperature on the Physicochemical Properties of Chicken Skin Gelatin

  • Kim, Hyun-Wook;Song, Dong-Heon;Choi, Yun-Sang;Kim, Hack-Youn;Hwang, Ko-Eun;Park, Jae-Hyun;Kim, Yong-Jae;Choi, Ji-Hun;Kim, Cheon-Jei
    • 한국축산식품학회지
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    • 제32권3호
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    • pp.316-322
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    • 2012
  • This study was conducted to evaluate the effects of soaking pH and extraction temperature on the physicochemical properties of chicken skin gelatin. In order to extract gelatin from chicken skin, the chicken skin was soaked at various pH ranges (1-13) and was extracted at 75 and $100^{\circ}C$. For the rate of weight increase, the highest value was obtained from two pH ranges (1-2 and 12-13). In addition, the rate of weight increase was affected by soaking time. The alkali treatments had greater crude protein content as well as total extraction yield compared to the acid process (p<0.05), and the increased extraction temperature resulted in a significant (p<0.05) increase of crude protein content and total extraction yield. All treatments showed ${\alpha}1$ and ${\alpha}2$ chains derived from type I collagen on SDS-PAGE. The pH value and color of gelatin gel (6.67%) were affected by soaking pH and extraction temperature. Chicken skin gelatin gel extracted at $75^{\circ}C$ after soaking at a pH of 2 had the highest melting point (p<0.05) and gel strength among all treatments. Although the chicken skin treated with the alkali process had a higher yield, a lower extraction temperature following the acid process would be better for obtaining superior gelatin from chicken skin.

Effects of a Soaking-Fermentation-Drying Process on the Isoflavone and ${\gamma}$-Aminobutyric acid Contents of Soybean

  • Kim, Tae-Jin;Sung, Chang-Hyun;Kim, Young-Jin;Jung, Byung-Moon;Kim, Eung-Ryool;Choi, Won-Sun;Jung, Hoo-Kil;Chun, Ho-Nam;Kim, Woo-Jung;Yoo, Sang-Ho
    • Food Science and Biotechnology
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    • 제16권1호
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    • pp.83-89
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    • 2007
  • In our study, lactic acid bacteria (LAB)-fermented whey solutions were applied in the soybean soaking process to minimize bacterial contamination and to enrich the biologically functional components of isoflavone and $\gamma$-aminobutyric acid (GABA). Among the 11 LAB tested, Bifidobacteria infantis and a mixed culture (Lactobacillus acidophilus, Bifidobacteria lactis, and Streptococcus thermophilus; ABT-3) displaying the greatest $\beta$-glucosidase activity were selected to produce improved biologically functional soybean preparations. In the soybean soaking processing (without water spraying), the LAB-cultured 10% whey solution was used to soak and to ferment the soybeans and the fermented soybeans were finally dried by heat-blowing at $55^{\circ}C$. The processing conditions used in this study demonstrated that the final soybean product had a reduced contamination by aerobic and coliform bacteria, compared to raw soybeans, likely due to the decrease in pH during LAB fermentation. The aglycone content of the isoflavone increased up to 44.6 mg per 100 g of dried soybean by the processing method, or approximately 8-9 times as much as their initial content. The GABA contents in the processed samples increased as the processing time of soaking-fermentation proceeded as well. The soybean sample that fermented by ABT-3 culture for 24 hr showed the greatest increase in GABA content (23.95 to 97.79 mg/100 g), probably as a result of the activity of glutamate decarboxylases (GAD) released from the soybean or produced by LAB during the soaking process.

명종 응고제를 사용한 두부의 침수시간에 따른 무형성분의 변화 (II) (A Study on Soybean Curds Prepared with Various Coagulants -Mineral Contents in Various Stages of Soaking Time-)

  • 문수재
    • 대한가정학회지
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    • 제18권2호
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    • pp.15-21
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    • 1980
  • Three kinds of soybean curd were prepared with three coagulants such as calcium chloride, magnesium chloride and glucono delta lactone. The mineral contents of the three soybean curds were analyzed before soaking and after various lengths of soaking(1/2 hour, 1 hour, 2 hours, and 2 hours(water changed after 1/2 hour)). Results therefrom were as follows: 1. Before the three soybean cured were soaked, their moisture contents were 79-83g/%. The ash contents were 5.04g% in the soybean curd made with CaCl_{2}4.42g/% in the soybean curd prepared with MgCl_{2} and 3.86g/% in the soybean curd coagulated by glucono delta lactone. an analysis of calcium, magnesium and phosphorous contents showed that each element had a greater concentration in the soybean curds made with divalent mineral salts than in the soybean curd made with acid. 2. Changes taking place in the mineral contents of the soybean curds according to different soaking times were examined. The mineral contents tended to decease in process of soaking time. The soybean curds showed the highest rate of mineral dissolution after one hour of soaking, and then they tended to reabsorb minerals. When the soybean curds were soaked I freshly changed water for one hour and 30 minutes, their mineral contents indicated a greater diminishing trend but no significant difference was noticed among the different kinds of soybean curd. In case coagulant has been used excessively, it is necessary to soak the bean curds for about one hour to get the coagulant dissolved.

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