• Title/Summary/Keyword: Slurry temperature

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CHARACTERIZATION OF MONOLITHIC RS-SiC AND RS-$SiC_f/SiC$ COMPOSITE MATERIALS (반응소결 SiC 재료와 $SiC_f/SiC$ 복합재료의 특성)

  • Jin, Joon-Ok;Lee, Sang-Pill;Lee, Jin-Kyung;Yoon, Han-Ki;Khoyama, Akira
    • Proceedings of the KSME Conference
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    • 2003.04a
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    • pp.376-380
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    • 2003
  • The microstructure and the mechanical properties of RS-SiC and RS-$SiC_f/SiC$ materials have been investigated in conjunction with the content of residual silicon and porosity. The mechanical properties of RS-SiC materials suffered from the thermal exposure were also examined. RS-SiC based materials bave been fabricated using the complex matrix slurry with different composition ratios of SiC and C panicles. The characterization of RS-SiC based materials was investigated by means of SEM, EDS ~d three point bending test. Based on the mechanical property-microstructure correlation, the high temperature applicability of RS-SiC based materials was discussed.

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Synthesis and disperse treatment of Cu powder from $Cu(OH)_2$ slurry by wet reduction methods (액상환원법에 의한 $Cu(OH)_2$ 슬러리로부터 미세구리분말 제조 및 분산화 처리)

  • Ahn Jong-Gwan;Hai Hoang Tri;Kim Dong-Jin;Kim Byeong-Gyu
    • Proceedings of the Korean Powder Metallurgy Institute Conference
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    • 2005.11a
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    • pp.87-88
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    • 2005
  • Ultra-fine copper powders with particle size about 150 nm were synthesized from copper hydroxide slurry by wet method using hydrazine as reduction agent and several sur factants at below $80^{\circ}C$. The particle size distribution and dispersion of synthesized powders as function of temperature, feeding rate of reduction and especially, sur factants were character ized by XRD, BET, PSA and SEM by this process.

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Growth of Ice Crystal with Concentration of Surfactant in Water Solution (계면활성제 농도가 빙결정의 입자크기에 미치는 영향)

  • ;稻葉英男
    • Journal of Advanced Marine Engineering and Technology
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    • v.26 no.2
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    • pp.240-247
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    • 2002
  • Recently, a thermal energy storage system has been developed actively fur the purpose of saving energy and reducing the peak electrical demand. Especially, ice slurry is a promising working fluid for low temperature energy storage systems. A flow of ice crystals has a large cooling capacity as a result of the involvement of latent heat. However, there are still problems related to the recrystallization of ice crystals for realizing long term storage and long distance transportation. To find improvements fur this, a method for the creation of ice crystals resistant to recrystallization has been proposed and researched by the use of an antifreeze protein (AFP) solution etc. In the present study, it has been investigated the growth of ice crystal in several kinds of water solution added non-ionic surfactant. The results shows that size of ice crystal was smaller with increasing in added surfactant. And ice crystal was not increased with added surfactant.

Influence of Control Pressure and Concentration of Water Solution at Continuous Ice Making in a Tube (제어압력 및 수용액의 농도가 관내 연속제빙에 미치는 영향)

  • ;;Hideo Inaba;Akihiko Horibe;Naoto haruki;Hidetoshi Miura
    • Korean Journal of Air-Conditioning and Refrigeration Engineering
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    • v.13 no.12
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    • pp.1236-1244
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    • 2001
  • In the present study, the possibility of continuous slurry ice making using flowing water solution in a cooled tube has been investigated. The experiments were carried out at various concentration and velocity of water solution, temperature of cooled tube wall, and control pressure in a tube. As a result, four types of operating conditions, that is super-cooling, continuous ice making, intermittent ice making and ice blockage, were classified. And it was found that the critical condition for the continuous ice making was acquired as a function of these experimental parameters.

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Preparation of Fine Co Powder from Co(OH)2 Slurry by Hydrothermal Reduction with Hydrogen

  • Kening Yu;Kim, Dong J.;Hun S. Chung
    • Proceedings of the Korea Association of Crystal Growth Conference
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    • 1996.06b
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    • pp.87-107
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    • 1996
  • The fine Co powder with an average particle sie of less than 1$\mu\textrm{m}$ was prepared by hydrothermal reduction with hydrogen from Co(OH)2 slurry obtained by mixing the solutons of CoSO4$.$7H2O and NaOH. A method to control pH of the end solution around neutrality was proposed. The reduction rate was found to be a function of pH, temperature, hydrogen pressure and the amount of catalyst.

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Slurry Phase Reaction of Elemental Silicon with Methanol in the Presence of Copper: Direct Synthesis of Trimethoxysilane

  • Han, Joon-Soo;Cho, Joo-Hyun;Lee, Myong-Euy;Yoo, Bok-Ryul
    • Bulletin of the Korean Chemical Society
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    • v.30 no.3
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    • pp.683-686
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    • 2009
  • Slurry phase reaction of elemental silicon with methanol has been studied in the presence of copper using a small amount of cuprous chloride as an activator in DBT (dibenzyltoluene) at various temperatures from 200 ${^{\circ}C}$ to 320 ${^{\circ}C}$. Trimethoxysilane (1a) with a Si-H unit was obtained as the major product and tetramethoxysilane (1b) as the minor product. The reaction worked well using a 0.5 wt % CuCl as an activator. The optimum temperature for this direct synthesis of 1a was 240 ${^{\circ}C}$. Methoxysilanes were obtained in 95% yield with 81% selectivity to 1a from 85% conversion of elemental silicon.

Fabrication of SiC Fiber-SiC Matrix Composites by Reaction Sintering

  • Lim, Kwang-Young;Kim, Young-Wook;Park, Ji-Yeon
    • Journal of the Korean Ceramic Society
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    • v.45 no.4
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    • pp.204-207
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    • 2008
  • This paper presents a new process for producing SiC fiber-SiC matrix(SiC/SiC) composites by reaction sintering. The processing strategy for the fabrication of the SiC/SiC composites involves the following: (1) infiltration of the SiC fiber fabric using a slurry consisting of Si and C precursors, (2) stacking the slurry-infiltrated SiC fiber fabric at room temperature, (3) cross-linking the stacked composites, (4) pyrolysis of the stacked composites, and (5) hot-pressing of the pyrolyzed composites. It was possible to obtain dense SiC/SiC composites with relative densities of >96% and a typical flexural strength of ${\sim}400$ MPa.

Simulation of Refrigeration System with MPCM slurry (마이크로캡슐 잠열재 적용 냉동기의 성능 시뮬레이션)

  • Cho, Jong-Min;Kim, Yong-Chan;Cheon, Deok-Woo;Yoon, Joon-Sang
    • Proceedings of the SAREK Conference
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    • 2006.06a
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    • pp.1213-1218
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    • 2006
  • In this study, a numerical model for a vapor compression refrigeration system using MPCM slurries as a secondary fluid through an evaporator was developed, and the system performance was compared with that using water Generally, the MPCM system showed higher performance than the water system. The COP of the MPCM system was higher by 16.6 to 18.6% than that of the water system at all conditions. The MPCM slurry yields better performance in the aspect of heat transfer and heat transportation comparing to the sensible heat transfer medium such as water.

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Tunable properties and low temperature sintering of BST thick films added ${Li_2}{CO_3}$ (${Li_2}{CO_3}$첨가에 의한 $BaSr(TiO_3)$의 저온 소결과 가변유전 특성)

  • Kim, In-Sung;Min, Bok-Ki;Jeong, Soon-Jong;Song, Jae-Sung;Jeon, So-Hyun
    • Proceedings of the KIEE Conference
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    • 2006.10a
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    • pp.7-9
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    • 2006
  • $(BaSr)TiO_3$ thick films were prepared by tape casting method using $BaTiO_3$ and $SrTiO_3$ powder slurry in order to investigate dielectric properties and low temperature sintering. Sintering density was $5.7\;g/cm^3$ and the BST sample exhibited the maximum dielectric constant, tunability at temperatures near phase transition point. The dielectric constant was increased and curie temperature was shifted to higher temperature with increasing of annealing temperature.

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An Experimental Approach to Evaluate the Desulfurization Yield in Spray Drying Sorber (반건식 세정기의 산성가스 제거성능에 관한 실험적 연구)

  • Yang, Hyun-Mo;Kim, Sang-Soo
    • Transactions of the Korean Society of Mechanical Engineers B
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    • v.24 no.4
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    • pp.589-598
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    • 2000
  • A pilot-scale Spray Drying Sorber (SDS) system was set up to evaluate the effect of spray characteristics on the desulfurization yield. The size distribution and the Sauter Mean Diameters of slurry droplets were measured in advance using the optical size measurement system, Malvern 2600. The desulfurization yield of the drying chamber by size was measured for the conditions of inlet gas and spray injection. As a reagent, 10% limestone slurry of $Ca(OH)_2$ was treated with flue gas containing $SO_2$, and the combustion gas analyzer and gas detectors were attached to measure the $SO_2$ concentration. With a flow rate of 144 Nm3/h and a temperature range of $200{\sim}300^{\circ}C$, the experiments were performed for the Stoichiometric Ratio (SR) of 1.0 to 3.0 and droplet mean diameter of 6.5 to $34.3{\mu}m$. In case of smaller spray droplets, the desulfurization efficiency improved due to the increase of total droplet surface area, while the reduction in evaporation time reduced the contact time between the droplets and $SO_2$ gas. In some typical region of droplet diameter, this negative effect, reduction of contact time, became dominant and the desulfurization yield decreases the desulfurization yield in spite of the expansion in absorption area. These results revealed that there exists the optimal size of spray droplets for a given state, which is determined by the compromise between the total surface area of slurry droplets and the evaporation time of droplets. The measurements also indicated that the inlet temperature of flue gas changes the optimal injection condition by varying the driving force for evaporation. The results confirm that the effect of the evaporation time of slurry droplets should be considered in analyzing the desulfurization yield as well as the total surface area, for it is a significant aspect of the correlation with the capabilities of $SO_2$ absorption in wet droplets. In conclusion, the optimal condition of spray can be determined based on these results, which might be applied to design or scale-up of SDS system.