• Tribology and Lubricants
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• 제15권2호
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• pp.184-192
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• 1999

Various compositions of$ Cr_2$$O_3$/Mo composite powders were fabricated using spray-drying method and plasma-spray coatings of these powders were prepared to understand their tribological properties. Experiments were conducted using a reciprocal type tribo-tester at room temperature under dry sliding condition. The worn surface of coated specimens were observed using SEM (Scanning Electron Microscopy) and chemical compositions were analyzed using XRD (X-ray Diffractometry) and XPS (X-ray Photoelectron Spectroscopy). The results showed that friction coefficient of the Mo added specimens were lower than that of $Cr_2$$O_3$specimen. However $Cr_2$$O_3$specimen showed the lowest wear loss. Wear protecting layer were observed at the worn surface of coated specimens with Mo addition. From the XPS analysis, the mixed phases of $Cr_2$$O_3$ $CrO_3$and $MoO_3$were founded in the wear protecting layer.

• 한국추진공학회지
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• 제17권3호
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• pp.15-20
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• 2013

Graphite는 고온/고압의 가스가 추진기관 내의 구동장치에 유입되지 않게 기밀 소재로 사용되며, 마모 과정에서 윤활막을 형성하여 구조물 안에서 윤활과 기밀을 돕는다. 본 연구는 기밀 소재로 사용되는 Graphite의 고온 마모 시험을 통해 고온 마모 특성을 평가하였다. 고밀도 Graphite (HK-6)에 대하여 실제 작동환경에 기초 한 온도, 미끄럼 속도, 접촉 하중 조건에 따른 마모 특성을 평가 및 고찰하였다. 마모 표면 관찰을 통해 마모 메카니즘을 파악하고 고온 마모 특성을 통하여 최적화된 작동 환경 조건에 대하여 제안 하였다. 결과적으로, 상온에서 보다 고온 환경에서 윤활막 형성에 유리 하여 마찰 계수가 비교적 낮게 나타나는 것을 알 수 있다.

• Tribology and Lubricants
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• 제28권3호
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• pp.117-123
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• 2012

Tribological properties of hybrid type friction materials were studied. Hybrid friction materials were produced by combining non-steel(NS) and low-steel(LS) type friction materials. The emphasis of the investigation was given to possible synergistic effects from the two different friction materials, in terms of friction stability at high temperatures and the amplitude of friction oscillation, also known as stick-slip at low sliding speeds. The high temperature friction test results showed that the friction effectiveness of the hybrid friction material was well sustained compared to LS and NS friction materials. Wear resistance of the hybrid type was similar to LS friction materials. Examination of the rubbing surfaces after tests revealed that the friction characteristics of the hybrid friction material were attributed to the wear debris produced from low-steel friction materials, which were migrated to the surface of the non-steel friction material, forming new contact plateaus. The stick-slip amplitude and its frequency were pronounced when non-steel friction material was tested, while hybrid and low-steel types showed relatively small stick-slip amplitudes. These results suggest possible improvement of tribological properties by designing a hybrid composite of low-steel and non-steel friction materials.

• KSTLE International Journal
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• 제6권2호
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• pp.39-44
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• 2005

Friction and wear properties of the Boron carbide ($B_{4}C$) coating 100 nm thickness were studied under various relative humidity (RH). The boron carbide film was deposited on silicon substrate by DC magnetron sputtering method using $B_{4}C$ target with a mixture of Ar and methane ($CH_4$) as precursor gas. Friction tests were performed using a reciprocation type friction tester at ambient environment. Steel balls of 3 mm in diameter were used as counter-specimen. The results indicated that relative humidity strongly affected the tribological properties of boron carbide coating. Friction coefficient decreased from 0.42 to 0.09 as the relative humidity increased from $5\%$ to $85\%$. Confocal microscopy was used to observe worn surfaces of the coating and wear scars on steel balls after the tests. It showed that both the coating surface and the ball were significantly worn-out even though boron carbide is much harder than the steel. Moreover, at low humidity ($5\%$) the boron carbide showed poor wear resistance which resulted in the complete removal of coating layer, whereas at the medium and high humidity conditions, it was not. X-ray photoelectron spectroscopy (XPS) and Auger electron spectroscopy (AES) analyses were performed to characterize the chemical composition of the worn surfaces. We suggest that tribochemical reactions occurred during sliding in moisture air to form boric acid on the worn surface of the coating. The boric acid and the tribochemcal layer that formed on steel ball resulted in low friction and wear of boron carbide coating.

• Carbon letters
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• 제10권2호
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• pp.94-96
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• 2009

[ $C_f/C-Cu$ ]composites were fabricated by infiltrating molten Cu into different $C_f/C$ preforms prepared by chemical vapor infiltration, resin impregnation and carbonization. The microstructure and properties of the composites were investigated. The results show that Cu in the composites filled the pores and showed network-like distribution. Compared with homemade J204 brush material and certain grade pantograph slider from abroad, the composites have higher flexural strength and better electrical conductivity. The friction and wear properties of the composites are better than that of J204, and closed to that of the abroad material.

• 대한기계학회논문집
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• 제19권4호
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• pp.968-980
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• 1995

Al/Al$_{2}$O$_{3}$/C hybrid metal matrix composites are fabricated by the direct squeeze infiltration method. From the microstructure of Al/Al$_{2}$O$_{3}$/C composites, uniform distribution of reinforcements and good bondings are found. Optimum processing conditions for preforms and squeeze castings are suggested. Mechanical properties, such as elastic modulus, elongation, 0.2% offset yield strength and ultimate tensile strength are obtained. Through the abrasive were test and wear surface analsis, wear behavior and its mechanism of AC2B aluminum and Al/Al$_{2}$O$_{3}$/C composites can be characterized under various sliding speed conditions. Tensile strenght elongation of Al/Al$_{2}$O$_{3}$/C composites are decreased with increasing the addition of carbon fiber. On the contrary, elastic modulus of Al/Al$_{2}$O$_{3}$/C composites is slightly improved compared with that of the unreinforced matrix alloy. The addition of carbon fiber to al/al$_{2}$O$_{3}$/C composites gives rise to improvement of the wear resistance. Specially, carbon chopped fibers play an important role in interfering sticking between the counter material and metal matirix composites. Al/Al$_{2}$O$_{3}$/C composites are suitable to high speed due to solid lubication of carbon. And wear model of Al/Al$_{2}$O$_{3}$/C composites is suggested by the examination of worn surfaces.

• Journal of Welding and Joining
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• 제17권5호
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• pp.107-115
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• 1999

The objective of this research was to study the formation of the thick hardened layer with the addition of metal powder(Cu) and ceramics powders(TiC) on the aluminum 5083 alloys by plasma transferred arc process(PTA process) and to characterize the effect of overlaying conditions on the overlaid layer formation. This was followed by investigating the microstructures of the overlaid layers and mechanical properties such as hardness and wear resistance. The overlaid layer containing copper powder was alloyed and intermetallic compound($CuAl_2$) was formed. The overlaid layers with high melting point TiC powders, however, did not react with base metal. Wear resistance of the alloyed layer was remarkably improved by the formation of $CuAl_2$, precipitate phase, which prevented wear of base aluminum alloys and at higher wear speed, accelerated sliding of the counter part. Wear resistance of the composite layer was also remarkably improved because TiC powder act as a load barring element and Fe debris fragments detached from the counter part act as a solid lubricant on the contact surface.

• 한국윤활학회:학술대회논문집
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• 한국윤활학회 1999년도 제30회 추계학술대회
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• pp.49-56
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• 1999

A material was formulated with Phenol novolac and HEXA only. The cure kinetics and thermal characteristics of phenol novolac with various HEXA contents were peformed by differential scanning calorimetry and thermal gravimetric analysis. All kinetic parameters of the curing reaction including the reaction order, activation energy, and rate constant were calculated and reported. The results indicate that the curing reaction goes through an autocatalytic kinetic mechanism. The friction and wear characteristics of this material were determined using friction material testing machine. The friction coefficient of phenol novolac with various HEXA contents was determined using the PV(pressure & velocity) factor. The most stable and highest friction coefficient with a various pressure and velocity condition was found at HEXA 10 wt.% material. The specific wear rate per unit sliding distance with a various HEXA contents was reported.

• 한국해양공학회:학술대회논문집
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• 한국해양공학회 2004년도 학술대회지
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• pp.347-351
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• 2004

[ $Si_3N_4$ ] composites have been extensively studied for engineering ceramics, because it has excellent room and high temperature strength, wear resistance properties, good resistance to oxidation, and good thermal and chemical stability. In the present work, carbon short fiber reinforced $Si_3N_4$ ceramics were fabricated by hot press method in $N_2$ atmosphere at $1800^{\circ}C$ using $Al_2O_3\;and\;Y_2O_3$ as sintering additives. Content of carbon short fiber was $0\%,\;0.1\%\;and\;0.3\%$. The composites were evaluated in terms of density, flexural strength and elastic modulus through the 3-point bending test at room temperature. Also, The wear behavior was determined by the pin on disk wear tester using silicon nitride ball. Experimental density and flexural strength decreased with increasing content of carbon fiber. But specific modulus increased with increasing content of carbon fiber. In addition, friction coefficient and specific wear loss decreased with increasing content of carbon short fiber by reason of interfacial defects between matrix and fiber.

• 대한치과보철학회지
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• 제37권2호
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• pp.212-234
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• 1999

Dental restorative materials must have the physical properties to withstand wear and corrosion. Base metal alloys possess better mechanical properties and lower price than the gold alloys. For these reasons such alloys have largely replaced the precious metal alloys. One aspect to con-sider is the release of metal substances to oral environment. The release of elements from dental alloys is a continuing concern because the elements may have the potentially harmful biological effects on local tissues. The purpose of this study was to minimize metal release on the nonprecious metal surfaces by ion beam assisted deposition(IBAD) of titanium nitride (TiN) Ni-Cr-Be alloys with and without TiN coatings were secured in an wear test machine opposing ruby ball to determine their relative resistance to wear with loom, 200m, 300m and 400m sliding distance. And the corrosion behavior of the Ni-Cr-Be alloys with and without TiN coatings and 3 dental noble alloys have been studied. Potentiodynamic curves were used to analyse the corrosion characteristics of the alloys. The measurement of the released Ni and Cr ions was conducted by analysis of the electrolyte solution with atomic absorption spectroscopy. The results were as follows : 1. The critical sliding distance that wore down TiN coatings of $2.5{\mu}m$ thickness in this study condition was 300m. 2. Ion beam assisted deposition of TiN showed a good surface modification with respect to the properties of wear and corrosion resistance. 3. X-ray diffraction showed that the strongest peak of TiN is TiN(111) in the coatings. 4. The release of Ni and Cr ions from alloys measured by means of atomic absorption spectroscopy was reduced by ion beam assisted deposition of TiN.