• 제목/요약/키워드: Sintering rate

검색결과 391건 처리시간 0.062초

지르코니아 분말의 치밀화와 소결거동 : I. 가압에 따른 치밀화 응답 (Compaction and Sintering Behaviour of Zirconia Powders: I. Compaction Response)

  • 박홍채
    • 한국세라믹학회지
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    • 제29권6호
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    • pp.489-495
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    • 1992
  • The continuous compaction response of zirconia powders prepared by different processing treatments was investigated. Though the yield point could be or not below 1 MPa, the change of slope was always observed at high pressure range around 60 MPa. Powder compaction was mainly governed by second compaction stage and compaction rate was decreased with increasing forming pressure. Rotary vacuum dried powder favored a high compaction density, whereas freeze dried and calcined powders favored an increase in the pressing efficiency. In order to extract more reliable information about powder compaction, it was necessary to use not only compaction response diagram but also compaction rate diagram.

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Ni/Mo 합금분말(FLC-4608)의 소결경화 공정에서 유한요소법을 이용한 마르텐사이트 분율의 예측 (Prediction of Martensite Fraction in the Sintering Hardening Process of Ni/Mo Alloy Powder (FLC-4608) Using the Finite Element Method)

  • 박효욱;주수현;이언식;권기혁;김형섭
    • 한국분말재료학회지
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    • 제22권1호
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    • pp.10-14
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    • 2015
  • In recent years, industrial demands for superior mechanical properties of powder metallurgy steel components with low cost are rapidly growing. Sinter hardening that combines sintering and heat treatment in continuous one step is cost-effective. The cooling rate during the sinter hardening process dominates material microstructures, which finally determine the mechanical properties of the parts. This research establishes a numerical model of the relation between various cooling rates and microstructures in a sinter hardenable material. The evolution of a martensitic phase in the treated microstructure during end quench tests using various cooling media of water, oil, and air is predicted from the cooling rate, which is influenced by cooling conditions, using the finite element method simulations. The effects of the cooling condition on the microstructure of the sinter hardening material are found. The obtained limiting size of the sinter hardening part is helpful to design complicate shaped components.

Ni, Mn가 첨가된 PMN-PSS-PZT 세라믹스의 유전 특성에 관한 연구 (A Study on Dielectric Properties of PMN-PSS-PZI ceramics with Ni, Mn)

  • 신혜경;김현철;성낙진;배선기
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 2004년도 하계학술대회 논문집 Vol.5 No.2
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    • pp.764-767
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    • 2004
  • This study was to measure the minuteness structure, dielectric properties of (0.3-x)PMN - XPSS-0.7PZT+0.5wt%NiO+0.5wt%$MnO_2$(x=0.05, 0.10, 0.15, 0.20, 0.25)ceramics according to sintering temperature and PSS moi percentage after manufacturing the specimens with a general method. the results of this study were gotten such as follows. The crystal structure of ceramic has the rombohedral structure in XRD. it appeared that addition of Ni, Mn additive was helpful to the formation of stable structure. Dielectric constant at $20^{\circ}C$ showed its maximum value 890.001 in specimens sintered at $1000^{\circ}C$, x=0.15mol. and dielectric loss showed its minimum value 6.95[%] in specimens sintered at $1000^{\circ}$, x=0.05mol. The variation rate of dielectric constant according to the change of frequency was decreased by increasing frequency, The variation rate of dielectric constant according to the change of temperature was increased by increasing temperature.

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Powder Injection Molding of Translucent Alumina using Supercritical Fluid Debinding

  • Kim, Hyung Soo;Byun, Jong Min;Suk, Myung Jin;Kim, Young Do
    • 한국분말재료학회지
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    • 제21권6호
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    • pp.407-414
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    • 2014
  • The powder injection molding process having advantages in manufacturing three-dimensional precision parts essentially requires a debinding process before sintering to remove the binders used for preparing feedstock. In this study, powder injection molding of translucent alumina was performed, and carbon dioxide ($CO_2$) is used as a supercritical fluid that makes it possible to remove a large amount of binder, which is paraffin wax. The relationship between the optical property of translucent alumina and the debinding condition (temperature and pressure) of supercritical $CO_2$ was investigated. As temperature and pressure increased, extraction rate of the binder showed rising tendency and average grain size after sintering process was relatively fine. On the other hand, optical transmittance was reduced. As a result, the debinding condition at $50^{\circ}C$ and 20 MPa that represents the lowest extraction rate, $8.19{\times}10^{-3}m^2/sec$, corresponds to the largest grain size of $14.7{\mu}m$ and the highest optical transmittance of 45.2%.

Processing of Kaolin-Based Microfiltration Membranes

  • Eom, Jung-Hye;Kim, Young-Wook;Song, In-Hyuck
    • 한국세라믹학회지
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    • 제50권5호
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    • pp.341-347
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    • 2013
  • Kaolin-based membranes with a pore size of 0.30-0.40 ${\mu}m$ were successfully prepared by a simple pressing route using low-cost starting materials, kaolin and sodium borate. The prepared green bodies were sintered at different temperatures ranging between 900 and $1200^{\circ}C$. The sintered membranes were characterized by X-ray diffraction, mercury porosimetry, scanning electron microscopy, and capillary flowmetry. It was observed that the porosity decreased with an increase in both the sintering temperature and the sodium borate content, whereas the flexural strength increased with an increase in both the sintering temperature and the sodium borate content. The air flow rate decreased with an increase in the sodium borate content. The typical porosity, flexural strength, and specific flow rate of the kaolin-based membrane sintered with 5 wt% sodium borate at $1100^{\circ}C$ were 37%, 19 MPa, and $1{\times}10^{-3}L/min/cm^2$, respectively, at a p of 30 psi.

파인 세라믹스의 초음파 진동절삭에 관한 연구 (A study on the ultrasonic vibration cutting properties of fine ceramics)

  • 강종표;송지복
    • 한국정밀공학회지
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    • 제10권1호
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    • pp.126-133
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    • 1993
  • Conventional cutting(CC) and Ultrasonic Vibration Cutting(UVC) of 20[KHz] are practised with standard lathe for fine ceramics(A1$_{2}$O$_{3}$. UVC is suggested to good cutting method for difficult-to-machine-materials and it is known to excellent cutting method to super precision cutting and elevation of productibility for general, nonferrous matals. In this research, main results to be obtained are as follows: 1. From the CC and UVC results by general lathe with sintering diamond tool, the surface roughness and roundness are improved in UVC. Also tool life is longer in UVC than CC. From the observation of machined surface, it is found that brittle fracutural material remove occured in fine ceramics cutting. 2. It is verified that the thrust force is the biggest in fine ceramics cutting, principal force is the next, and feed rate force the third and it is appear a little, on the other hand the principal force is the biggest in metal cutting, feed rate frece is the second, and thrust force is the next.

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