• 제목/요약/키워드: Sintering Time

검색결과 672건 처리시간 0.029초

쾌속조형 기술과 진공성형법을 이용한 시작차량용 대형 중공 부품의 제작에 관한 연구 (A Study on the Manufacturing of Large Size Hollow Shape Parts for Prototype-Car using Rapid Prototyping Technology and Vacuum Molding)

  • 박경수;양화준;최경현;이석희
    • 한국정밀공학회:학술대회논문집
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    • 한국정밀공학회 2000년도 추계학술대회 논문집
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    • pp.362-365
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    • 2000
  • Rapid Prototyping(RP) techniques have revolutionized traditional manufacturing methods. These techniques allow the user to fabricate a part directly from a conceptual model before investing in production tooling and help develop new models with significant short time. This paper suggests to new process to manufacture large size hollow shape parts for prototype-car using Rapid Prototyping technology and Vacuum Molding with the reduction of delivery time. In addition, This paper introduces the dividing and combining method to make large size RP master model in spite of the limit of the build chamber dimensions of commercialized RP system and post-processing method to achieve sufficient surface quality.

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Al-isopropoxide로부터 AlN 소결체의 입계상 거동 및 열처리 효과 (Grain Boundary Behavior and Heat Treatment Effect of AlN Ceramics Prepared from Al-isopropoxide)

  • 황해진;이홍림
    • 한국세라믹학회지
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    • 제28권4호
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    • pp.269-278
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    • 1991
  • Fine AlN powder was synthesized by carbothermal reduction and nitridation of alumimun hydroxide prepared from Al-isopropoxide. AlN ceramics with Y2O3 and CaO were prepared by hot-pressing under the pressure of 30 MPa at 180$0^{\circ}C$ for 1 h in N2 atmosphere. Grain boundary behavior and purification mechanism of AlN lattice were examined by heat treatment of AlN ceramics at 185$0^{\circ}C$ for 1-6 h in N2 atmosphere. AlN ceramics without sintering additives showed poor sinterability. However, Y2O3-doped and CaO-doped AlN ceramics were fully densified nearly to theoretical density. As the heat treatment time increased, c-axis lattice parameter increased. This is attributed to the removal of Al2O3 in AlN lattice. This purification effect of AlN attice depended upon the quantity of secondary oxide phase in the inintial stage of heat treatment and the heat treatment time.

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냉간가공과 열처리한 Ni 테이프에서의 집합조직 발달 (Texture development in cold-roiled and heat-treated Ni tapes)

  • 이동욱;지봉기;임준형;주진호;정충환;박순동;전병혁;홍계원;김찬중
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 2002년도 하계학술대회 논문집
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    • pp.535-538
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    • 2002
  • Cube-textured Ni substrates for YBCO coated conductors were fabricated by cold-rolling and annealing of Ni powder compacts. To establish the optimum sintering temperature, tensile test was performed for the Ni rod sintered at various temperatures. The Ni rods prepared at above 100$0^{\circ}C$ showed good mechanical properties due to the complete densification of the Ni rods. The Ni rods were rolled to final thickness of 100 ${\mu}{\textrm}{m}$ and then annealed at 100$0^{\circ}C$ for various annealing time for texture development. The texture analysis made by 2 $\theta$ scan and pole-figure showed that the cube texture was developed in a short time of a few munitues. The FWHM of in-plane and out of plane texture of the prepared Ni tapes was 8-10$^{\circ}$. The AEM surface roughness of the Ni tapes was as smooth as 3 nm.

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0.15BaO-$0.15Sm_2O_3-0.7TiO_2$ 세라믹스의 마이크로파 유전 특성 (Microwave Dielectric Properties of 0.15BaO-$0.15Sm_2O_3-0.7TiO_2$ Ceramics)

  • 이근일;박인길;이영희;윤석진
    • 대한전기학회:학술대회논문집
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    • 대한전기학회 1993년도 정기총회 및 추계학술대회 논문집 학회본부
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    • pp.185-187
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    • 1993
  • 0.15BaO-$0.15Sm_2O_3-0.7TiO_2$, ceramics were fabricated by mixed-oxide method. Microwave dielectric properties were investigated with sintering temperature and annealing time. In the specimen sintered at 1350[$^{\circ}C$], dielectric constant, quality factor and temperature coefficient of resonant frequency had a good values of 80.19, 2006 (at 4.6851[GHz]), -27.54[ppm/$^{\circ}C$], respectively. Increasing the annealing time, dielectric constant was almost constant and quality factor was increased. Temperature coefficient of resonant frequency was minimum value (-1.28[ppm/$^{\circ}C$]) at 4 [hr] annealed.

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기계적 합금화법에 의해 제조된 Cu-l0wt%W 소결재의 미세조직 및 물성 (Microstructure and Physical Properties of Cu-l0wt%W Sintered Material Fabricated by Mechanical Alloying Method)

  • 김보수
    • 한국분말재료학회지
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    • 제1권2호
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    • pp.167-173
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    • 1994
  • Cu-10wt%W composite powders have been manufactured by a high energy ball milling technique. The composite powders were pressed at 250 MPa and sintered in a dry hydrogen at 103$0^{\circ}C$ for 4 hours. After sintering, Cu-10wt%W composite materials were forged. And the arc-resistance of forged materials which have the same relative density of 94% has been tested. Composite particles, i.e. tungsten particles distributed homogeneously in the copper matrix, was formed after 480 min mechanical alloying. Densities of these sintered materials were ranged from 74 to 84%. Densification degree was due to the formation of composite powders. As the mechanical alloying time increased, the hardness was increased and tungsten particle size was decreased. Arc loss of the forged specimens was decreased as increasing the mechanical alloying time.

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CaTiO$_3$:Pr 형광체의 전기 전도성이 음극선 발광에 미치는 영향 (Effect of conductivity on Cathodoluminescence of CaTiO$_3$:Pr Phosphors)

  • 박용규;한정인;곽민기;이인규;김대현
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 1998년도 춘계학술대회 논문집
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    • pp.105-108
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    • 1998
  • In the present study, the luminescence characteristics and the effect of conductivity on cathodoluminescene of CaTiO$_3$:Pr was studied using dick specimens sintered at various temperatures and atmosphere. As a sintering temperature was increased from 1100 to 1400 $^{\circ}C$, conductivity of CaTiO$_3$:Pr phosphor was improved and CL brightness was also increased about four times and decay times was reduced from 0.29 to 0.21 msec. And all samples prepared in Ar showed high conductivity, CL brightness and short decay time in comparison with those sintered in air.

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화염법을 이용한 Pt/C 촉매 제조 (Pt Coating on Flame-Generated Carbon Particles)

  • 최인대;이동근
    • 대한기계학회논문집B
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    • 제33권2호
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    • pp.116-123
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    • 2009
  • Carbon black, activated carbon and carbon nanotube have been used as supporting materials for precious metal catalysts used in fuel cell electrodes. One-step flame synthesis method is used to coat 2-5nm Pt dots on flame-generated carbon particles. By adjusting flame temperature, gas flow rates and resident time of particles in flame, we can obtain Pt/C nano catalyst-support composite particles. Additional injection of hydrogen gas facilitates pyrolysis of Pt precursor in flame. The size of as-incepted Pt dots increases along the flame due to longer resident time and sintering in high temperature flame. Surface coverage and dispersion of the Pt dots is varied at different sampling heights and confirmed by Transmission electron microscopy (TEM), Energy-dispersive spectra (EDS) and X-ray diffraction (XRD). Crystalinity and surface bonding groups of carbon are investigated through X-ray photoelectron spectroscopy (XPS) and Raman spectroscopy.

BaO-Sm2O3-TiO2 세라믹스의 마이크로파 유전특성에 미치는 어닐링 효과 (Annealing Effect on the Microwave Dielectric Properties of the BaO-SmS12TOS13T-TiOS12T Ceramics)

  • Lee, Geun-Ill;Chung, Jang-Ho;Lee, Young-Hie
    • 대한전기학회논문지
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    • 제43권5호
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    • pp.789-794
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    • 1994
  • In this study, the structural and microwave dilelectric properties of 0.15BaO-0.15SmS12TOSI3T-0.7TiOS12T ceramics with sintering and annealing conditions were investigated. In the specimen sintered at 1350 [$^{\circ}C$], dielectric constant and quality factor were good values of 80.19,2006 (fS10T=4.6851[GHz]). To improve the $\tau$S1fT of specimen which was manufactured by the optimumsintering condition (1350[$^{\circ}C$],2[Hr.]), annealed from 2[hr.] to 16[hr.] at the annealing temperature of 1200 [$^{\circ}C$]. Increasing the annealing time, dielectric constant was almost constant and quality factor was increased. In the specimen of 4[hr.] annealed, the temperature coefficient of resonant frequency was minimum value, and increased with increasing the annealing time.

Bi-(Pb)-Sr-Ca-Cu-O계 초전도체의 Sb 첨가 효과 (Effect of Sb doppd in Bi-Pb-Sr-Ca-O Superconductor)

  • 한태희;김민기;최성환;최효상;황종선
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 1992년도 춘계학술대회 논문집
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    • pp.64-69
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    • 1992
  • Bi-Sr-Ca-Cu-O superconducting system have the low and high Tc phases. In order to get the superconductor above crtitical temperature 100K, we added with Pb and sintered for a long time about 200 hrs. In this study, the influence of superconducting characteristics on the Bi(Pb)SrCaCuO system characteristics on the Bi(Pb)SrCaCuO system dopped Sb was investigate too. Adding Sb of 0.1 mol, the sintering time is short than that dopped Pb only. We could get the critical temperature 102 K at sintered for 24 hrs and 109 K for 210 hrs.

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SLS에서의 자동적인 조형자세 및 배치 결정에 관한 연구 (Determination of Part Orientation and Packing in SLS Process)

  • 허성민;장복근;최경현;이석희
    • 한국정밀공학회지
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    • 제16권11호
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    • pp.139-147
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    • 1999
  • Rapid Prototyping has made a drastic change in all industries which needs to reduce the time for the development of new products. Orientation and packing in rapid prototyping is considered as the most important factors to maximize the utilization of space in the build chamber and reduce build time. However, the decision of these parameter is mainly dependant on the operators's experience. This paper presents the methodology to find the optimal build layout considering an orientation and packing of multiple parts in SLS processing. Each part is represented as a voxel structure to deal with the inefficiency in a bounding box approach. Test results show that the adapted BL algorithm with a genetic algorithm(GA) can be applicable to a real industry.

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