• 한국세라믹학회지
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• 제34권6호
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• pp.659-667
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• 1997

The effect of calcination temperature of Mg(OH)2 on the green density and densification of MgO was investigated. It was observed that the impure magnesium hydroxide powder showed a higher crystallization rate while it had a lower tendency of agglomeration between periclae crystallites, as compared to that of the pure magnesium hydroxide powder. In the case of calcination of the powders under 85$0^{\circ}C$, the impure powder showed the higher green and sintered density. In spite of higher green density upon the calcination over 100$0^{\circ}C$, the impure powder showed the lower sintered density, caused by exaggerated growth of the periclase crystallites. The highest sintered densities in the both powders were obtained at the calcination temperature of 100$0^{\circ}C$. And the green density was inversely proportional to the sintered density at the calcination over 100$0^{\circ}C$.

• 한국분말야금학회:학술대회논문집
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• 한국분말야금학회 2006년도 Extended Abstracts of 2006 POWDER METALLURGY World Congress Part 1
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• pp.580-581
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• 2006

The present paper investigates the possibilities of niobium using for the mechanical properties of the common low alloyed Cu-Ni-Mo-C sintered structural steels enhancing. On both thermodynamic and experimental bases there were demonstrated the Nb nitrides/carbides/carbonitrides preferential formation in these steels during sintering in dissociated ammonia at both common and elevated temperatures. The obtained results for $0.2\;{\div}\;1.0\;%$ fine Nb powder and 0.3% graphite additions to Distaloy AB iron base powder cold compacted and sintered in dissociated ammonia proved the expected strengthening effect, leading to higher mechanical properties of the processed steels than of the common Cu-Ni-Mo-C ones.

• 한국분말재료학회지
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• 제10권4호
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• pp.249-254
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• 2003

WC-6wt%Co hard metal powders were sintered by a 2.45 GHz multimode microwave applicator in Ar atmosphere. Microwave sintering of WC-6wt%Co powder lowered the sintering temperature and shortened the processing time in less than two hours than by a conventional method. Microstructures of the sintered specimen were studied with scanning electron microscope (SEM) and no abnormal grain growth was observed. Mechanical properties were similar to the values of the specimens sintered by a conventional method. Specimen sintered at 135$0^{\circ}C$ for 30 minutes ,hewed 99%, 20.5 GPa and 8.1 MPa$\sqrt{m}$ of theoretical density, hardness and fracture strength, respectively.

• 한국분말야금학회:학술대회논문집
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• 한국분말야금학회 2006년도 Extended Abstracts of 2006 POWDER METALLURGY World Congress Part 1
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• pp.611-612
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• 2006

In a manufacturing technique of the sintered filter, pressureless sintering method has good permeability, it is not need the binder and lubricant used on compacting process, so it has little contamination and it is easy to control the pore size and shape but the mechanical strength is low relatively and it is difficult that parts of complicate form are manufactured. In the case of manufacturing the filter by press and sintering method, in order to be satisfactory characteristic of un-pressed filter, in this study sintered metal filter fabricated by using 30-40mesh stainless steel 316L powder and additive agents. Porosity and structure of pores, permeability and mechanical strength of the sintered filter were investigated with the variation sintering conditions. Porosity was nearly constant about $60{\sim}70%$, density, permeability and mechanical strength were changed markedly with quantity of additive materials and sintering conditions.

• 한국분말야금학회:학술대회논문집
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• 한국분말야금학회 2006년도 Extended Abstracts of 2006 POWDER METALLURGY World Congress Part 1
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• pp.270-271
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• 2006

Nd-Fe-B type powder was sintered using spark plasma sintering method. Fabricated compact sintered at the temperature of $700\;^{\circ}C$, is found to be a composite magnet with Nd-Fe-Co-B and ${\alpha}-Fe$. The compact sintered at $700\;^{\circ}C$ shows slightly low coercivity and large remanent magnetization comparing to the compact sintered at $600^{\circ}C$ due to the formation of ${\alpha}-Fe$ phase, resulting in the large maximum energy product. Maximum energy product tends to decrease with decreasing thickness of sintered compacts below 0.5 mm in thickness.

• 한국분말야금학회:학술대회논문집
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• 한국분말야금학회 2006년도 Extended Abstracts of 2006 POWDER METALLURGY World Congress Part2
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• pp.1087-1088
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• 2006

The microstructure and electrical conductivity of CNTs dispersed $Al_2O_3$ nanocomposites depending on the powder processing and CNTs content were demonstrated. The composite powders with homogeneous dispersion of CNTs could be synthesized by a catalytic route for direct formation of CNTs on nano-sized Fe dispersed $Al_2O_3$ powders. The sintered nanocomposite using the composite powder with directly synthesized CNTs showed homogeneous microstructure and enhanced elelctrical conductivity. The influence of powder processing on the properties of sintered nanocomposites was discussed by the observed microstructural features.

• 한국세라믹학회지
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• 제31권11호
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• pp.1265-1270
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• 1994

Ultra-fine hydroxyapatite powder were synthesized by the hydrothermal reaction at 10 atm, 3 hrs of Ca(OH)2 suspension with (NH4)2HPO4 solution, and were characterized sintering behavior. Sintered bodies of hydroxyapatite powders which synthesized by hydrothermal reaction method has less weight loss, less sintering shrinkage and superior mechanical property, and was more dense than sintered bodies of hydroxyapatite powder which synthesized by wet method. Sintered bodies were hydroxyapatite single phase. When soack in Ringer's solution for 2 weeks, hydroxyapatite powders preserved hydroxyapatite and sintered body absorbed trace of Ca2+ ion with soaked time.

• 한국분말야금학회:학술대회논문집
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• 한국분말야금학회 2006년도 Extended Abstracts of 2006 POWDER METALLURGY World Congress Part2
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• pp.1153-1154
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• 2006

Effects of sintering conditions such as sintering temperature and heating rate on oxygen content, density, microstructure and toughness of sintered Mo were investigated. The oxygen content of the sintered Mo significantly depended on the sintering conditions. The oxygen content of the primary sintered(below 1673 K) Mo influenced the densifications. The number of pores at grain boundaries of the secondary sintered(at 2073 K)Mo depended on the oxygen content of the primary sintered Mo. Grain growth of the secondary sintered Mo was inhibited by the existence of pores at the grain boundaries. The secondary sintered Mo having larger number of pore and smaller grain size demonstrated higher strength.

• 한국분말재료학회지
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• 제11권5호
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• pp.383-390
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• 2004

In order to investigate behavior of abnormal expansion of the iron-copper compacts, we compared the dilatometric curves of the compacts which mixed the copper powder to the iron powder with those of compacts which mixed the copper powder to the iron-copper alloy powder. The dilatometric curves were obtained below the sintering conditions, which heated up to 115$0^{\circ}C$ by a heating rate of 1$0^{\circ}C$/min, held for 60min at 115$0^{\circ}C$ and cooled down at a rate of 2$0^{\circ}C$/min to room temperature. The dilatometric curves of the compacts showed the different expansion behavior at temperatures above the copper melting point in spite of same chemical composition. All of the compacts of former case showed large expansion, but all of the compacts in latter case showed large contraction. The microstructures of sintered compacts also showed the different progress in alloying of the copper into the iron powder. Namely we could observe the segregation at alloy part of copper into iron powder in case of the sintered compacts, which mixed the copper powder to the iron powder, but could not observe the segregation in compacts which mixed the copper powder to the iron-copper alloy powder. But the penetration of liquid copper into the interstices between solid particles was occurred at both cases. Therefore, the showing of the different dimensional changes in the compacts in spite of same chemical composition is due to more the alloying of copper into iron powder than the penetration of liquid copper into the interstices between solid particles.

• 한국분말재료학회지
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• 제31권1호
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• pp.43-49
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• 2024

In this study, a core-shell powder and sintered specimens using a mechanically alloyed (MAed) Ti-Mo powder fabricated through high-energy ball-milling are prepared. Analysis of sintering, microstructure, and mechanical properties confirms the applicability of the powder as a sputtering target material. To optimize the MAed Ti-Mo powder milling process, phase and elemental analyses of the powders are performed according to milling time. The results reveal that 20 h of milling time is the most suitable for the manufacturing process. Subsequently, the MAed Ti-Mo powder and MoO₃ powder are milled using a 3-D mixer and heat-treated for hydrogen reduction to manufacture the core-shell powder. The reduced core-shell powder is transformed to sintered specimens through molding and sintering at 1300 and 1400℃. The sintering properties are analyzed through X-ray diffraction and scanning electron microscopy for phase and porosity analyses. Moreover, the microstructure of the powder is investigated through optical microscopy and electron probe microstructure analysis. The Ti-Mo core-shell sintered specimen is found to possess high density, uniform microstructure, and excellent hardness properties. These results indicate that the Ti-Mo core-shell sintered specimen has excellent sintering properties and is suitable as a sputtering target material.