• 제어로봇시스템학회논문지
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• 제8권1호
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• pp.21-27
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• 2002

Inspection and shape measurement of three-dimensional objects are widely needed in industries for quality monitoring and control. A number of visual or optical technologies have been successfully applied to measure three-dimensional surfaces. However, those conventional visual or optical methods have inherent shortcomings such as occlusion and variant surface reflection. X-ray vision system can be a good solution to these conventional problems, since we can extract the volume information including both the surface geometry and the inner structure of any objects. In the x-ray system, the surface condition of an object, whether it is lambertian or specular, does not affect the inherent characteristics of its x-ray images. In this paper, we propose a three-dimensional x-ray imaging method to reconstruct a three dimensional structure of an object out of two dimensional x-ray image sets. To achieve this by the proposed method, two or more x-ray images projected from different views are needed. Once these images are acquired, the simultaneous algebraic reconstruction technique(SART) is usually utilized. Since the existing SART algorithms have several shortcomings such as low performance in convergence and different convergence within the reconstruction volume of interest, an advanced SART algorithm named as USART(uniform SART) is proposed to avoid such shortcomings and improve the reconstruction performance. Because, each voxel within the volume is equally weighted to update instantaneous value of its internal density, it can achieve uniform convergence property of the reconstructed volume. The algorithm is simulated on various shapes of objects such as a pyramid, a hemisphere and a BGA model. Based on simulation results the performance of the proposed method is compared with that of the conventional SART method.

• Mass Spectrometry Letters
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• 제10권1호
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• pp.18-26
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• 2019

We developed a bioanalytical method for simultaneous determination of nine NBOMe derivatives (25H-NBOMe, 25B-NBOMe, 25E-NBOMe, 25N-NBOMe, 25C-NBOH, 25I-NBOH, 25B-NBF, 25C-NBF, and 25I-NBF) in human plasma using liquid chromatography tandem mass spectrometry (LC-MS/MS). Human plasma samples were pre-treated using solid-phase extraction. Separation was achieved on a C18 column under gradient elution using a mobile phase containing 0.1% formic acid in acetonitrile and 0.1% formic acid in water at a flow rate of 0.3 mL/min. Mass detection was performed in the positive ion mode using multiple reaction monitoring. The calibration range was 1-100 ng/mL for all quantitative analytes, with a correlation coefficient greater than 0.99. The intra- and inter-day precision and accuracy varied from 0.85 to 6.92% and from 90.19 to 108.69%, respectively. The recovery ranged from 86.36 to 118.52%, and the matrix effects ranged from 27.09 to 99.72%. The stability was acceptable in various conditions. The LC-MS/MS method was validated for linearity, accuracy, precision, matrix effects, recovery and stability in accordance with the FDA guidance. The proposed method is suitable for reliable and robust routine screening and analysis of nine NBOMe derivatives in forensic field.

• 한국환경농학회지
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• 제39권4호
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• pp.368-374
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• 2020

BACKGROUND: The residual analysis of polar pesticides has remained a challenge. It is even more difficult to simultaneously analyze multiple polar pesticides. Diquat, paraquat, and chlormequat are typical examples of highly polar pesticides. The existing methods for the analysis of diquat, paraquat and chlormequat are complex and time consuming. Therefore, a simple, quick and effective method was developed in the represent study for simultaneous analysis of diquat, paraquat and chlormequat in animal products, meat and fat using UPLC-MS/MS. METHODS AND RESULTS: Sample extraction was carried out using acidified acetonitrile and water and re- extracted with acidified acetonitrile and combine the extracts followed by centrifugation. The extract was then cleaned up with a HLB cartridge after reconstitution with acidic acetonitrile and water. The method was validated in quintuplicate at three different concentrations. The limits of detection (LOD) and quantification (LOQ) were 0.0015 and 0.005 mg/L, respectively. Matrix suppression effect was observed for all of the analytes. A seven point matrix matched calibration curve was constructed for each of the compound resulted excellent linearity with determination coefficients (R2) ≥ 0.991. Accuracy and precision of the method was calculated from the recovery and repeatability and ranged from 62.4 to 119.7% with relative standard deviation less than 18.8%. CONCLUSION: The recovery and repeatability of the developed method were in the acceptable range according to the Codex Alimentarius guideline. The developed method can be applied for the routine monitoring of diquat, paraquat, and chlormequat in animal products, meat and fat.

• 한국수산과학회지
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• 제57권4호
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• pp.327-335
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• 2024

A simultaneous analytical method was developed to quantify antifouling agents and triazine herbicides in seawater using liquid chromatography-tandem mass spectrometry (LC-MS/MS). The target compounds included diuron, irgarol 1051, and prometryn, which are prevalent in marine environments owing to their extensive use in antifouling coatings and agriculture. The analytical procedure involves solid-phase extraction (SPE) using HLB cartridges followed by LC-MS/MS analysis for precise quantification. The method exhibits high recovery rates for diuron (101% ± 1.25), irgarol 1051 (94.7% ± 2.08), and prometryn (93.7% ± 3.06). Seawater samples from 30 coastal sites in Korea were analyzed. Irgarol 1051 was not detected, whereas diuron was consistently detected across all sites, with concentrations from 0.68 to 11.3 ng/L, and prometryn was present at levels between 0.12 and 7.06 ng/L. The highest diuron and prometryn concentrations were recorded along the southeastern and western coasts, respectively. These findings underscore the critical need for continuous monitoring and regulations to manage these contaminants in marine ecosystems, thereby safeguarding ecological integrity and public health. This study establishes a robust analytical framework for the comprehensive assessment of multiple marine contaminants.

• 한국식품과학회지
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• 제45권3호
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• pp.382-384
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• 2013

본 연구에서는 2012년 1월부터 8월까지 농산물 중 엽채류에 대하여 GC-ECD 및 GC-MSD를 이용하여 uniconazole의 잔류실태조사를 실시하였다. 겨자채에 표준용액을 0.05, 0.5 mg/kg 농도로 하여 회수율을 측정한 결과 98.9%에서 109.4%까지 양호한 결과를 나타내었다. 2012년 1월부터 8월까지 서울지역에 유통되고 있는 농산물 중 엽채류 3,632건에 대하여 모니터링을 실시한 결과 14건에서 uniconazole이 검출되었다. Uniconazole의 검출양은 0.098 mg/kg에서 2.2 mg/kg로 나타났다. 본 연구를 통하여 동시분석법으로 보다 효율적인 검사가 가능할 것으로 기대된다.

• 한국전산구조공학회논문집
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• 제36권6호
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• pp.407-414
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• 2023

본 논문에서는 다양한 분야에 적용할 수 있는 자동화 동시 인상 시스템을 3D 콘크리트 프린팅에 적용하여 동시 인상이 가능한 3D 콘크리트 프린팅 시스템으로 개발하였다. 개발된 시스템은 3D 콘크리트 프린팅 작업 중 측정되는 인상량을 피어슨 상관계수를 통해 분석하고, 유압시스템을 사분위수 기법으로 실시간 모니터링하여 안전하고 정밀한 인상이 가능하다. 이를 활용하면 3D 콘크리트 프린팅 구조물의 출력 품질을 확보함과 동시에 3D 콘크리트 프린팅의 규모보다 큰 구조물을 출력할 수 있다. 시스템의 성능을 평가하기 위해 기존의 3D 콘크리트 프린팅과 동시 인상이 가능한 3D 콘크리트 프린팅을 각각 이용하여 시편을 출력하였다. 출력된 시편은 3D 스캐너를 활용하여 측정하였다. 스캔한 시편의 층별 직경과 시편의 교차각을 측정하였으며, 분석을 통해 동시 인상이 가능한 3D 콘크리트 프린팅의 성능을 검증하였다.

• 대한원격탐사학회지
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• 제27권4호
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• pp.403-410
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• 2011

연안 환경에 대한 효과적인 관측을 위해서는 높은 주기 및 공간 해상도의 지속적인 관측이 필요하다. 지상에 설치한 기기로부터 이루어지는 원격 관측은 소수의 현장 기기 개수로는 관측할 수 없는 넓은 범위의 해역을 통시에 관측할 수 있고 또한 높은 빈도의 지속적인 관측이 가능하다. 본 연구에서는 연안 환경에 대한 대표적인 지상 원격 관측 기기인 마린 레이다와 카메라 시스템의 활용에 대하여 고찰해본다. 마린 레이다는 시간적으로 연속된 레이다 영상으로부터 파수 스펙트럼을 계산하고 이를 통합 적분하고 조정 전달함수를 적용하여 시간에 따른 주파수 스펙트럼을 산출할 수 있다. 또한 시간에 따른 파랑 레이다 영상을 평균함으로서 쇄파대와 이안류 그리고 연안사주의 위치 등에 대한 분석도 기능하다. 카메라 시스템은 해안선의 변화뿐만 아니라 오염 등으로 인하여 해안에서 발생하는 거품 발생량의 변화에 대한 분석을 할 수 있다. 빗각 촬영된 거품 영상을 기하 보정 후 거품부분을 따로 추출함으로서 거품량에 대한 정량적인 분석이 가능하다. 위의 두 기기는 각기 그 특성이 다른 센서로서 이를 동시에 활용하면 연안환경 관측에 있어 시너지 효과를 얻을 수 있다.

• 천문학회보
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• 제46권1호
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• pp.52.1-52.1
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• 2021

We present the results of multi-epoch, multi-frequency monitoring of a blazar 4C +29.45, which was regularly monitored as part of the Interferometric Monitoring of GAmma-ray Bright AGNs program - a key science program of the Korean Very long baseline interferometry Network (KVN). Observations were conducted simultaneously at 22, 43, 86 and 129 GHz during the 4 years from December 2012 to December 2016. We also used additional data from the 15 GHz Owens Valley Radio Observatory (OVRO) monitoring program. From the 15 GHz light curve, we estimated the variability time scales of the source during several radio flux enhancements. We found that the source experiencesd 6 radio flux enhancements with variability time scales of 9-187 days during the observing period, yielding corresponding variability Doppler factors of 9-27. From the multi-frequency simultaneous KVN observations, we were able to obtain accurate radio spectra of the source and hence to more precisely measure the turnover frequencies 𝜈_r of synchrotron self-absorbed (SSA) emission with a mean value of ${\bar{\nu}_r}=28.9GHz$. Using jet geometry assumptions, we estimated the size of the emitting region at the turnover frequency. Taking into account these results, we found that the equipartition magnetic field strength is up to two orders of magnitudes higher than the SSA magnetic field strength (0.6-99 mG). This is consistent with the source being particle dominated.

• 한국식품영양과학회지
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• 제38권12호
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• pp.1779-1784
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• 2009

우리 국민의 주식이 되는 쌀(백미)과 콩류, 감귤류, 열대과 일류, 엽채류, 엽경채류, 근채류, 과채류, 버섯류에 속하는 농산물(989건)에 대해 8종의 EBI계 농약의 잔류 여부를 분석하였다. 그 결과 8건의 검체에서 농약이 검출되었고 농약 수는 5종이 검출되었다. 기준 미설정 농약은 2종이었으며, 곡류 134건 중 4건 검출로 3.0%, 채소류 471건 중 4건 검출로 0.8%의 검출율을 나타내었다. 그 외 콩류(48건), 견과종실류(72건), 과실류(197건), 버섯류(67건)에서는 전혀 검출되지 않았으며 부적합율은 0.1%로 나타났다. 국내 미등록농약인 paclobutrazole이 근대에서 잠정허용기준을 초과하는 것으로 확인되었다. 그리고 EBI계의 검출율은 0.8%로 매우 낮았으며 검출된 농약의 경우도 기준규격 이하로 안전한 수준이었다.

• Journal of Ginseng Research
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• 제43권4호
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• pp.508-516
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• 2019

Background: Ginsenosides are not only the principal bioactive components but also the important indexes to the quality assessment of Panax ginseng Meyer. Their contents in cultivated ginseng vary with the growth environment and age. The present study aimed at evaluating the significant difference between 36 cultivated ginseng of different cultivation areas and ages based on the simultaneously determined contents of 14 ginsenosides. Methods: A high-performance liquid chromatography (HPLC) coupled with triple quadrupole mass spectrometer (MS) method was developed and used in the multiple reaction-monitoring (MRM) mode (HPLC-MRM/MS) for the quantitative analysis of ginsenosides. Multivariate statistical analysis, such as principal component analysis and partial least squares-discriminant analysis, was applied to discriminate ginseng samples of various cultivation areas and ages and to discover the differentially accumulated ginsenoside markers. Results: The developed HPLC-MRM/MS method was validated to be precise, accurate, stable, sensitive, and repeatable for the simultaneous determination of 14 ginsenosides. It was found that the 3- and 5-yr-old ginseng samples were differentiated distinctly by all means of multivariate statistical analysis, whereas the 4-yr-old samples exhibited similarity to either 3- or 5-yr-old samples in the contents of ginsenosides. Among the 14 detected ginsenosides, Rg1, Rb1, Rb2, Rc, 20(S)-Rf, 20(S)-Rh1, and Rb3 were identified as potential markers for the differentiation of cultivation ages. In addition, the 5-yr-old samples were able to be classified in cultivation area based on the contents of ginsenosides, whereas the 3- and 4-yr-old samples showed little differences in cultivation area. Conclusion: This study demonstrated that the HPLC-MRM/MS method combined with multivariate statistical analysis provides deep insight into the accumulation characteristics of ginsenosides and could be used to differentiate ginseng that are cultivated in different areas and ages.