• 대한치과재료학회지
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• 제43권4호
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• pp.343-349
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• 2016

This experiment was carried out to examine whether the post-firing heat treatment is effective in increasing the hardness of metal-ceramic alloy of the Pd-Au-Ag-Sn system. Precipitation hardening by holding at $600^{\circ}C$ after simulated complete porcelain firing in a metal-ceramic alloy of the Pd-Au-Ag-Sn system was examined by observing the change in hardness, crystal structure, and microstructure using a hardness test, X-ray diffraction (XRD), and field emission scanning electron microscopy (FE-SEM). The hardness of the alloy increased apparently by holding the specimen at $600^{\circ}C$ for 30 min after simulated complete porcelain firing. The formation of fine grain interior precipitates during holding at $600^{\circ}C$ caused the formation of lattice strain in the grain interior, resulting in apparent hardening. The faster cooling rate (stage 0) during simulated complete porcelain firing resulted in more effective precipitation hardening during holding at $600^{\circ}C$. From the above results, an appropriate post-firing heat treatment, such as holding at $600^{\circ}C$ for 30 min after complete porcelain firing may increase the durability of metal-ceramic prostheses composed of Pd-Au-Ag-Sn alloy.

• 한국군사과학기술학회지
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• 제24권1호
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• pp.79-83
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• 2021

The expiration date of high energetic materials(HEM), such as HMX, RDX, TNT, is important. If the expiration date is violated, the expected specification of HEM would not be satisfied which may cause a different conclusion in an urgent situation. As a result, this HEM should maintain fresh conditions which cause the accumulation of waste HEM. If HEM is landfilled during demilitarization, the impact on living organizations is serious. Additionally, landfilling HEM has a possibility of explosion. In this research, the process flow diagram of the demilitarization gas treatment process was simulated while satisfying the law of the environment in Korea. After validation of simulation, it was optimized thermodynamically using Heat Exchanger Network Synthesis(HENs). This study is expected to enhance the energy efficiency of the original facility by suggesting developed designs. This research was supported by Agency of Defense Development NE32 Korea. Thanks to Agency of Defense Development, Korea

• 대한기계학회논문집B
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• 제37권5호
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• pp.467-472
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• 2013

정수장 내 축열조 설치 원수열원 히트펌프시스템의 동적 특성을 TRNSYS 프로그램을 이용하여 모델링 하였다. 원수열원 히트펌프의 실증평가를 위해 성남정수장 내 축열조가 설치된 히트펌프 실험결과를 이용하여 검증하였고, 본 설비는 2010년 11월부터 운전되고 있다. 모델링 결과 원수열원 히트펌프의 평균 COP는 냉 난방 시 각각 4.97과 3.17을 나타냈다. 축열조 용량은 $5m^3$에서 $20m^3$로 변화시킬 때, 축열조 용량 $10m^3$ 에서 가장 높은 COP와 소비전력이 나타났다. 설치지역으로 서울, 인천, 강릉, 그리고 광주를 고려하였고, 지역에 따른 COP와 소비전력은 큰 변화가 없었으나 소비전력량에 있어서 난방 시에 위도가 높은 서울의 소비전력량이 가장 높으며, 냉방 시에 가장 낮게 나타났다. 본 시스템을 동일한 용량의 물-공기방식의 히트펌프와 비교할 때 평균 25%정도 낮은 소비전력량을 나타냈다.

• 대한기계학회논문집B
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• 제38권7호
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• pp.639-646
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• 2014

난류모델에서 벽면처리법이 터빈 노즐 베인의 열전달 예측에 미치는 영향을 비교 분석하였다. 본 연구를 위해 NASA의 C3X 터빈 노즐 베인을 사용하였다. 벽함수 방법, 저레이놀즈수 방법, 천이모델을 사용하여 베인 표면에서의 압력 및 온도를 해석하였다. 해석 결과 터빈 노즐 베인의 중간 압력분포는 각 벽면처리법에 따른 차이 없이 실험값과 잘 일치하였다. 그러나 터빈 노즐 베인의 온도와 열전달 계수는 각 벽면처리법에 따라 큰 차이를 보였다. 전반적으로 저레이놀즈수 방법과 천이모델은 벽함수 방법에 비해 온도 및 열전달 계수 예측에 특별한 이점을 보이지 않았으며, 벽함수 방법을 적용한 레이놀즈응력 난류모델이 터빈 노즐 베인 표면의 온도 및 열전달 계수를 비교적 잘 예측하였다.

• Nuclear Engineering and Technology
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• 제55권4호
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• pp.1300-1309
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• 2023

Simulated debris was synthesized using UO₂, Zr, and stainless steel and a heat treatment method under inert or oxidizing conditions. The primary U solid phase of the debris synthesized at 1473 K under inert conditions was UO₂, whereas a (U, Zr)O₂ solid solution formed at 1873 K. Under oxidizing conditions, a mixture of U₃O₈ and (Fe, Cr)UO₄ phases formed at 1473 K, whereas a (U, Zr)O_2+x solid solution formed at 1873 K. The leaching behavior of the fission products from the simulated debris was evaluated using two methods: the irradiation method, for which fission products were produced via neutron irradiation, and the doping method, for which trace amounts of non-radioactive elements were doped into the debris. The dissolution behavior of U depended on the properties of the debris and aqueous solution for immersion. Cs, Sr, and Ba leached out regardless of the primary solid phases. The leaching of high-valence Eu and Ru ions was suppressed, possibly owing to their solid-solution reaction with or incorporation into the uranium compounds of the simulated debris.

• Journal of Welding and Joining
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• 제22권1호
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• pp.43-49
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• 2004

Contact tip is located so near to welding arc that it is heated to high temperature during long time welding. In such a situation, tip changes in its microstructure and in turn its mechanical properties. This study was intended to investigate those changes by using simulated heat treatment. As a result of this study, it was confirmed that tip of Cu-P alloy hardened with severe cold deformation lose its initial hardness to a large extent within 60 min due to the occurrence of rapid recrystallization while that of Cu-Cr composition hardened by proper aging treatment can preserve its intial hardness for about 1,000 min or longer. Based on these results, suggested was a guideline that can classify contact tips into two different grades: deformation-hardened type and precipitation-hardened type. Following a guideline, a tip with Cu-Cr composition can be classified into the deformation-hardened type if it is in the over-aged condition. Such a guideline is well described.

• 대한전자공학회논문지SD
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• 제41권12호
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• pp.1-6
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• 2004

본 연구는 PCB 기판용 FRP 재료의 열화현상을 규명하기 위하여 열 및 방전에 의한 열화를 각각 모의하여 표면에서의 화학적, 정전적 상관관계를 조사하였다. 열 처리에 따른 시료의 특성변화는 $200^{\circ}C$ 까지는 표면의 소수화로 인하여 접촉각 및 표면전위가 증가하였다. XPS에 의한 분석결과 열처리에 따라 표면측쇄상 산소기의 이탈과 탄소쇄의 불포화 이중결합의 증가로 처리시료에서는 소수성이 증가하였다. 또한 열처리로 인해 착색현상이 발생되었고, 이러한 현상은 ether기에 의해 발생된다는 것을 확인하였다. 방전 처리된 시료의 접촉각 및 표면전위는 표면에 카르복실기 라디칼을 포함하는 다량의 측쇄화가 집중적으로 발생되어 처리시간에 따라 급격한 친수화가 진행되었다.

• 한국산학기술학회논문지
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• 제19권4호
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• pp.69-76
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• 2018

본 연구에서는 유정용 강관의 열처리 조건 및 합금원소(B, Ti)에 따른 미세조직 및 기계적 성질을 조사하였다. 실험에는 J55, J55+B,Ti 강재를 사용하였고, 열처리 조건은 각각 오스테나이트 처리온도 ($880^{\circ}C$, $910^{\circ}C$, $940^{\circ}C$), 냉각방식 (수냉, 유냉), 템퍼링 온도 (미실시, $550^{\circ}C$, $650^{\circ}C$) 이다. 열처리 조건에 따라 얻어지는 미세조직을 예측하기 위해 J55, J55+B,Ti 강재의 화학적 성분을 기준으로 평형상태도와 CCT 곡선을 예측하였다. 시뮬레이션 결과 평형상태도는 A1, A3 온도가 약 $20^{\circ}C$ 감소하였고, CCT 곡선은 B, Ti이 첨가됨에 따라 ferrite와 bainite nose 부분이 오른쪽으로 이동하였다. J55, J55+B,Ti 강재의 CCT 곡선을 기준으로 냉각속도에 따른 martensite, bainite, ferrite등 예상되는 미세조직을 예측하였고, J55 강재의 미세조직 예측값은 실제 실험값과 유사한 양상을 나타내었지만. J55+B,Ti 강재의 예측값은 실제 실험값과는 차이가 있었다. 열처리 조건이 변화됨에 따라 martensite, bainite, ferrite 등 다양한 조직이 생성되었으며, 이는 경도, 강도 및 연신율에 밀접한 영향을 미쳤다. J55시편의 수냉의 경우 martensite 조직이 형성되었고, 유냉의 경우 bainite와 ferrite 조직이 형성되었지만, J55+B,Ti시편은 B의 첨가에 의한 경화능 향상으로 냉각방식에 관계없이 martensite 조직이 형성되었다. 전반적으로 B, Ti을 첨가하면서 기계적 성질은 향상되었고, quenching 이후의 시편보다 tempering 이후의 시편에서 크게 향상되었다. 이는 Ti의 첨가로 인해 생성된 미세한 석출물이 재결정시 결정립 성장을 억제하여 미세한 오스테나이트 결정립을 생성하였고, tempering 열처리 이후에도 결정립 미세화 효과가 큰 영향을 미친 것으로 판단된다.

• 한국해양공학회지
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• 제22권6호
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• pp.27-34
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• 2008

The temperature distribution in the weldment is not uniform because a weldment is locally heated. Thermal plastic deformation results from the local expansion and shrinkage by the heating and cooling of metal. Therefore, residual stresses and distortion occur in the weldment. In this study, we had conducted on the weld thermal cycle simulation that is supposed as the HAZ on SS400 steel and STS304 steel. The residual stresses that were obtained from the drawing and the weld thermal cycle simulation were estimated by X-ray diffraction. We also carried out ultrasonic test for the weld thermal cycle simulated specimens, and then conducted on nondestructive evaluation by the ultrasonic parameters obtained ultrasonic test. From the results, residual stresses of weld thermal cycle simulated specimens after the residual stress removal heat treatment are lower than that of the drawing.

• Biomolecules & Therapeutics
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• 제9권1호
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• pp.7-14
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• 2001

The chicken meat has been reported as one of the food causing allergic reactions predominantly to Korean. At present, several in vitro tests for immunoglobulinG (IgG)-mediated as well as IgE-mediated food allergy are available. 13 clinically chicken meat-allergic patients were investigated together with 4control subjects for identification of chicken meat-specific reactivity by ELISA. Also, protein profile and IgE, IgGtotal and IgG4-reacting allergens were detected by means of sodium dodecyl sulfate-polyacrylamide gel electro-phoresis (SDS-PAGE)and immunoblotting. Chicken meat extracts were prepared as raw, heated, heat and simulated gastric fluid (SGF) treated samples to characterize the stability of allergen to physicochemical treatment. SDS-PAGE revealed 9~200 kDa bands. And in immunoblotting 7 sera were identified most major bands between 10 and 78 kDa. In case of IgE, six proteins (17, 26, 35, 40, 78 kDa) were predominant in heat-treated extract, and the one (35 kDa) was present in SGF-treated preparations. In case of IgG$_{total}$ and IgG4, most of them showed a patters simmilar to IgE. There were significant differences (P<0.05) in IgE, IgG$_{total}$ , IgG4 Abs to chicken meat between the allergic and control subjects in ELISA. In addition, the concentration of IgG4Abs in the challenge-positive subjects was significantly higher than that of control subjects. It is considered that the specific IgE response to chicken meat was rarely prevalent to Koreans. However, the specific IgG4 response play an important role in the development of allergic symptoms.