• 대한화학회지
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• 제52권2호
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• pp.155-163
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• 2008

유기-실리카 이용한 잔유 구리(II)의 양을 빠른 추출을 위한 간단하고 재현성을 가지는 방법과 불꽃원자 흡수분광법으로의 검출에 대해 연구하였다. 공통으로 존재하는 이온은 분리와 검출에 간섭받지 않았다. 예비농축인자는 100 ml시료 용량에 대해 100 (1 ml 추출용량) 이 였다.제안된 방법의 검출한계는 1.0 ng ml-1이다. 최적조건하에서 흡착제의 최고흡수용량은 5 mg 구리/g 흡착제 였다. 최적조건하에서 상대표준편차는 2.8% (n=10)을 얻었다. 다양한 양의 구리(II)이온은 스파이크한 자연수와 합성수를 시험 시료로 하여 정확도 등을 시험하였다.

• Bulletin of the Korean Chemical Society
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• 제29권6호
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• pp.1173-1178
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• 2008

A simple and sensitive high-performance liquid chromatographic method was developed for the simultaneous identification of enrofloxacin and its active metabolite ciprofloxacin in chicken muscle. Norflorxacin imprinted polymers synthesized in water-containing systems show high selectivity to enrofloxacin and ciprofloxacin in an aqueous environment. Using these water-compatible imprinted polymers as selective adsorbents in the solid-phase extraction of enrofloxacin and ciprofloxacin from chicken samples, the remaining biological matrix could be quickly washed out from the imprinted column while enrofloxacin and ciprofloxacin were selectively retained and enriched. Analytical separation was performed on a $C_{18}$ column using acetonitrile-water as a mobile phase and fluorescence detection. Good linearity was obtained from 0.8 to 500 ng/g (r > 0.998) with relative standard deviation of less than 3.9%. The mean recoveries of enrofloxacin and ciprofloxacin from chicken muscle were 80.6-94.5% and 77.8-91.8% at three different concentrations. The limits of determinations based on S/N=3 were 0.07 ng/g and 0.09 ng/g, which are below the maximum residue limits established in many countries.

• 한국연초학회지
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• 제33권1호
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• pp.21-27
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• 2011

Amadori compounds(1-deoxy-1-amino-2-ketoses) are important precursors of color, flavor and aroma produced in foods. Amadori compounds occur naturally in tobacco. The contribution of amadori compounds to smoke quality has been (of) interest because of their roles of the Maillard reaction in the leaf chemistry. The amounts of these compound in tobacco are affected by the processes of aging, drying and storage conditions. In this study, eight compounds were chemically synthesized because amadori compounds (have not been sold commercially these days.) were not available for obtaining commercially. The aim of this study was to develop the analytical method of amadori compounds in tobacco leaf by the liquid chromatography mass spectrometry using triple quadrupole analyzer(LC-MS/MS). This method was simple, rapid, selective and sensitive, and eight amadori compounds were simultaneously and quantitatively analyzed within 20 minutes. This method showed excellent accuracy and precision. Recovery rates of amadori compounds ranged from 86% to 102%, with relative standard deviation(RSD) ranged from 2.6% to 5.9%. This method was applied to analysis of amadori compounds contents of tobacco leaves in different varieties. Furthermore, it was expected that the method could be extended to the analysis of other amadori compounds.

• 대한원격탐사학회:학술대회논문집
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• 대한원격탐사학회 2005년도 Proceedings of ISRS 2005
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• pp.589-592
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• 2005

Gravity characteristics and Moho undulations are investigated in the Korean peninsula by using satellite gravity data. According to the development of satellite geodesy, gravity potential models which have high accuracy and resolution were released. Using the EIGEN-CGOIC model based on low orbit satellite data such as CHAMP and GRACE, geoid and gravity anomaly were calculated by spherical harmonic analysis. The study area is located at $123^{\circ}\sim132^{\circ}E, 33^{\circ}\sim43^{\circ}$N including Korea. Free-air anomalies, which show the effect of terrain, have the values between $-37\sim724 mgal. After Bouguer correction, the range of simple Bouguer anomalies is $-221\sim246$ mgal. Complete Bouguer anomalies after terrain correction increase from continent to marine. This phenomenon is related rise of Moho discontinuity. The cut-frequency for extraction of Moho undulation was determined by power spectrum analysis, and then 3D inversion modeling was implemented. The mean, maximum, minimum, and standard deviation of Moho depth undulation are -26, -36, -8, and 4.9 krn, respectively.

• Clinical and Experimental Pediatrics
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• 제61권1호
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• pp.6-11
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• 2018

Purpose: Mid-upper-arm circumference (MUAC) is considered an alternative screening method for obesity. The aims of this investigation were to examine the ability of MUAC to correctly identify children with elevated body mass index (BMI) and to determine the best MUAC cutoff point for identification of children with high BMI. Methods: Anthropometric measurements (height, weight, and MUAC) from a cross-sectional sample of 7,921 Pakistani children aged 5-14 years were analyzed. Pearson correlation coefficients between MUAC and other anthropometric measurements were calculated. Receiver operating characteristic curve analysis was used to determine the optimal MUAC cutoff point for identifying children with high BMI. Results: Among 7,921 children, the mean (${\pm}$standard deviation) age, BMI, and MUAC were 10.00 (${\pm}2.86years$), 16.16 (${\pm}2.66kg/m^2$), and 17.73 (${\pm}2.59cm$), respectively. The MUAC had a strong positive correlation with BMI. The optimal MUAC cutoff points indicating elevated BMI in boys ranged from 16.76 to 22.73, while the corresponding values in girls ranged from 16.38 to 20.57. Conclusion: MUAC may be used as a simple indicator of overweight/obesity in children, with reasonable accuracy in clinical settings.

• Journal of Chest Surgery
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• 제27권10호
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• pp.833-837
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• 1994

Lung contusion due to blunt chest trauma is the most common lung injury and correlated with the clinical course and prognosis. Its diagnosis by CT[Computerized Tomogram] gives a more clear and understandable three dimensional view, by which we are able to measure the volume of the contused and entire lung. Other variables are arterial blood gas, number of rib fracture, presence of hemopneumothorax, sternal fracture and clavicle fracture, number of associated non-thoracic injuries, ventilator time and presence of pulmonary complication. Percentage[%] of lung contusion are expressed as mean $\pm$ standard deviation and data analysis was performed by means of multivariate repeated measures analysis of variance to detect significant differences in variables between positive thoracic injury group and negative group. The paired t-test was used. Differences of percentage of lung contusion between groups were assessed by one-way analysis of variance. Simple linear regression was used to perform correlation analysis in the number of rib fracture and ventilator time. A p value less than 0.05 was considered statistically significant. Pneumothorax and the number of associated other injuries affect the amount of lung contusion and pulmonary complication group has more contused lung volume. Arterial blood gas study shows no correlation with the amount of lung contusion statistically. The number of rib fracture correlated with the amount of lung contusion, which also correlated with ventilator time[r=0.56, p<0.05]. In conclusion, quantitative anlysis of lung contusion by CT predicts the clinical course and treatment such as ventilator care.

• 한국연소학회:학술대회논문집
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• 한국연소학회 2005년도 제31회 KOSCO SYMPOSIUM 논문집
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• pp.231-237
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• 2005

Interruption of good fluidization in a fluidized bed ash cooler(FBAC) for discharging bed materials such as sand or coal ash particles from the CFB combustor is frequently happened because of agglomeration of the particles in the bed. This unstable operation may, in the worst case, result in an unscheduled boiler shut down. In this study, we examined the operation problems of the FBAC of Tonghae CFB boiler and studied and introduced the simple detection and solution techniques with analyzing the mixing property and the occurrence of defluidization in a simulated fluidized bed ash cooler system (0.5m-H x 0.5m-W x 1.0m-L). The bridge of the large particles at the bed surface could be observed, and this caused to form the defluidization area at the entrance of the FBAC. The defluidization was affected not only by airflow rates but also by the particles discharging rates as well as particle size distribution in the FBAC. The local defluidization could be detected by analysis of the accumulated standard deviation error at a given period of time. Also, the regulation of the overall or local airflow rate made clearing up the local defluidization possible.

• 대한의용생체공학회:의공학회지
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• 제38권5호
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• pp.219-226
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• 2017

Penalized-likelihood (PL) reconstruction methods for transmission tomography are known to provide improved image quality for reduced dose level by efficiently smoothing out noise while preserving edges. Unfortunately, however, most of the edge-preserving penalty functions used in conventional PL methods contain at least one free parameter which controls the shape of a non-quadratic penalty function to adjust the sensitivity of edge preservation. In this work, to avoid difficulties in finding a proper value of the free parameter involved in a non-quadratic penalty function, we propose a new adaptive method of space-variant smoothing with a simple quadratic penalty function. In this method, the smoothing parameter is adaptively selected for each pixel location at each iteration by using the image roughness measured by a pixel-wise standard deviation image calculated from the previous iteration. The experimental results demonstrate that our new method not only preserves edges, but also suppresses noise well in monotonic regions without requiring additional processes to select free parameters that may otherwise be included in a non-quadratic penalty function.

• 한국정보통신학회:학술대회논문집
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• 한국해양정보통신학회 2007년도 춘계종합학술대회
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• pp.605-608
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• 2007

본 논문은 절대평균 임계값을 웨이블릿 패킷에 적용하여 영상의 노이즈를 제거하기 위한 연구이다. 기존에 사용된 임계값은 표준편차 추정치를 사용하므로 노이즈 크기가 커지면 임계값이 증가하고 영상도 손상된다. 또한 노이즈 크기에 비례하여 임계값이 설정되므로 영상이 변해도 동일한 임계값이 적용되어 복원영상의 PSNR이 저하된다. 반면 절대평균의 임계값을 적용기법은 극단적인 영향을 피할 수 있고 분해된 영상의 통계량에 따라 임계값이 결정되므로 영상의 변화에 적응적이다. 실험 결과 표준편차 추정 임계값을 적용한 웨이블릿 변환기법과 비교하여 12%, 웨이블릿 패킷 기반 노이즈 제거기법과는 6% PSNR이 증가하였다.

• 한국통신학회논문지
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• 제25권6A호
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• pp.782-793
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• 2000

본 논문은 10GHz이상의 주파수 대역을 사용하는 위성 통신 링크에서 강우에 의해 감쇠된 신호 레벨을 동적으로 예측하기 위한 비교적 간단한 예측 기법을 제시한다. 예측 기법은 이산시간 저역 통과 필터링, 기울기에 근거한 예측, 평균 오차 보정, 고정 및 가변 혼합 예측 여유 할당의 4가지 기능 블록을 갖는다. Ku 대역의 측정 데이터로부터 주파수 스케일링에 의해 얻어진 Ka 대역 강우 감쇠 데이터를 이용하여 시뮬레이션을 수행하였다. 평균 오차 보정을 갖는 기울기 예측 기법은 1dB 이하의 표준 편차를 가지며, 평균 오차 보정에 의해 약 1.5~2.5 배의 예측 오차 감소를 보인다. 요구되는 평균 여유 면에서, 혼합 예측 여유 할당은 고정 여유 방법과 가변 여유 방법에 비해 더 적은 평균 여유를 요구한다.