• The Journal of Advanced Prosthodontics
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• 제9권4호
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• pp.294-301
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• 2017

PURPOSE. Temperature increase of $5.5^{\circ}C$ can cause damage or necrosis of the pulp. Increasing temperature can be caused not only by mechanical factors, e.g. grinding, but also by exothermic polymerization reactions of resin materials. The aim of this study was to evaluate influences of the form material on the intrapulpal temperature during the polymerization of different self-curing resin materials for temporary restorations. MATERIALS AND METHODS. 30 provisonal bridges were made of 5 resin materials: Prevision Temp (Pre), Protemp 4 (Pro), Luxatemp Star (Lux), Structure 3 (Str) and an experimental material (Exp). Moulds made of alginate (A) and of silicone (S) and vacuum formed moulds (V) were used to build 10 bridges each on a special experimental setup. The intrapulpal temperatures of three abutment teeth (a canine, a premolar, and a molar,) were measured during the polymerization every second under isothermal conditions. Comparisons of the maximum temperature ($T_{Max}$) and the time until the maximum temperature ($t_{TMax}$) were performed using ANOVA and Tukey Test. RESULTS. Using alginate as the mould material resulted in a cooling effect for every resin material. Using the vacuum formed mould, $T_{Max}$ increased significantly compared to alginate (P<.001) and silicone (P<.001). In groups Lux, Pro, and Pre, $t_{TMax}$ increased when the vacuum formed moulds were used. In groups Exp and Str, there was no influence of the mould material on $t_{TMax}$. CONCLUSION. All of the mould materials are suitable for clinical use if the intraoral application time does not exceed the manufacturer's instructions for the resin materials.

• 한국응용과학기술학회지
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• 제31권2호
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• pp.238-243
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• 2014

합성된 스테인레스 스틸에 대한 NATM(New Austria Tunnel Method) 수지의 기계적 특성은 SEM, FT-IR, 인장특성, 그리고 [NCO]/[OH]의 mole %, 입도분석에 의해 측정하였다. 친환경적인 NATM에 관한 관심이 고조됨에 따라 스테인레스 등의 금속에 코팅하는 무용제 도료를 합성하였다. 폴리올, IPDI, 충진제, 실리콘 계면활성제, 촉매 등이 함유된 기존 NATM수지보다 폴리올, MDI, 충진제, 실리콘 계면활성제, 촉매, 가교제가 함유되어 합성된 NATM 수지의 도료가 내구력과 강도가 양호하였다. 견고한 NATM 수지의 기계적 특성은 가교와 [NCO]/[OH]의 mole%가 증가함에 따라 강도가 증가하였다. 결론적으로 NATM의 가교된 미세조직는 스테인레스 스틸 같은 금속물질 코팅에 좋은 물질이다.

• International Journal of Concrete Structures and Materials
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• 제2권1호
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• pp.21-25
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• 2008

Surface treatments act as a barrier between the environment and the concrete, preventing or retarding the entry of harmful substances and cutting off the transportation path into concrete. The effectiveness of a surface protection preventing the permeation depends on how close and strongly connected are the resin molecules. This work intends to contribute to a better understanding of the performance of protected concrete in chemically aggressive environments, by presenting results of ion diffusion and resistance to aggressive solutions of several hydrophobic agents and coatings used to protect concrete. Three different types of surface protections were tested: silicone hydrophobic agent, acrylic and epoxy coatings. The obtained results indicate that the overall performance of epoxy resin was better than the other selected types of protections.

• 대한치과기공학회지
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• 제38권3호
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• pp.185-191
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• 2016

Purpose: The purpose of this study were to evaluate the quality of dental prostheses printed by 3-dimensional printing system. Methods: Mater model was prepared and ten study models were fabricated. Ten single crowns were printed by 3D-printing system(Resin group) and another ten single crowns using casting method were manufactured(Metal group). The marginal adaptation of single crowns were measured using by silicone replica technique. Silicone replicas were sectioned four times. The marginal adaptations were evaluated using by digital microscope. Statistical analyses were performed with Mann-Whitney test(${\alpha}=0.05$). Results: $Mean{\pm}standard$ deviations of all marginal adaptations were $92.1(20.0){\mu}m$ for Metal group and $69.7(12.3){\mu}m$ for Resin group. Two groups were no statistically significant differences(p>0.05). Conclusion: Marginal adaptation of single crowns printed by 3D-printing system were ranged within the clinical recommendation.

• 대한치과보철학회지
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• 제30권3호
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• pp.411-436
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• 1992

The purpose of this study was to assess the adhesion of resilient denture liners (such as, heat-cured silicone molloplast B,cold- cured silicone Mollosil) to polymethyl metacrylate (K-33) and metal (Megalloy) in the laboratory by peel test. The resilient denture lines were processed according to manufactures instruction, onto prepared specimens(original resin base plate, rough resin base plate, stippled metal plate, mesh metal plate ) 75mm long and 25m wide. And then, the peel test was performed by instron. The results were as follows : 1. The bonding strength of Mollosil was stronger than that of Molloplast B except the specimen of stippled metal plate. 2. The tensile strength of Mollosil was weaker than that of Molloplast Bas tearing of Mollosil was occured in the peel test. 3. Mesh metal plate had the highest bonding strength in the case of Molloplast B and Mollosil. But stippled metal plate have high bonding strength in the case of Molloplast B and have the lowest bonding strength in the case of Mollosil. 4. The bonding strength of rough resin base plate was stronger than that of original resin base plate in the case of Molloplast B and Mollosil. 5. The bonding strength of metal plates was stronger than that of resin base plates in the case of Molloplast B and Mollosil except the case of bonding strength between the stippled metal plate and Mollosil. 6. It seems that the Increase of surface and retention form of metal plate and resin base plate produces higher physical bonding strength.

• 한국전기전자재료학회:학술대회논문집
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• 한국전기전자재료학회 2008년도 하계학술대회 논문집 Vol.9
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• pp.495-496
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• 2008

This paper describes the influence of Ultra-violet irradiation on time to tracking resistance of epoxy insulating materials by use of the inclined plane test. And, the influence of surface degradation was evaluated through several method such as measurement of contact angle, surface roughness, using a scanning electron microscopy. As the 1000 hours of the surface degradation with UV-CON, the flashover time decreases at different rates depending on epoxy resin and silicone rubber specimen. As the duration of the surface degradation with UV-CON is prolonged, the contact angle of epoxy resin decreases at the rate of degradation time, while that of silicone rubber was not exchanged. It is assumed that this phenomenon is related to the decrease in hydrophobicity of the surface of the materials. Also, as to epoxy resin, the decrease of hydrophobicity due to surface degradation with UV-CON is greater than that resulting from surface degradation with WOM. The UV radiation produced chalking and crazing on the surface of the insulating materials specimen.

• 대한치과기공학회지
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• 제42권1호
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• pp.9-16
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• 2020

Purpose: The purpose of this study was to compare the marginal and internal fit of lithium disilicate ceramic inlay produced by heat pressing that inlay pattern made by subtractive manufacturing and additive manufacturing method. Methods: A mandibular lower first molar that mesial occlusal cavity (MO cavity) die was prepared. After fabricating an epoxy resin model using a silicone impression material, epoxy resin die was scanned with a dental model scanner to design an MO cavity inlay. The designed STL pile was used to fabricate wax patterns and resin patterns, and then lithium disilicate ceramic inlays were fabricated using hot-press method. For the measurement of the marginal and internal gap of the lithium disilicate, silicone replica method was applied, and gap was measured through an optical microscope (x 80). Data were tested for significant differences using the Mann-Whitney Utest. Results: The marginal fit was 103.56±9.92㎛ in the MIL-IN group and 81.57±9.33㎛ in the SLA-IN group, with a significant difference found between the two groups (p<0.05). The internal fit was 120.99±17.52㎛ in the MIL-IN group and 99.18±6.65㎛ in the SLA-IN group, with a significant difference found between the two groups (p<0.05). Conclusion: It is clinically more appropriate to apply the additive manufacturing than subtractive manufacturing method in producing lithium disilicate inlay using CAD/CAM system.

• Design & Manufacturing
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• 제8권2호
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• pp.46-49
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• 2014

Silicone is recently used for LED chip lense due to its good thermal stability and optical transmittance. In order to predict residual stress which causes optical briefringence and mechanical warpage of silicone, finite element analysis was conducted for curing process during silicone molding. For analysis of curing process, a dynamic cure kinetics model was derived based on the differential scanning calorimetry(DSC) test and applied to the material properties for finite element analysis. Finite element simulation result showed that the slow cure reduced abrupt reaction heat and it was predicted decrease of the residual stress.

• Transactions on Electrical and Electronic Materials
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• 제17권3호
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• pp.155-158
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• 2016

The effect of microsilica content modified with silicone-modified epoxy on electrical and mechanical properties of cycloaliphatic epoxy/microsilica system was investigated. The cycloaliphatic epoxy resin was diglycidyl 1,2-cyclohexanedicarboxylate and curing agent was an anhydride. Surface of microsilica was modified with silicone-modified epoxy. Electrical breakdown strength, the most important property for electrical insulation materials was tested. Tensile and flexural tests were also performed using universal testing machine (UTM). The microcomposite with 60 wt% microsilica shows maximum values in electrical breakdown strength.

• 대한치과보철학회지
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• 제29권2호
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• pp.59-66
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• 1991

This study was designed to investigate the marginal accuracy of resin temporary crown with different matrix in indirect technique. Matrices were made from irreversible hydrocolloid impression material, putty type of vinyl polysiloxane silicone rubber and vacuum formed plastic sheet. The marginal discrepancies of the temporary crowns were measured using a measuring microscope. The obtained results were as follows 1. The marginal accuracy temporary crown using vinyl polysiloxane silicone rubber or vacuum formed plastic form was better than that of the temporary crown using irreversible hydrocolloid impression material. 2. The marginal accuracies of the temporary crown using the irreversible hydrocolloid impression material and putty type of the vinyl polysiloxane silicone rubber obtained the best results at the distal measuring point. 3. The vacuum formed plastic form was recorded a more acceptable marginal accuracy at the distal and mesial measuring points.