• 제목/요약/키워드: Sigma S

검색결과 1,136건 처리시간 0.023초

GC에서 검출한계 결정을 위한 새로운 접근 방법에 대한 연구 (Study on the new approaching method to determine limit of detection by gas chromatography)

  • 오도석;신경애;이지아;임종호;신미선
    • 한국산업보건학회지
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    • 제20권4호
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    • pp.217-224
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    • 2010
  • The purity methods to determine LOD/LOQ using standard deviation of the residual, intercept and blank by IUPAC and ACS describe many of the pitfalls and pose significant challenges to analytical chemists. Therefore, the aim of this study is the development of the simple, easy, convenient and statistically significant method to determine LOD in quantitative analysis of organic solvents by GC. The new approaching method by linearization in the given concentration range used coefficient of variation ; ${\sigma}_{n-1}$/S(standard deviation, ${\sigma}_{n-1}$ and average, S) of sensitivity(Response/concentration). The comparison of results among the purity methods(IUPAC and ACS) and the linearization have been fulfilled the F-test for standard deviations and t-test for LOD range values. The results of F-test and t-test are satisfied within 95 % confidence level, respectably. The LOD values determined by the new procedure are n-Hexane 0.0116 mg/$m^3$, Toluene 0.0807 mg/$m^3$, and o-Xylene 0.0494 mg/$m^3$. Because the standard deviation of the residual, intercept and blank and the slope of calibration curve are not calculated and the new approaching method use the coefficient of variation of sensitivity by linearization, this new method is simple, easy, convenient and statistically significant. In future, many chemical analysts will expect to applicate and routinely use this method in the all quantitative analysis.

족부보장구(A.F.O.) 판스프링용 Glass/Epoxy와 Aramid/Epoxy의 충격속도 변화에 따른 손상 거동 (The Damage Behavior of Glass/Epoxy and Aramid/Epoxy in Leaf Spring of Ankle Foot Orthosis (A.F.O) due to the Various Impact Velocities)

  • 송삼홍;오동준;정훈희;김철웅
    • 대한기계학회논문집A
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    • 제28권10호
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    • pp.1526-1533
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    • 2004
  • The needs of walking assistant device such as the Ankle Foot Orthosis (A.F.O) are getting greater than before. However, most of the A.F.O are generally imported rather than domestic manufacturing. The major reason of high import reliability is the rack of impact properties of domestic commercial products. Therefore, this research is going to focus on the evaluation of impact properties of the A.F.O which has the high import reliability. Unfortunately, these kinds of researches are not performed sufficiently. This research is going to evaluate impact energy behavior in composite materials such as the glass/epoxy (S-glass, [0/90]sub 2S/) and the aramid/epoxy (Kevlar-29, woven type, 8 ply) of ankle foot orthosis. The approach methods were as follows. 1) The history of impact load and impact energy due to the various velocities. 2) Relationship between the deflection and damage shape according to the impact velocities. 3) The behavior of absorbed energy and residual strength rate due to the various impact velocities.

STUDY OF M82 USING SPECTRA FROM THE INFRARED SPACE OBSERVATORY

  • SOHN JUNGJOO;ANN H. B.;PAK SOOJONG;LEE H. M.
    • 천문학회지
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    • 제34권1호
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    • pp.17-24
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    • 2001
  • We have studied the central parts of M82, which is a well-known infrared luminous, starburst galaxy, by analyzing archival data from the Infrared Space Observatory (ISO). M82 was observed at 11 positions covering $\pm$45" from the center along the major axis. We analyzed 4 emission lines, [ArIII] 8.99 ${\mu}m$, $H_2$ 17.034 ${\mu}m$, [FeII] 25,98 ${\mu}m$, and [SiII] 34,815 ${\mu}m$ from $SWSO_2$ data. The integrated flux distributions of these lines are quite different. The $H_2$ line shows symmetric twin peaks at $\~$18" from the center, which is a general characteristic of molecular lines in starburst or barred galaxies. This line appears to be associated with the rotating molecular ring at around $\~$200 pc just outside the inner spiral arm. The relative depletion of the $H_2$ line at the center may be due to the active star formation activity which dissociates the $H_2$ molecules. The other lines have peaks at the center and the distributions are nearly symmetric. The line profiles are deconvolved assuming that both intrinsic and instrumental profiles are Gaussian. The velocity dispersion outside the core is found to be $\~50 km s^{-1}$. The central velocity dispersion is much higher than $50 km s^{-1}$, and different lines give different values. The large central velocity dispersion ($\sigma$) is mostly due to the rotation, but there is also evidence for a high $\sigma$ for [ArIII] line. We also generated position-velocity maps for these four lines. We found very diverse features from these maps.

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THE FRACTAL DIMENSION OF THE 𝜌 OPHIUCUS MOLECULAR CLOUD COMPLEX

  • Lee, Yongung;Li, Di;Kim, Y.S.;Jung, J.H.;Kang, H.W.;Lee, C.H.;Yim, I.S.;Kim, H.G.
    • 천문학회지
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    • 제49권6호
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    • pp.255-259
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    • 2016
  • We estimate the fractal dimension of the ${\rho}$ Ophiuchus Molecular Cloud Complex, associated with star forming regions. We selected a cube (${\upsilon}$, l, b) database, obtained with J = 1-0 transition lines of $^{12}CO$ and $^{13}CO$ at a resolution of 22" using a multibeam receiver system on the 14-m telescope of the Five College Radio Astronomy Observatory. Using a code developed within IRAF, we identified slice-clouds with two threshold temperatures to estimate the fractal dimension. With threshold temperatures of 2.25 K ($3{\sigma}$) and 3.75 K ($5{\sigma}$), the fractal dimension of the target cloud is estimated to be D = 1.52-1.54, where $P{\propto}A^{D/2}$, which is larger than previous results. We suggest that the sampling rate (spatial resolution) of observed data must be an important parameter when estimating the fractal dimension, and that narrower or wider dispersion around an arbitrary fit line and the intercepts at NP = 100 should be checked whether they relate to firms noise level or characteristic structure of the target cloud. This issue could be investigated by analysing several high resolution databases with different quality (low or moderate sensitivity).

구조선의 도착시간 산출을 위한 실험 데이터 구축 (Construction of experimental data to calculate the arrival time of the rescue ship)

  • 정재용;정초영
    • Journal of Advanced Marine Engineering and Technology
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    • 제41권1호
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    • pp.111-117
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    • 2017
  • 조난 사고 발생 시 구조선의 현장 도착시간은 매우 중요하다. 본 연구에서는 구조선의 도착시간을 추정하기 위한 실험 데이터 구축 방법을 제시하였다. 이를 위하여 선박통항확률분포를 활용하였다. 목포항을 연구 대상 해역으로 선정하고, 1년간의 AIS 데이터를 활용하였다. 선박통항확률분포를 조사하기 위해 기준선을 설정하고, 선박의 횡거리 분포를 계산하여, 정규분포와 이중 가우시안 혼합분포로 적합 시킨 후 각 매개변수를 추출하였다. 정규분포의 ${\mu}$, ${\mu}{\pm}1{\sigma}$와 이중 가우시안 혼합분포의 ${\mu}_1$ 위치를 각각 변침점으로 설정하여 위치와 확률을 도출하였다. 이를 매개변수 종류별로 연결하여 시나리오를 구축하여 도착시간을 계산할 수 있었다.

이축 정적 하중이 부가된 반복 인장 혹은 비틀림 하중하에서 균열 발생과 성장 거동 (Behavior of Fatigue Crack Initiation and Propagation under Cyclic Tensile or Torsional Loading with Superimposed Static Biaxial Load)

  • 허용학;박휘립;권일범;김진영
    • 대한기계학회논문집A
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    • 제24권6호
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    • pp.1446-1455
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    • 2000
  • Fatigue crack initiation and propagation behavior under cyclic biaxial loading has been investigated using thin-walled tubular specimen with a hole. Two types of biaxial loading system, i.e. cyclic tensile loading with super-imposed static torsional load and cyclic torsional loading with superimposed static tensile load, with various values of the biaxial loading ratio, $\tau$ s/ $\sigma$ max (or $\tau$ max/ $\sigma$s) were employed. Fatigue tests show that fatigue crack near the hole initiates and propagates at 900 and 450 direction to the longitudinal direction of the specimen under cyclic tensile and torsion loading with static biaxial stress, respectively, and the static biaxial stress doesn't have any great influence on fatigue crack initiation and growth direction. Stress analysis near the hole of the specimen shows that the crack around the hole initiates along the plane of maximum tangential stress range. Fatigue crack growth rates were evaluated as functions of equivalent stress intensity factor range, strain energy density factor range and crack tip opening displacement vector, respectively. It is shown that the biaxial mode fatigue crack growth rates can be relatively consistently predicted with these cyclic parameters.

Doublet 반사경을 이용한 도트 사이트 장치의 개발 (Development of the Dot Sight Device by Using the Doublet Reflector)

  • 이동희
    • 한국안광학회지
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    • 제13권1호
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    • pp.65-69
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    • 2008
  • 목적: Doublet 반사경을 이용한 조준사격용 도트 사이트 장치의 개발. 방법: Sigma 2000 광학 설계 프로그램으로 Singlet 반사경과 Doublet 반사경을 설계하여 비교 검토하였다. 결과: 유한광선수차 분석에서 기존 Singlet 반사경을 사용한 도트 사이트 장치에 비해 시차(parallax)가 제거된 유효 시야가 3.3배 확대되는 성능을 보인다. Doublet 반사경을 사용하는 경우 광학계의 중심 두께가 기존 Singlet 반사경을 사용한 경우보다 2배 이상 두꺼워지기 때문에 목표점이 관측자의 망막에 결상할 때 Singlet 반사경의 경우와 같이 제1면과 제3면의 곡률반경을 동일하게 할 경우에는 배율 변화가 나타난다. 이를 극복하기 위해 Doublet 반사경인 경우에는 어포칼 조건을 만족하는 것이 필요하다. 결론: 기존의 Singlet 반사경의 방식보다 시차(parallax)가 제거된 유효 시야가 3.3배 확대되는 성능을 가지는 Doublet 반사경을 이용한 조준사격용 도트 사이트 장치를 개발하였다.

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Dependence of Barredness of Late-Type Galaxies on Galaxy Properties and Environment

  • 이광호;박창범;이명균;최윤영
    • 천문학회보
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    • 제35권1호
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    • pp.75.2-75.2
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    • 2010
  • We investigate the dependence of occurrence of bar in galaxies on galaxy properties and environment. The environmental conditions considered include the large-scale background density and distance to the nearest neighbor galaxy. We use a volume-limited sample of 33,296 galaxies brighter than $M_r$=-19.5+5logh at $0.02{\leqq}z{\leqq}0.05489$, drawn from the Sloan Digital Sky Survey Data Release 7. We classify the galaxies into early and late types, and identify bars by visual inspection. We find that the fraction of barred galaxies ($f_{bar}$) is 18.2% on average in the case of late-type galaxies, and depends on both u-r color and central velocity dispersion $(\sigma);f_{bar}$ is a monotonically increasing function of u-r color, and has a maximum value at intermediate velocity dispersion (${\sigma}{\simeq}170km\;s^{-1}$). This trend suggests that bars are dominantly hosted by systems having intermediate-mass with no recent interaction or merger history. We also find that $f_{bar}$ does not directly depend on the large-scale background density as its dependence disappears when other physical parameters are fixed. We discover the bar fraction decreases as the separation to the nearest neighbor galaxy becomes smaller than 0.1 times the virial radius of the neighbor regardless of neighbor's morphology. These results imply that it is difficult for bars to be maintained during strong tidal interactions, and that the source for this phenomenon is gravitational and not hydrodynamical.

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Thermal conductivity of individual single-crystalline Bi nanowires grown by stress-induced recrystallization

  • Roh, Jong-Wook;Chen, Ren-Kun;Lee, Jun-Min;Ham, Jin-Hee;Lee, Seung-Hyn;Hochbaum, Allon;Hippalgaonkar, Kedar;Yang, Pei-Dong;Majumdar, Arun;Kim, Woo-Chul;Lee, Woo-Young
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 2009년도 춘계학술대회 논문집
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    • pp.23-23
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    • 2009
  • It has been challenging to increase the thermoelectric figure of merit ($ZT=S^2{\sigma}T/\kappa$) of materials, which determine the efficiency of thermoelectric devices, because the three parameters Seebeck coefficient (S), electrical conductivity ($\sigma$), and thermal conductivity ($\kappa$) of bulk materials are inter-dependent. With the development of nanotechnology, ZT values of nanostructured materials are predicted to be enhanced by classical size effects and quantum confinement effects. In particular, Bi nanowires were suggested as one of ideal thermoelectric materials due to the expected quantum confinement effects for the simultaneous increase in Sand. In this work, we have investigated the thermal conductivity of individual single crystalline Bi nanowires with d = 98 nm and d = 327 nm in the temperature range 40 - 300 K using MEMS devices. The for the Bi nanowire with d = 98 nm was observed to be ~ 1.6 W/m-K at 300 K, which is much lower than that of Bi bulk (8 W/m-K at 300 K). This indicates that the thermal conductivity of the Bi suppressed due to enhanced surface boundary scattering in one-dimensional structures. Our results suggest that Bi nanowires grown by stress-induced method can be used for high-efficiency thermoelectric devices.

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시그마 델타 변조에 의한 LED 드라이버의 입력 콘트롤러 설계 (Delta Sigma Modulation of Controller Input Signal for the LED Light Driver)

  • 엄기홍
    • 한국인터넷방송통신학회논문지
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    • 제16권2호
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    • pp.151-155
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    • 2016
  • 우리는 이 논문에서 ADPCM (adaptive differential pulse code modulation)을 적용함으로써 디밍 콘트롤러를 갖는 LED 드라이버의 설계를 제시한다. ADPCM 장비는 고해상도를 가지고 LED 전류를 정확하게 제어하며, 고조파 전류 펄스의 퍼짐으로 인하여 초래되는 RFI 를 감소시켜 준다. 또한 제어 동작의 정밀도를 높여준다. 이 연구에서 LED에 펄스 전류를 인가함으로써 고효율 에너지의 LED를 제어하는 디지털 제어회로의 설계를 제시한다. 우리가 설계한 LED 전류구동시스템은 디지털 제어 부와 아날로그 SMPS (스위치 모드 파워 서플라이)를 별도로 구현한 두개의 시스템이다. 입력레벨이 0.7 인 경우의 시뮬레이션 결과는 시그마 델타 변조를 하여 얻은 D/A 컨버터의 출력을 나타내었다. 개수가 510 개인 펄스신호의 경우 0.15 % 의 정밀도를 얻을 수 있었다.