• Title/Summary/Keyword: Si infiltration

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Fabrication and Mechanical Properties of $SiC_p/Al$ Composites by Pressureless Infiltration Technique (무가압침투법에 의한 $SiC_p/Al$ 복합재료의 제조 및 기계적 특성)

  • Jin, H.G.;Oh, M.S.;Kim, Y.S.
    • Journal of Power System Engineering
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    • v.5 no.4
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    • pp.74-81
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    • 2001
  • The infiltration behavior of molten Al-alloy, microstructures, hardness, and the interfacial reactions of $SiC_p/Al$ composites fabricated by the pressureless infiltration technique were investigated. It was made clear that both the weight fraction of SiC reinforcement and additive Mg content considerably influenced on the infiltration behavior of the molten Al-alloy matrix. Complete infiltration of molten Al-alloy achieved under the conditions that weight fraction of SiC content is more than 30wt%, and additive Mg content is more than 9wt%. Interfacial region of Al-alloy matrix and SiC reinforcement phase, $Mg_2Si$ was formed by the reaction between Mg and SiC. Another reaction product AlN was also formed by the reaction between Al-alloy matrix and gas atmosphere nitrogen.

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Nicalon-Fiber-Reinfored SiC Composites Via Infiltration (Infiltration 공정으로 제조한 Nicalon 섬유강화 SiC 복합재료)

  • 김민수;김영욱;한경섭;박정현
    • Journal of the Korean Ceramic Society
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    • v.30 no.12
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    • pp.993-998
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    • 1993
  • Nicalon-fiber-reinforced SiC composites were fabricated via polymer solution infiltration/chemical vapor infiltration (PSI/CVI) and CVI. Specifically, data were taken and compared for flexural strength, fracture toughness, and processing time. The two process resulted in comparable mechanical properties, and PSI/CVI process resulted in significantly reduced infiltration time.

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A study on the wettability of the Al-Li/SiC interface (Al-Li/SiC 계면의 젖음성에 관한 연구)

  • Kim, Ki-Bae;Kim, Do-Hyang;Lee, Ho-In
    • Journal of Korea Foundry Society
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    • v.12 no.2
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    • pp.149-154
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    • 1992
  • The wetting behaviour of SiC/Al-Li composite interface has been investigated by using an infiltration method. The critical pressure for melt infiltration into SiC particulate preform has been determined by measuring the melt infiltration distance changes with the variation of applied pressure. The threshold pressure of pure Al, Al-0.2wt%Li, Al-0.5wt%Li for melt infiltration are 3.94, 3.93, $3.7Kg/cm^2$ respectively, which implies a slight improvement in wettability of SiC/Al composite by addition of Li. The threshold pressure for melt infiltration also changes with the variation of other parameters such SiC particulate size, SiC particulate fraction and melt temperature.

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Preparation of SiC-Al alloy Composite by Pressureless Powder Packing Forming Method (분말 충전 성형법을 이용한 SiC-Al Alloy 복합체의 제조)

  • 박정현;송준광;백승수;염강섭;강민수
    • Journal of the Korean Ceramic Society
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    • v.34 no.4
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    • pp.343-350
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    • 1997
  • To fabricate the ceramic/metal(SiC/ Al alloy) composite, SiC preform was prepared by Pressureless Powder Packing Forming Method and 6061 Al alloy was infiltrated into the preform. Uniform compact having an average pore size of 10 ${\mu}{\textrm}{m}$ and narrow pore size distribution was prepared. Phenolic resin solution(40 wt%) was penetrated into the SiC compact, and then the compact was preheated at the temperature of 120$0^{\circ}C$. The pore size distribution and the microstructure of the preform were not changed by preheating. An uniform microstructure without any crack in the preform was obtained in SiC-Al alloy composite. The infiltration of 6061. Al alloy into the preform began at the temperature of 130$0^{\circ}C$ and the amount of infiltration increased in proportion to the infiltration temperature and the soaking time. The increasement rate of the infiltration amount decreased after 3 h. As a result of the infiltration at 140$0^{\circ}C$ for 4 h, Al alloy was well distributed in the interparticle channels and the relative density of the composite was above 98%. The strength and the fracture toughness of the composite were 303 MPa and 21.65 MPam1/2, respectively.

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Shear strength characteristics of a compacted soil under infiltration conditions

  • Rahardjo, H.;Meilani, I.;Leong, E.C.;Rezaur, R.B.
    • Geomechanics and Engineering
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    • v.1 no.1
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    • pp.35-52
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    • 2009
  • A significantly thick zone of steep slopes is commonly encountered above groundwater table and the soils within this zone are unsaturated with negative pore-water pressures (i.e., matric suction). Matric suction contributes significantly to the shear strength of soil and to the factor of safety of unsaturated slopes. However, infiltration during rainfall increases the pore-water pressure in soil resulting in a decrease in the matric suction and the shear strength of the soil. As a result, rainfall infiltration may eventually trigger a slope failure. Therefore, understanding of shear strength characteristics of saturated and unsaturated soils under shearing-infiltration (SI) conditions have direct implications in assessment of slope stability under rainfall conditions. This paper presents results from a series of consolidated drained (CD) and shearing-infiltration (SI) tests. Results show that the failure envelope obtained from the shearing-infiltration tests is independent of the infiltration rate. Failure envelopes obtained from CD and SI tests appear to be similar. For practical purposes the shear strength parameters from the CD tests can be used in stability analyses of slopes under rainfall conditions. The SI tests might be performed to obtain more conservative shear strength parameters and to study the pore-water pressure changes during infiltration.

Diffusion of Si Vapor Infiltrating into Porous Graphite (다공성 흑연의 기공내부로 침투하는 Si 증발입자의 확산)

  • Park, Jang-Sick;Hwang, Jungtae
    • Journal of the Korean institute of surface engineering
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    • v.49 no.1
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    • pp.104-109
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    • 2016
  • Graphite's thermal stability facilitates its widespread use as crucibles and molds in high temperatures processes. However, carbon atoms can be rather easily detached from pores and outer surfaces of the graphite due to the weak molecular force of the c axis of graphites. Detached carbon atoms are known to become a source of dust during fabrication processes, eventually lowering the effective yield of products. As an effort to reduce these problems of dust scattering, we have fabricated SiC composites by employing Si vapor infiltration method into the pores of graphites. In order to understand the diffusion process of the Si vapor infiltration, Si and C atomic percentages of fabricated SiC composites are carefully measured and the diffusion law is used to estimate the diffusion coefficient of Si vapor. A quadratic equation is obtained from the experimental results using the least square method. Diffusion coefficient of Si vapor is estimated using this quadratic equation. The result shows that the diffusion length obtained through the Si vapor infiltration method is about 10.7 times longer than that obtained using liquid Si and clearly demonstrates the usefulness of the present method.

Influence of Winding Patterns and Infiltration Parameters on Chemical Vapor Infiltration Behaviors of SiCf/SiC Composites (SiCf/SiC 복합체의 화학기상침착 거동에 미치는 권선 구조와 침착 변수의 영향)

  • Kim, Daejong;Ko, Myoungjin;Lee, Hyeon-Geun;Park, Ji Yeon;Kim, Weon-Ju
    • Journal of the Korean Ceramic Society
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    • v.51 no.5
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    • pp.453-458
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    • 2014
  • SiC and its composites have been considered for use as nuclear fuel cladding materials of pressurized light water reactors. In this study, a $SiC_f$/SiC composite as a constituent layer of SiC triplex fuel cladding was fabricated using a chemical vapor infiltration (CVI) process in which tubular SiC fiber preforms were prepared using a filament winding method. To enhance the matrix density of the composite layer, winding patterns, deposition temperature, and gas input ratio were controlled. Fiber arrangement and porosity were the main parameters influencing densification behaviors. Final density of the composites decreased as the SiC fiber volume fraction increased. The CVI process was optimized to densify the tubular preforms with high fiber volume fraction at a high $H_2$/MTS ratio of 20 at $1000^{\circ}C$; in this process, surface canning of the composites was effectively retarded.

Fabrication and Mechanical Property of $Al_2$O$_.3$/Al Composite by Pressureless Infiltration (무가압 침윤법에 의한 $Al_2$O$_.3$/Al 복합재료 제조와 기계적 특성)

  • 이동윤;박상환;이동복
    • Journal of the Korean Ceramic Society
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    • v.35 no.3
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    • pp.303-309
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    • 1998
  • The fabrication of Al2O3/Al composite by pressureless infiltration was investigated by the change of Mg and Si content in Al alloy infiltration process and infiltration atmosphere. The effect of alloying elements infiltration atmosphere and interfacial reactants between Al alloy matrix and Al2O3 particles were in-vestigated in terms of bendingstrength and harness test,. The fabrication of Al2O3/Al composite by the vestigated in terms of bending strength and hardness test. The fabrication of Al2O3/Al composite by the pressureless infiltration was done in nitrogen atmosphere with Mg in Al alloy. It was successfully fabricated at $700^{\circ}C$ according to Mg contents in Al alloy and infiltration condition. Because Mg in the Al alloy and ni-trogen atmosphere of infiltratio condition produced Mg-N compound(Mg3N2) it decreased the wetting an-gle between molten Al alloy and Al2O3 particles by coating on surface of Al2O3 particles. The fracture strength of Al2O3/Al-Mg composite was 800MPa and Al2O3/Al-Si-Mg composite was 400MPa. Si in Al alloy decreased the interfacial strength between Al alloy matrix and Al2O3 particles.

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Property Evaluation of Reaction Sintered SiC/SiC Composites Fabricated by Melt Infiltration Process (용융함침법에 의한 반응소결 SiC/SiC 복합재료의 특성 평가)

  • Lee, Sang-Pill;Shin, Yun-Seok;Kohyama, Akira
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.31 no.2 s.257
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    • pp.205-210
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    • 2007
  • SiC/SiC composites and monolithic SiC materials have been fabricated by the melt infiltration process, through the creation of crystallized SiC phase by the chemical reaction of C and Si. The reinforcing material used in this system was a braided Hi-Nicalon SiC fiber with double interphases of BN and SiC. The microstructures and the mechanical properties of RS-SiC based materials were investigated through means of SEM, TEM, EDS and three point bending test. The matrix morphology of RS-SiS/SiC composites was greatly composed of the SiC phases that the chemical composition of Si and C is different. The TEM analysis showed that the crystallized SiC phases were finely distributed in the matrix region of RS-SiC/SiC composites. RS-SiC/SiC composites also represented a good flexural strength and a high density, accompanying a pseudo failure behavior.

A Study on the Si-SiC Composites Fabricated by Pressureless Powder Packing Forming Method (무가압 분말 충전 성형법에 의해 제조된 Si-SiC 복합체에 관한 연구)

  • 박정현;임은택;성재석;최헌진;이준석
    • Journal of the Korean Ceramic Society
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    • v.32 no.6
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    • pp.710-718
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    • 1995
  • The new forming method, Pressureless Powder Packing Forming Method was applied to the manufacturing of reaction sintered SiC. After the experiments of vibratory powder packing and binder infiltration, the abrasive SiC powder of which mean size is 45${\mu}{\textrm}{m}$ was selected to this forming method. Uniform green bodies with porosity of 45% and narrow pore size distribution could be formed by this new forming method. Also, complex or varied cross-sectional shapes could be easily manufactured through the silicone rubber mould used in this forming method. Maximum 15 wt% amorphous carbon was penetrated into green body by multi impregnation-carbonization cycles. And reaction-bonded SiC was manufactured by infiltration of SiC-carbon shaped bodies with liquid silicon.

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