• Title/Summary/Keyword: Shear bond test

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Push-Shear Bond Strength of Veneering Ceramics and Zirconia Ceramic (비니어 세라믹과 지르코니아 세라믹의 Push-Shear 결합강도)

  • Ahn, Jae-Seok;No, Hyeong-Rok;Lee, Jung-Hwan
    • The Journal of the Korea Contents Association
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    • v.15 no.9
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    • pp.384-394
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    • 2015
  • The purpose of this study was to evaluate the push-shear bond strength between five commercial zirconia veneering ceramics and zirconia core cylinder, and to investigate the effect of biaxial flexural strength and zirconia liner glass treatments. The biaxial flexural strengths of the veneering ceramics were evaluated by a piston-on-three-ball test. The bond strengths between the Y-TZP cylinder and zirconia veneering ceramics were evaluated using the push-shear bond strength test. The data was analyzed using two-way ANOVA and Scheffe's test. The biaxial flexural strength of Cercon ceram kiss (CE) was higher than those of the other groups. The glass-treated and Triceram zirconia groups showed the highest value and the Creation ZI(CR) showed the lowest. In all groups, the liner glass treatment groups showed significantly higher push-shear bond strength than those without(P<0.05). The liner glass treatments of zirconia can improve the bond strength between the zirconia ceramic core and veneering ceramics.

Effect of sandblasting and liner on shear bond strength of veneering ceramic to zirconia (샌드블라스팅 처리와 라이너가 지르코니아와 전장도재의 전단결합 강도에 미치는 영향)

  • Kim, Ki-Baek;Kim, Jae-Hong
    • Journal of Technologic Dentistry
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    • v.43 no.1
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    • pp.6-12
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    • 2021
  • Purpose: This study aimed to compare the shear bond strength between zirconia cores and veneer ceramics as per the sand blasting and liner treatments. Methods: The following 4 groups of zirconia-veneering ceramic specimens were prepared: (1) Group I, untreated; (2) Group II, with 110 ㎛ aluminium oxide (Al2O3) sandblasting; (3) Group III, with liner (IPS e.max ZirLiner; Ivoclar Vivadent); and (4) Group IV, with 110 ㎛ Al2O3 sand blasting and liner. Surface roughness was measured for all the prepared specimens, and the surface morphology was observed using a scanning electron microscope. All the samples (n=40) were fixed with measuring jigs, and shear bond strengths were obtained using a universal testing machine with a crosshead speed of 0.5 mm/min. The shear bond strength data were analyzed using one-way analysis of variance and t-test. The post hoc comparison was performed using the Tukey's test (α=0.05). Results: A significant difference in the surface roughness was observed between the specimens of groups I and II (p<0.05). Surface treatment with liner and sandblasting showed higher shear bond strength between zirconia core and veneering ceramic (p<0.05). Conclusion: The sand blasting and liner treatment increased the shear bond strength between zirconia core and veneering ceramic.

COMPARISON OF SHEAR BOND STRENGTHS OF FOUR DENTINAL ADHESIVES (네가지 상아질 접착제의 전단 결합 강도 비교)

  • Cho, Kyeong-Mee;Hur, Bock;Lee, Hee-Joo
    • Restorative Dentistry and Endodontics
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    • v.21 no.1
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    • pp.280-288
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    • 1996
  • The purpose of this study was to assess comparatively the shear bond strength on dentin of four dentin bonding agents used in conjunction with light-curing composite resins. Clearfil New Bond, Scotchbond Multipurpose Dentin Adhesive, All-Bond 2 and X-R Bond were applicated on labial dentin surfaces just below dentin - enamel juction of bovine incisor teeth. After shear bond strength testing with the universal testing machine, the bonding interface of the specimens were observed under light stereomicroscope. Following results were obtained. 1. The shear bond strength was high in the order of B,C,D,A and group B Scotchbond Multipurpose Dentine Adhesive revealed greater bond strength than Clearfil New Bond and X-R Bond. (p<.001) 2. When using ANOVA and Duncan's multiple range test, there were statistical differences among the four groups, except between group Band C,group D and A. 3. There was no relationship between mode of failure and shear bond strength.

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Bond Strength between Concrete and Steel and Shear Behavior of Shear Connectors of H-shaped Steel Encased Composite Columns (H형강 매입형 합성기둥의 부착강도 및 전단연결재의 전단거동)

  • Wang, Ning;Lee, Hye Lim;Lee, Myung Jae
    • Journal of Korean Society of Steel Construction
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    • v.29 no.5
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    • pp.377-387
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    • 2017
  • The objective of this study is to investigate the influence that how does contact surface between concrete and steel influence the steel encased composite column by push-out test. Also nominal bond stress indicated by design standard such as Eurocode 4 is underestimated in small scale steel encased composite column. The other objective of this study is to investigate how does the number and space of shear connector influence the H-shaped steel encased composite column. The shear behavior of shear connectors is investigated by push-out test.

The effect of resin cement type and cleaning method on the shear bond strength of resin cements for recementing restorations

  • Koodaryan, Roodabeh;Hafezeqoran, Ali;Maleki, Amin Khakpour
    • The Journal of Advanced Prosthodontics
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    • v.9 no.2
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    • pp.110-117
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    • 2017
  • PURPOSE. This laboratory study assessed the effect of different dentin cleaning procedures on shear bond strength of resin cements for recementing prosthesis. MATERIALS AND METHODS. A $4{\times}4$ flat surface was prepared on the labial surface of 52 maxillary central incisors. Metal frames ($4{\times}4{\times}1.5mm$) were cast with nickel-chromium alloy. All specimens were randomly divided into 2 groups to be cemented with either Panavia F2.0 (P) or RelyX Ultimate (U) cement. The initial shear bond strength was recorded by Universal Testing Machine at a crosshead speed of 0.5 mm/min. Debonded specimens were randomly allocated into 2 subgroups (n = 13) according to the dentin cleaning procedures for recementation. The residual cement on bonded dentin surfaces was eliminated with either pumice slurry (p) or tungsten carbide bur (c). The restorations were rebonded with the same cement and were subjected to shear test. Data failed the normality test (P < .05), thus were analyzed with Mann Whitney U-test, Wilcoxon signed rank test, and two-way ANOVA after logarithmic transformation (${\alpha}=.05$). RESULTS. The initial shear bond strength of group P was significantly higher than group U (P = .001). Pc and Uc groups presented higher bond strength after recementation compared to the initial bond strength. However, it was significant only in Pc group (P = .034). CONCLUSION. The specimens recemented with Panavia F2.0 provided higher bond strength than RelyX Ultimate cement. Moreover, a tungsten carbide bur was a more efficient method in removing the residual resin cement and increased the bond strength of Panavia F2.0 cement after recementation.

Effect of Shear Key and Edge Length of Near Surface-Mounted FRP Plate in Concrete (콘크리트에 표면매입 보강된 FRP판의 전단키 및 연단거리 효과)

  • Seo, Soo-Yeon
    • Journal of the Korea institute for structural maintenance and inspection
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    • v.20 no.1
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    • pp.41-47
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    • 2016
  • This paper presents a bond test to find the effect of shear key and edge length from the bonded FRP in near surface-mounted(NSM) retrofit using FRP plate. Main parameters in the test are the location and size of shear key and the edge length. For the test, 10 specimens were made by embedding FRP plate of $3.6mm{\times}16mm$ into $400mm{\times}200(300)mm{\times}400mm$ concrete block and fixing it by using epoxy. Tensile load was applied to the FRP of the specimens until failure and was recorded at each load increase. In addition, the bond slip and elongation of FRP were measured during the test. From the test, it was found that the further the shear key located from the loading, the higher strength we could get. The bond strength inversely depended on the size of shear key. Especially, when the size of shear key was to be lagger than certain size, the bond strength decreased to very low value; even less than that of the case without shear key. The bond strength somewhat increased corresponding to the increase of edge length from the bonded end of FRP to loading in spite of same bond length. The bond-slip between FRP and concrete governed overall deformation in the bond test of NSM FRP so that the effect of excessive slip is necessary to be considered in the design.

Evaluation of Characteristics of Tack Coat for Porous Pavement using Direct Shear Test (직접 전단 실험을 통한 배수성포장용 택코트 특성 평가)

  • Kim, Nak-Seok;Hong, Eun-Cheol;Jo, Shin-Haeng
    • Journal of the Korean Society of Hazard Mitigation
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    • v.9 no.1
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    • pp.27-32
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    • 2009
  • The main objective of this study is to develop a test for measuring the bond shear strength between pavement layers. The research is also conducted to evaluate tack coat materials and application rate in porous pavement. The experiment includes using two types of emulsions (RSC-4, Modified Emulsion) and a asphalt binder type (HM-1). HM-1 was developed to be applied in porous pavement. The bond shear strengths were measured by a direct shear type device under various test conditions. The shear strength may not be appropriate in the evaluation of the bond shear strength, while the toughness of the test may be useful. In case of the tack coat application rate in porous pavement, RSC-4 has to be used a minimum amount of $0.8l/m^2$ and modified emulsion asphalt has to be applied a volume of use $0.5{\sim}0.6l/m^2$. HM-1, asphalt cement type, is far stronger bond shear strength than emulsified asphalt tack coat and had showed the excellent trackless property.

Comparative study of the shear bond strength of various veneering materials on grade II commercially pure titanium

  • Lee, Eun-Young;Jun, Sul-Gi;Wright, Robert F.;Park, Eun-Jin
    • The Journal of Advanced Prosthodontics
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    • v.7 no.1
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    • pp.69-75
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    • 2015
  • PURPOSE. To compare the shear bond strength of various veneering materials to grade II commercially pure titanium (CP-Ti). MATERIALS AND METHODS. Thirty specimens of CP-Ti disc with 9 mm diameter and 10 mm height were divided into three experimental groups. Each group was bonded to heat-polymerized acrylic resin (Lucitone 199), porcelain (Triceram), and indirect composite (Sinfony) with 7 mm diameter and 2 mm height. For the control group (n=10), Lucitone 199 were applied on type IV gold alloy castings. All samples were thermocycled for 5000 cycles in $5-55^{\circ}C$ water. The maximum shear bond strength (MPa) was measured with a Universal Testing Machine. After the shear bond strength test, the failure mode was assessed with an optic microscope and a scanning electron microscope. Statistical analysis was carried out with a Kruskal-Wallis Test and Mann-Whitney Test. RESULTS. The mean shear bond strength and standard deviations for experimental groups were as follows: Ti-Lucitone 199 ($12.11{\pm}4.44$ MPa); Ti-Triceram ($11.09{\pm}1.66$ MPa); Ti-Sinfony ($4.32{\pm}0.64$ MPa). All of these experimental groups showed lower shear bond strength than the control group ($16.14{\pm}1.89$ MPa). However, there was no statistically significant difference between the Ti-Lucitone 199 group and the control group, and the Ti-Lucitone 199 group and the Ti-Triceram group. Most of the failure patterns in all experimental groups were adhesive failures. CONCLUSION. The shear bond strength of veneering materials such as heat-polymerized acrylic resin, porcelain, and indirect composite to CP-Ti was compatible to that of heatpolymerized acrylic resin to cast gold alloy.

THE EFFECT OF ETCHING TIME ON SHEAR BOND STRENGTH AND ADAPTIBILITY OF ONE-BOTTLE DENTIN ADHESIVE (One-bottle 상아질 접착제의 전단결합강도와 접착성에 관한 부식시간의 효과)

  • Park, Kwang-Soo;Park, Il-Yoon;Cho, Young-Gon
    • Restorative Dentistry and Endodontics
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    • v.24 no.1
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    • pp.240-250
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    • 1999
  • The purpose of this study was to evaluate the effect of different etching time on the shear bond strength and adaptibility of composite to enamel and dentin when used one-bottle adhesive Prime & Bond$^{TM}$ 2.0. The proximal and occlusal surfaces of 88 extracted human molars were ground to expose enamel(n=44) and dentin (=44) using diamond wheel saw. Teeth were randomly assigned to four test groups(n=11) and received the following treatments : Control group were conditioned with 36% phosphoric acid for 20 sec. according to the manufacturer's directions. Experimental 10 sec. group, 30 sec. group and 60 sec. group were conditioned with 36% phosphoric acid for 10 sec., 30 sec. and 60 sec., respectively. Teeth were rinsed and dried for 2 sec. Prime & Bond$^{TM}$ 2.0 were applied according to the manufacturer's directions and Spectrum$^{TM}$ TPH composite resins were bonded to enamel and dentin surfaces. All specimens were stored in distilled water for 24 hours. Eighty specimens were sheared in a Universal Testing Machine with a crosshead speed of 5mm/minute. One way ANOVA and LSD test were used for statistical analysis of the data. Failure modes of all specimens after shear bond strength test were examined and listed. Also, representive postfracture modes and eight specimens were examined under scanning electron microscope. The results of this study were as follows: 1. The shear bond strength to enamel was the highest value in 30 sec. group (20.68${\pm}$8.54MPa) and the lowest value in 10 sec. group (14.92${\pm}$6.07MPa), so there was significant difference of shear bond strength between two groups (p<0.05). But there was no significant difference among other groups (p>0.05). With longer etching time to enamel from 10 sec. to 30 sec., higher the shear bond strength was obtained, but the shear bond strength was decreased at 60 sec. etching time. 2. The shear bond strength to dentin was the highest value in control group (13.08${\pm}$6.25MPa) and the lowest value in 60 sec. group (9.47${\pm}$3.35MPa), but there was no significant difference among the all groups (p>0.05). The eching time over 20 sec. decreased the shear bond strength to dentin. 3. In SEM observation, the enamel and resin interfaces were showed close adaptation with no relation to etching time of enamel. And the dentin and resin interfaces were showed close adaptation at 20 sec. and 30 sec. etching time, but showed some gaps at 10 sec. and 60 sec. etching time. Accordingly, these results indicated that a appropriate etching time in Prime & Bond$^{TM}$ 2.0 was required to be 30 sec. in enamel and 20 sec. in dentin for the high shear bond strength and good adaptation between the composite resin and tooth substance.

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THE EFFECTS OF FLUORIDE RELEASING ORTHODONTIC SEALANT ON THE SHEAR BOND STRENGTH Of LIGHT-AND CHEMICAL-CURED ORTHODONTIC RESINS (불소가 유리되는 교정용 전색제가 광중합형 및 화학중합형 교정용 접착제의 전단결합강도에 미치는 영향)

  • Kim, Bong-Hyun;Yoon, Young-Jooh;Kim, Kwang-Won
    • The korean journal of orthodontics
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    • v.27 no.5 s.64
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    • pp.781-789
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    • 1997
  • The purpose of this study was to evaluate the effects of fluoride relasing orthodontic sealant on the shear bond strength of light-and chemical-cured orthodontic rosins, to compare the shear bond strenth with light-and chemical-cured orthodontic resins, and to identify the changes of shear bond strength by rebonding in vitro. The brackets were divided into eight groups. Each group of metal brackets had different bonding mechanisms with adhesives. Group A : Transbond only Group B : Mono-Lok 2 only Group C : Light cured FluoroBond+Transbond Group D : Light cured FluoroBond+Mono-Lok 2 Group E : Transbond only(rebonded) Group F : Nomo-Lok 2 only(rebonded) Group G : Light cured FluoroBond+Transbond(rebonded) Group H : Light cured FluoroBond+Mono-Lok 2(rebonded) 65 extracted human premolars were prepared for bonding and 65 metal brackets for each group were bonded to prepared enamel surfaces of buccal surfaces as the above prescription. 24 hours bonding after, the Instron universal testing machine was used to test the shear bond strength of metal brackets to enamel. After debonding, same kind of metal brackets for each group were rebonded to prepared enamel surfaces of buccal surfaces to test the shear bond strength at the rebonding to enamel. Statistical analysis of the data was carried out Student's t-test ANOVA test, and Scheffe test using $SPSS/PC^+$ The results were as follows : 1. The order of shear bond strength was Group B(11.84MPa), Group A(10.75MPa), Group, D(9.69MPa), and Group C(9.39MPa)in lst bonded groups. 2. The order of shear bond strength was Group E(7.40MPa), Group G(6.48MPa), Group F(5.89MPa), and Group H(5.15MPa) in rebonded groups. 3. The shear bond strength of chemical cured orthodontic rosins had higher than that of light-cured orthodontic resins in all groups, but there was no statistical significance between groups(P>0.05). 4. In rebonded groups, the shear bond strength of light cured orthodontic rosins had higher than that of chemical cured orthodontic resins, but there was no statistical significance between groups(P>0.05). 5. The shear bond strength of all rebonded groups progressively decreased than that of 1st bonded groups, and there was statistical significance between groups(p<0.05, p<0.001).

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