• Title/Summary/Keyword: Separation time

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Preparation and Characterization of Porous Glass in $Na_2O-B_2O_3-SiO_2$ System ; Addition Effects of $ZrO_2$ and MgO (분상법을 이용한 봉규산염계 다공질 유리의 제조 및 특성;$ZrO_2$와 MgO 첨가 영향)

  • 김영선;최세영
    • Journal of the Korean Ceramic Society
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    • v.32 no.3
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    • pp.385-393
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    • 1995
  • Akali-resistant porous glass was prepared by phase separation in Na2O-B2O3-SiO2 system containing ZrO2 and MgO. ZrO2 was added for alkali-resistance and MgO for anti-cracking during leaching. Optimal content of ZrO2 for alkali-resistance was 7wt% and devitrification by heat treatment resulted from further addition. Pore size and pore volume were decreased and specific surface area was increased with ZrO2 addition due to depression in phase separation. Addition of 3mol% MgO to mother glass containing 7wt% ZrO2 was effective for anti-crack during leaching. In this case, with phase separation at 55$0^{\circ}C$ and 5$25^{\circ}C$ for 20 hrs. crack-free porous glasses could be prepared. The relation between pore size r and heat treatment time t at 55$0^{\circ}C$ was D=25.58+18.16t. According to measurement of gas permeability, the mechanism of gas permeation was Knudsen flow. N2 and He permeability of porous glass which was prepared by heat treatment at 55$0^{\circ}C$ for 20 hrs. were 0.843$\times$10-7mol/$m^2$.s.Pa and 2.161$\times$10-7mol/$m^2$.s.Pa respectively.

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Non-Explosive Actuator Technology for Satellite Applications (인공위성용 비폭발식 분리장치 기술동향)

  • Lim, Jae-Hyuk;Kim, Kyung-Won;Kim, Sun-Won;Lee, Chang-Ho;Rhee, Ju-Hun;Hwang, Do-Soon
    • Current Industrial and Technological Trends in Aerospace
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    • v.7 no.1
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    • pp.97-104
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    • 2009
  • Successful separation of satellites from launch vehicles and release its appendages such as solar arrays and antennas are one of the most important tasks for mission accomplishment during in-orbit maneuver. Especially, specific release devices called NEA(Non-Explosive Actuator) have been widely adopted to perform safe separation and release due to its outstanding performance of low functional shock (below 500g), no contamination and easy handing as opposed to the pyroshock device. In the paper, various kinds of NEA and its history of development are reviewed along with a summary on the domestic research trend.

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Enantiomeric Separation of Methamphetamine Abused in Korea (우리나라에서 남용되는 메스암페타민의 거울상 이성질체분리)

  • Yoo, Young-Chan;Chung, Hee-Sun;Choi, Hwa-Kyung;Kim, Eun-Mi;Kim, Mi-Kyung;Kim, Sun-Choon
    • YAKHAK HOEJI
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    • v.41 no.3
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    • pp.277-282
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    • 1997
  • Methamphetamine, which is the most commonly abused drug in Korea, exists in terms of d-, l- isomers and a racemate(dl). d-Methamphetamine is a potent central nervous system stimulant, whereas l-Methamphetamine is sold freely as a nasal decongestant. In addition, methamphetamine appears in different ratios of optical isomers by the clandestine synthesis applied. In this study, enetiomeric separation of methamphetamines was estabilished to distinguish the chirality of methamphetamines trafficked and abused in Korea. A gas chromatograph/mass spectrometer(GC/MS) system equipped with an achiral capillary column is used to isolate the isomers of methamphetamine after (S)-N-(trifluoroacetyl)-l-prolyl(TFP) deravatization.After analyzing 10 illicit methamphetamine powders and 10 positive urine samples, following findings were found: d-Methamphetamine was well resolved from l-Methamphetamine by chromatographic separation of TFP derivatibes on DB-5 with retention time of 11.80 and 11.35 min respectively. The detection of d-Methamphetamine in all 10 powders and 10 urine samples proves that all methamphetamines abused in Korea are illegally manyfactured and administred.

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Non-explosive Separation Device Harnessing Spring Clamp and Shape Memory Alloy Wire (스프링 클램프와 형상기억합금 와이어를 이용한 비폭발식 분리장치)

  • Choi, Junwoo;Lee, Dongkyu;Hwang, Kukha;Lee, Minhyung;Kim, Byungkyu
    • Journal of Aerospace System Engineering
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    • v.9 no.2
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    • pp.7-12
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    • 2015
  • In this paper, we report a non-explosive separation device for a small satellite which utilize a shape memory alloy actuator and spring clamp. In order to increase the preload, the proposed device employs spring clamp that can generate high toque when the shape memory alloy actuator makes the cylinder key unlatch a holding ball effectively. Owing to simple design of separation device configuration, we could obtain good repeatability(up to 30 times activation). Conclusively, we could develop a non-explosive separation device which can reliably activate within 1.2 sec under high preload(up to 300kgf).

The Phase Separation of Low Alkali Borosilicate Glass by Substituting $Li_2O$ for $Na_2O$ (산화리튬의 치환에 따른 붕규산 유리의 분상에 관한 연구)

  • 양중식
    • Journal of the Korean Ceramic Society
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    • v.18 no.1
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    • pp.27-34
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    • 1981
  • The phase separation of low-alkali borosilicate glass with the composition of $6.25Na_2O$.$18.75B_2O_3$.$75.00SiO_2$(mole%) substituting $Li_2O$ for $Na_2O$ was studied. The phase separation in the temperature range of transformation was examined with various heating temperatures and soaking times. Durability to water, thermal expansion and specific density of the specimen were investigated and the microstructure of the separated phase was also observed by transmission electron micrograph techniques. The maximum alkali extraction result with the best phase separation effect was obtained when $Na_2O$ of the base glass was replaced with $1.88Li_2O$ (mole %) and electron micrograph of carbon film replica of $1.88Li_2O$$4.37Na_2O$.$18.75B_2O_3$.$75.00SiO_2$ (mole %) glass showed that the glass consisted of homogeneous two phases. The minimum specific density was shown with the specimen treated at 57$0^{\circ}C$ and it was also shown that the longer the treating time the lower the specific density. The apparent activation energies of approximately 45 kcal/mole by the alkali extraction and 43kcal/mole by the thermal expansion method were derived from the Arrhenius plots, respectively.

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Spinodal Phase Separation and Isothermal Crystallization Behavior in Blends of VDF/TrFE(75/25) Copolymer and Poly(1,4-butylene adipate) (I) -Spinodal Phase Separation Behavior-

  • Kim, Kap Jin;Kyu, Thein
    • Fibers and Polymers
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    • v.4 no.4
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    • pp.188-194
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    • 2003
  • Phase behavior and spinodal phase separation kinetics in binary blends of a random copolymer of vinylidene fluoride and trifluoroethylene (75/25) [P(VDF/TrFE)] and poly(l,4-butylene adipate) (PBA) have been investigated by means of optical microscopic observation and time-resolved light scattering. The blends exhibited a typical lower critical solution temperature (LCST)∼${34}^{\circ}C$ above the melting temperature of the P(VDF/TrFE) crystals over the entire blend composition range. P(VDF/TrFE) and PBA were totally miscible in the temperature gap between the melting point of P(VDF/TrFE) and the LCST. Temperature jump experiments of the 3/7 P(VDF/TrFE)/PBA blend were carried out on a light-scattering apparatus from a single-phase melt state (${180}^{\circ}C$) to a two-phase region (205∼${215}^{\circ}C$). Since the late stage of spinodal decomposition (SD) is prevalent in the 3/7 blend, SD was analyzed using a power law scheme. Self-similarity was preserved well in the late stage of SD in the 3/7 blend.

The PDS(Power Transfer Display Separation) method and implementation of SPIDER (Sustainer with Primary sided Integration of DC/DC converter and Energy Recovery circuit) for AC-PDP (AC-PDP를 위한 SPIDER(Sustainer with Primary sided Integration of DC/DC converter and Energy Recovery circuit)의 구현 및 PDS 구동법)

  • Shin, Yong-Saeng;Park, Jae-Sung;Hong, Sung-Soo;Han, Sang-Kyoo;Roh, Chung-Wook
    • The Transactions of the Korean Institute of Power Electronics
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    • v.17 no.2
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    • pp.107-113
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    • 2012
  • This paper proposes a PDS(Power Transfer Display separation) method for AC-PDP. The proposed PDS method can transfer power and perform an energy recovery by a power conversion circuit operates differently depending on the time. As a result, it uses less of components than conventional PDP power supply and sustain circuit use. Moreover, the manufacturing process can be streamlined. Therefore, the proposed method is suitable for low cost PDP module. To confirm the operation, validity and features of the proposed PDS method, experimental results from a prototype for 42-in diagonal PDP are presented.

Multiple Camera Collaboration Strategies for Dynamic Object Association

  • Cho, Shung-Han;Nam, Yun-Young;Hong, Sang-Jin
    • KSII Transactions on Internet and Information Systems (TIIS)
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    • v.4 no.6
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    • pp.1169-1193
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    • 2010
  • In this paper, we present and compare two different multiple camera collaboration strategies to reduce false association in finding the correspondence of objects. Collaboration matrices are defined with the required minimum separation for an effective collaboration because homographic lines for objects association are ineffective with the insufficient separation. The first strategy uses the collaboration matrices to select the best pair out of many cameras having the maximum separation to efficiently collaborate on the object association. The association information in selected cameras is propagated to unselected cameras by the global information constructed from the associated targets. While the first strategy requires the long operation time to achieve the high association rate due to the limited view by the best pair, it reduces the computational cost using homographic lines. The second strategy initiates the collaboration process of objects association for all the pairing cases of cameras regardless of the separation. In each collaboration process, only crossed targets by a transformed homographic line from the other collaborating camera generate homographic lines. While the repetitive association processes improve the association performance, the transformation processes of homographic lines increase exponentially. The proposed methods are evaluated with real video sequences and compared in terms of the computational cost and the association performance. The simulation results demonstrate that the proposed methods effectively reduce the false association rate as compared with basic pair-wise collaboration.

A Study on the Separation of Fetal ECG from a Single Channel Abdominal ECG (단일채널 복부 심전도를 통한 태아 심전도 분리)

  • Park Kwang-Li;Lee Kyoung-Joung;Lee Jeon
    • The Transactions of the Korean Institute of Electrical Engineers D
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    • v.54 no.3
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    • pp.198-205
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    • 2005
  • In this paper, we proposed a new algorithm for the separation of fetal ECG from single channel abdominal ECG. The algorithm consists of a stage of demixing vector calculation for initial signal and a stage of fetal beat detection for the rest of signal. The demixing vector was obtained by applying independent component analysis technique to projected signals into time-frequency domain. For the test of this algorithm, simulation signals, De Lathauwer's data and some measured data, which was acquired from 8 healthy volunteers whose pregnant periods ranged from 22 weeks to 35 weeks and whose ages from 27 to 37, were used. For each data, the accuracy of fetal beat detection was $100\%$ and with the location of fetal beats, fetal heart rate variability and morphology could be offered. In conclusion, this proposed algorithm showed the possibility of fetal beat separation with a single channel abdominal ECG and it might be adopted to a fetal health monitoring system, by which a single channel abdominal ECG is acquired.

Dehydration of Alcohol Solutions Through Crosslinked Chitosan Composite Membranes III. Effects of Substrate, Neutralization and Active Layer Thickness on Pervaporation of Water/Ethanol Mixture (가교키토산 복합막을 통한 알콜수용액의 탈수 III. 화학가교시 지지체, 중화에 의한 효과와 이온가교시 활성층두께 변화에 의한 효과)

  • 이영무;남상용;유제강;류경옥
    • Membrane Journal
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    • v.6 no.4
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    • pp.250-257
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    • 1996
  • Surface crosslinked chitosan composite membranes were prepared with glutaraldehyde and surfuric acid. Effects of neutralization for complex between chitosan and acetic acid and of water permeability for substrate membranes on pervaporation performance were investigated. For ionically crosskinked membranes, effect of active layer thickness on separation factor of water/ethanol mixture was studied. With increasing the water permeability of the substrate, the membrane showed an increased separation factor, while it maintained a constant permeate flux. Neutralized chitosan composite membranes revealed a decreased separation factor and a constant permeate flux. When the thickness of the active layer increased, an optimum crosslinking time to achieve higher separation factor shifted to a prolonged times.

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