• Resources Recycling
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• v.16 no.6
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• pp.34-38
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• 2007

For recycling of tantalum from obsolete condenser, physical separations and chlorination of tantalum scraps with $Cl_2$ and $CCl_4$ were investigated. The recovery ratio of tantalum from obsolete condenser was 98% by using a multidisciplinary process of crushing by stamp mill, wet gravity separation by the shaking table, and air classification. In the chlorination reaction of non-oxidized Ta anode with $Cl_2$, the highest weight loss ratio is at least 60%, while in the chlorination reaction of Ta anode with $CCl_4$, the reaction rate for the oxidized Ta anode is faster than that of the non-oxidized Ta anode.

• KSBB Journal
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• v.24 no.2
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• pp.212-215
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• 2009

In this study, the process parameters of liquid-liquid extraction were optimized to obtain a high purity and yield of paclitaxel in a pre-purification step. The optimal solvent ratio (methylene chloride/concentrated methanol extract ratio), extraction times, mixing time, and standing time for liquid-liquid extraction were 0.28 (v/v), 3(times), 30 min, and 40 min, respectively. The polar impurities from the biomass extraction were efficiently removed by liquid-liquid extraction. The complete concentration of liquid-liquid extract by rotary evaporator was reliable enough to obtain a high purity and yield of paclitaxel for subsequent purification steps.

• Proceedings of the Korean Society For Composite Materials Conference
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• 2000.11a
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• pp.265-270
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• 2000

Injection molding is a very important industrial process for the manufacturing of plastics objects. During an injection molding process of composites, the fiber-matrix separation and fiber orientation are caused by the flow of molten polymer/fiber mixture. As a result, the product tends to be nonhomogeneous and anisotropic. Hence, it is very important to clarify the relations between separation· orientation and injection molding conditions. So far, there is no research on the measurement of fiber orientation using image processing. In this study, the effects of fiber content ratio and molding condition on the fiber orientation-angle distributions are studied experimentally. Using the image processing method, the fiber orientation distribution of weld-line parts in injection-molded products is assessed. And the effects of fiber content and injection molding conditions on the fiber orientation functions are also discussed

• The Korean Journal of Nuclear Medicine
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• v.11 no.1
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• pp.9-15
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• 1977

Radioiodine labelled human follicle stimulating hormone has been prepared using chloramine-T, with the approximate labelling yield of 65%. The labelled product is purified by means of a starch gel electrophoresis, and a Sephadex gel filtration, and the separation efficiencies are assessed for the effective use in radioimmunoassay. The results indicate that the gel filtration is efficient in view of the separation time, simplicity and bindability of the labelled hormone to the antibody. In determining the ratio of the free to the antibody hound labelled hormone, a double antibody technique is applied in comparison with a chromatoelectrophoresis. The ratio could be obtained only in the case of applying the double antibody technique.

• Proceedings of the Korean Society of Propulsion Engineers Conference
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• 2008.03a
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• pp.168-172
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• 2008

Three different geometry shapes of the blade leading edge in a centrifugal compressor were investigated in this paper. Numerical simulation was done to analyze the effect of the leading edge shape on the performance of the centrifugal compressor. The result shows that compared to the blunt leading edge, the circular leading edge will raise the chocking mass flow. The pressure ratio and efficiency will increase obviously. Using elliptical leading edge will get a further improvement on the performance than circular leading edge. The analysis of the flow field shows that the leading edge often causes flow separation near the inlet; using circular leading edge and elliptical leading edge will reduce the separation. What's more, using circular and elliptical leading edge will also reduce the wake loss near the outlet of the impeller. In a centrifugal compressor, using circular or elliptical leading edge on the splitter will improve the pressure loading distribution of main blade near the position of the splitter leading, which will increase the pressure ratio.

• Membrane and Water Treatment
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• v.10 no.5
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• pp.353-360
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• 2019

ZSM-5 membrane was prepared on tubular macroporous ${\alpha}$-alumina support using a different synthesis route. The effects of organic template agent and Si/Al ratio of the synthesis gel on morphology, structure, and separation performance of the ZSM-5 membrane used for dehydration of isopropanol were investigated. High water perm-selectivity ZSM-5 membrane with a thickness of about $3.0{\mu}m$ and a low Si/Al ratio of 10.1 was successfully prepared from organotemplate-free synthesis gel with a molar composition of $SiO_2$ : $0.050Al_2O_3$ : $0.21Na_2O$ : NaF : $51.6H_2O$ at $175^{\circ}C$ for 24 h. The ZSM-5 membrane exhibited high pervaporation performance with a flux of $3.92kg/(m^2{\cdot}h)$ and corresponding separation factor of higher than 10,000 for dehydration of 90 wt.% isopropanol/water mixture at $75^{\circ}C$.

• Transactions of the Korean hydrogen and new energy society
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• v.33 no.5
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• pp.525-533
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• 2022

In this study, in order to numerically analyze the heat flow characteristics in the valve according to the opening rate for the solenoid valve for hydrogen supply applied to the hydrogen storage tank, flow characteristics were comparatively analyzed. Through the analysis of pressure and temperature distributions within the valve according to the high-pressure supply condition of 70 MPa or more, the heat flow characteristics in the valve, inlet and outlet passage according to the opening rate of the valve were identified. As a result a sudden change in the fluid behavior appears in the neck region of the valve, and it is understood that the flow separation caused by the flow path shape of the expanded tube has a dominant influence on the flow characteristics. And, it was confirmed that the shape of the valve seat is a factor significantly affecting the improvement of flow rate and differential pressure performance.

• Membrane Journal
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• v.24 no.2
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• pp.158-166
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• 2014

In this research, microporous and bicontinuous poly vinylidene fluoride(PVDF) hollow fiber membranes were prepared via hybrid process of the thermally induced phase separation (TIPS) and stretching method. The mechanism of the membrane preparation is based on liquid-liquid phase separation. The final membranes have characteristic structures which have both bicontinuous and fibrillar morphology by applying the stretching method. They showed quite different structure when compared with the spherulitic or nodular structure from S/L TIPS and bicontinuous structure from L/L TIPS. At first, PVDF hollow fiber precursors were prepared via TIPS method using various kind of diluent mixtures. We used gamma-butyrolacton, dimethyl phthalate (DMP), diethyl phthalate (DEP), dibutyl phthalate (DBP) as diluents. We could make hollow fiber membranes which had porous outer surface or dense outer surface by controling the parameters such as cooling conditions, PVDF concentration and the ratio of diluent mixtures. Finally, these hollow fiber were stretched at room temperature and diluents were extracted by ethanol. Effects of the stretching ratio on the membrane morphology were investigated using scanning electron microscope (SEM), and its effects on water flux, porosity, pore size, roughness and tensile strength were examined.

• KCI Concrete Journal
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• v.14 no.1
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• pp.51-60
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• 2002

Strengthening of existing concrete structures is a major concern in recent years as the number of degraded structures increases. The purpose of this paper is to investigate the static and fatigue behavior of reinforced concrete (RC) beams strengthened with steel plates. To this end, a comprehensive test program has been set up and many series of strengthened beams have been tested. The major test variables include the plate thickness, adhesive thickness, and the shear-span to depth ratio. The test results indicate that the separation of plates is the dominant failure mechanism even for the full-span-length strengthened beams with steel plate. The theoretical ultimate load capacities for strengthened beams based on the full composite action of concrete beam and steel plate are found to be larger than the actual measured load capacities. The strengthened beams exhibit more dominant shear cracking as the shear-span to depth ratio decreases. The ultimate capacity of strengthened beams increases slightly with the increase of adhesive thickness, which may be caused by the late initiation of plate separation in the beams with thicker adhesive. A realistic concept of ductility for plate-strengthened beams is proposed in this study. It is seen that the strengthened beams show relatively low ductility compared with unstrengthened beams. The present study indicates that the strengthened beams exhibit much higher fatigue resistance than the unstrengthened beams. The increase of deflections of strengthened beams according to the number of load cycles is much smaller than that of unstrengthened beams. The present study provides very useful results for the realistic application of plate-strengthening method in reinforced concrete structures.

• Journal of the Korean Society for Aeronautical & Space Sciences
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• v.37 no.1
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• pp.69-75
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• 2009

This paper studies the aerodynamic performance that the vent mixer-new conceptual supersonic mixer-showed with its geometric characteristics. The hole is 2 mm with 2 mm's distance from the wall in case 1 and with no distance in case 2. In case 3 die hole is 1 mm. Case 1 and case 2 showed the same total pressure recovery ratio, of which the case 3 was lower than that. While cases 1-3 had the same reattachment length, the shear layer was thicker in cases 1 and 2 than in case 3. Within the recirculation zone, cases 1 and 2 had lower pressure loss and higher velocity gradient difference than case 3-they enhance mixing between air and fuel. Separation bubble which is developed by the inflow into the recirculation zone has a significant effect on the total pressure recovery ratio in the combustor. Also separation bubble influences pressure distributions and recirculation flows in the recirculation zone. Therefore, inflow rate of air into the recirculation zone mainly affects the performance of vent mixer.