• Title/Summary/Keyword: Separation ratio

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Development of Analysis Method for Cholesterol in Infant Formula by Direct Saponification (직접 검화법을 이용한 조제분유의 콜레스테롤 분석법 개발)

  • Kim, Jin-Man;Park, Jung-Min;Yoon, Tae-Hyung;Leem, Dong-Gil;Yoon, Chang-Yong;Jeong, Ja-Young;Jeong, In-Seek;Kwak, Byung-Man;Ahn, Jang-Hyuk
    • Food Science of Animal Resources
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    • v.31 no.6
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    • pp.944-951
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    • 2011
  • An improved cholesterol analysis method was developed for powdered infant formula by gas chromatographic separation after liquid-liquid extraction and partition. In the official Korea Food Standard method for cholesterol analysis, the water phase and solvent phase were not well separated in the case of emulsified foods such as powdered infant formulas and baby foods. For the rapid and simple sample preparation method, an optimized direct saponification condition was established for heating temperature, heating time, and KOH concentration. From the results, the optimum conditions were as follows: heating temperature $90^{\circ}C$, heating time 60 min, and 16 M KOH 10 mL for a 2 g infant formula sample; improved separation condition for gas chromatography was as follows: the initial oven condition was $250^{\circ}C$ for 25 min, the oven temperature was increased to $290^{\circ}C$ by $10^{\circ}C$/min ratio, and finally the oven temperature remained at $290^{\circ}C$for 9 min. The developed method could be implemented for the study of cholesterol, providing the advantages of reduced inspection time and cost in emulsified foods such as infant formula.

Fundamental Studies on the Development of Axial-Flow Combine(I) -Evaluation of the Design Parameters of Grain-Straw Separator- (축류(軸流) 콤바인의 개발(開發)에 관(關)한 기초(基礎) 연구(硏究)(I) -조선별장치(粗選別裝置)의 설계변수(設計變數)의 평가(評價)-)

  • Lee, S.K.;Kim, S.T.;Choi, K.H.
    • Journal of Biosystems Engineering
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    • v.11 no.2
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    • pp.31-40
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    • 1986
  • Cylindrical and conical types of grain-straw separation equipment which has a stationary crimped sieve drum with rotating inner rotor were constructed. The developed equipments were tested to investigate the characteristics of separating performance under various mechanical conditions and crop conditions. As increase of the inclination of equipment and decrease of pitch of cover vane, the grain recovery was increased while straw rejection was decreased. The grain recovery and overall efficiency were decreased as the rotor speed and feeding velocity were increased for both varieties of rice, moisture contents, and test equipments. Conical prototype equipment performed higher straw rejection, lower grain recovery, and lower power requirement. However, separation performance of conical type equipment was more widely varied with various test conditions compared to cylindrical one. The performance of both equipments showed relatively insensitive to crop feedrate and crop properties, such as variety, moisture content, and grain-to-straw ratio.

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Hydrograph Separation and Flow Characteristic Analysis for Observed Rainfall Events during Flood Season in a Forested Headwater Stream (산지계류에 있어서 홍수기의 강우사상에 대한 유출수문곡선 분리 및 특성 분석)

  • Nam, Sooyoun;Chun, Kun-Woo;Lee, Jae Uk;Kang, Won Seok;Jang, Su-Jin
    • Korean Journal of Ecology and Environment
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    • v.54 no.1
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    • pp.49-60
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    • 2021
  • We examined the flow characteristics by direct runoff and base flow in a headwater stream during observed 59 rainfall events of flood season (June~September) from 2017 to 2020 yrs. Total precipitation ranged from 5.0 to 400.8 mm, total runoff ranged from 0.1 to 176.5 mm, and runoff ratio ranged from 0.1 to 242.9% during the rainfall events. From hydrograph separation, flow duration in base flow (139.3 days) was tended to be longer than direct runoff (78.3 days), while the contribution of direct runoff in total runoff (54.2%) was greater than base flow (45.8%). The total amount and peak flow of direct runoff and base flow had the highest correlation (p<0.05) with total precipitation and duration of rain among rainfall and soil moisture conditions. Dominant rainfall events for the total amount and peak flow of base flow were generated under 5.0~200.4 and 10.5~110.5 mm in total precipitation. However, when direct runoff occurred as dominant rainfall events, total amount and peak flow were increased by 267.4~400.8 and 169.0~400.8 mm in total precipitation. Therefore, the unique aspects of our study design permitted us to draw inferences about flow characteristic analysis with the contribution of base flow and/or direct runoff in the total runoff in a headwater stream. Furthermore, it will be useful for the long-term strategy of effective water management for integrated surface-groundwater in the forested headwater stream.

A Model Experiment Study to Secure the Straight Line Distance between the Air Inlet and Exhaust Section of the Living Room (거실제연설비중 공기유입구와 배출구간 직선거리 확보를 위한 모형실험연구)

  • Saeng-Gon Lee;Se-Hong Min
    • Journal of the Society of Disaster Information
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    • v.19 no.2
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    • pp.439-450
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    • 2023
  • Purpose: When conducting fire inspections in Korea, there are objects that violate the fire protection regulations that require a straight line distance of more than 5m between the air inlet and the discharge section if the floor area is less than 400m2, and this paper analyzes the reasons and conducts a model experimental study to support the need for related fire protection regulations. Method: Domestic firefighting objects were investigated and confirmed, domestic and foreign papers, policies, and laws and regulations were examined, and spaces with a straight line distance of less than 5m and more than 5m between the air inlet and discharge section were selected and analyzed through model experiments in a living room of less than 400m2 . Result: When examining the domestic fire protection regulations (NFPCNational Fire Perpormance Code), the separation distance between the air inlet and the outlet is more than 5m when the floor area is less than 400m2 , but as a result of the actual investigation, it was confirmed that there are firefighting objects that cannot keep the separation distance. In addition, when a paper review of overseas fire protection regulations for a straight line distance of more than 5m showed that there was no regulation on the straight line distance between the air inlet and the discharge section, the model experiment showed that the discharge speed was better when the straight line distance between the air inlet and the discharge section was more than 5m than when it was less than 5m. Conclusions: In this study, when examining overseas fire laws and regulations by comparing the performance of the fire protection ratio for the straight line distance between the air inlet and the exhaust section, there is no mandatory regulation for the straight line distance, but the domestic fire protection regulations (NFPCNational Fire Perpormance Code) require more than 5m. It is hoped that this will be reflected in the design stage in the future, and a foundation will be laid to reduce the responsibility and burden of fire superintendents.

Phenanthrene Uptake by Surfactant Sorbed on Activated Carbon (활성탄에 흡착된 계면활성제에 의한 Phenanthrene 흡착)

  • Ahn, Chi-Kyu;Woo, Seung-Han;Park, Jong-Moon
    • Journal of Soil and Groundwater Environment
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    • v.13 no.2
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    • pp.1-11
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    • 2008
  • Phenanthrene uptake by surfactant sorbed on activated carbon was investigated to recycle of surfactant in washed solution for contaminated soil. The partitioning of phenanthrene to the activated carbon coating with Triton X-100 as a surfactant was also evaluated by a mathematical model. Phenanthrene-contaminated soil (200 mg/kg) was washed in 10 g/L of surfactant solution. Washed phenanthrene in solution was separated by various particle loadings of granular activated carbon through a mode of selective adsorption. Removal of phenanthrene was 99.3%, and surfactant recovery was 88.9% by 2.5 g/L of granular activated carbon, respectively. Phenanthrene uptake by activated carbon was greater than that of phenanthrene calculated by a standard model for a system with one partitioning component. This is accounted for enhanced surface solubilization by hemi-micelles adsorbed onto granular activated carbon. The effectiveness factor is greater than 1 and molar ratio of solubilization to sorbed surfactant is higher than that of liquid surfactant. Results suggest that separation of contaminants and surfactants by activated carbon through washing process in soil is much effective than that of calculated in a theoretical model.

Identification of Proteins in Egg White Using Ion Exchange Cartridge and RP-HPLC (이온교환 카트리지와 RP-HPLC를 이용한 난백 단백질의 확인)

  • Kim, Hyun Moon;Kim, Ah Reum;Lee, Chang Soo;Kim, In Ho
    • Korean Chemical Engineering Research
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    • v.50 no.4
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    • pp.713-717
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    • 2012
  • Approximately forty proteins in egg white have been widely studied for their functional properties. To develop a procedure of separation for pure and non-altered proteins from egg white, purification study was conducted to isolate lysozyme, ovotransferrin, and ovalbumin. Ion exchange cartridge can selectively separate proteins from egg white, and reversed-phase HPLC (RP-HPLC) could identify separated proteins. Proteins in egg white were purified by HI trap ion exchange cartridge SP and Q with buffers pH 8.0 and 5.2. C18 column (Phenomenex, USA) was used for RP-HPLC analysis and isocratic mobile phase was used with acetonitrile (ACN)/distilled water (DW)/trifluoroacetic acid (TFA) in the ratio of 50/50/0.1. Comparing the retention times of standards in RP-HPLC experiments showed that ovotransferrin, ovalbumin, and lysozyme in egg white were eluted successively in the RP-HPLC column after the pretreatment in SP and Q ion exchange cartridges.

Immobilization and Recycling of Arsenic-Contaminated Fine Soil Cake Produced after Soil Washing Process (토양세척 후 발생하는 비소오염 탈수미세토의 불용화 및 재활용 평가)

  • Oh, Minah;Moon, SoYoung;Hyun, Min;Chae, HeeHoon;Lee, Jai-Young
    • Journal of the Korean Geosynthetics Society
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    • v.11 no.4
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    • pp.9-16
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    • 2012
  • Standardized remediation process for the soil contaminated with arsenic is insufficient due to characteristics of its anion-mobility and speciation changed by Eh-pH of soil. One of the well-known efficient remediation processes is the modified soil washing that particle separation process by only water. However, it is required that the treatment plan for the fine soil what was discharged after modified soil washing. Therefore, this research suggests the treatment plan that the recycling method using arsenic immobilization by FeS-$H_2O_2$. The batch experiments results for the arsenic immobilization showed that the water content was at least 50%, the injection of FeS and $H_2O_2$ (assay-35%) were 8% (w/watdrybase) and 0.2 mL/10 g of fine soil respectively. Arsenic concentration with KSLT was decreased about 95.4%. The results indicated that the mixing of FeS-$H_2O_2$ was highly efficient on the immobilization of As-contaminated soil. The mixing ratio as 13% of bentonite with 3% of cement (at based on 100% of immobilized fine soil) was satisfied with standard of liner for landfill construction.

Characterization of Ethanol Fermentation with Wild Type Yeast Strains (야생 효모 종류에 따른 알코올 발효 특성)

  • Baek, Seong Yeol;Lee, You Jung;Kim, Myoung-Dong;Yi, Jae-Hyoung;Mun, Ji-Young;Yeo, Soo-Hwan
    • Microbiology and Biotechnology Letters
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    • v.43 no.3
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    • pp.227-235
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    • 2015
  • The objective of this study was to improve the quality of Korean rice wine with wild type yeast strains isolated from various traditional Korean fermented foods. Herein the fermentation and sensory characterization of wild yeast, for the purposes of brewing Korean rice wine, was investigated. 12 yeast strains were examined for their ethanol and glucose tolerance. In addition, the pH, soluble solids, acidity, amino acidity, ethanol content, organic acids, and volatile compounds were also studied for the alcoholic beverages made with the wild yeasts. Almost all Saccharomyces genera yeasts were showed to have a tolerance at 10% ethanol, but non-Saccharomyces genera yeasts displayed a low tolerance. The alcoholic beverages fermented by non-Saccharomyces yeasts demonstrated higher levels of soluble solids, titratable acidity, amino acids, and lower ethanol content, when compared with the alcoholic beverages fermented by Saccharomyces genera yeasts. The organic acid content, such as malic acid, acetic acid, and succinic acid, was seen to also be higher. The electronic nose was analyzed, and discriminant function analysis (DFA) was used for discriminating wild yeast strains. The DFA plots indicated a significant separation of Saccharomyces genera and non-Saccharomyces yeast strains. For volatile compounds, ethyl acetate from non-Saccharomyces yeasts, and ethanol from Saccharomyces genera yeast, a high area ratio was observed.

Characterization of Heavy Metal-enriched Particles from Contaminated Soils in a Military Shooting Range (군사격장 오염토양 내 고농도 중금속함유 입자의 기초특성연구)

  • Kim, Jeeeun;Kim, Jeongjin;Bae, Bumhan;Kim, Younghun
    • Journal of the Korean GEO-environmental Society
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    • v.14 no.11
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    • pp.25-31
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    • 2013
  • Civil and military firing ranges are usually contaminated with heavy metals such as lead and copper and remediation is required. Acid washing and extraction are common remediation methods. Lead contaminated firing range soil samples were collected and a preliminary study was conducted to evaluate the characteristics of the contamination and the contribution of high specific gravity particles. Ethylenediamine tetra acetic acid(EDTA) extraction was applied for the removal of heavy metal but the extraction was not feasible for the firing range soil. Even after the repeated EDTA extraction, the contamination were still over the Korean environmental standard indicating that soil particles highly contaminated with heavy metal which release the heavy metal ion even after the repeated extraction. Some colored and higher specific gravity particles were separated from the soil samples and analyzed. The colored particles have specific gravity of 2.5-6.6. The saturation ratio of Pb and EDTA was 4.9-32%. After removal of these colored particles, the sandy soil showed moderate contamination which can be treated with soil washing. This was proved with the five-level sequential extraction and TCLP tests.

Analysis on the Causes of the Oil Leakage Phenomenon for Complex Waterproofing Methods of Asphalt Mastic and Modified Asphalt Sheet (콘크리트 구조물에 사용되는 개량아스팔트 시트와 아스팔트 매스틱을 복합화한 방수공법의 누유현상 원인 분석)

  • Park, Jin-Sang;Kim, Dong-Bum;Park, Wan-Goo;Oh, Sang-Keun
    • Journal of the Korea Institute of Building Construction
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    • v.18 no.4
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    • pp.337-345
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    • 2018
  • In this study, observations of oil leakage samples taken from the actual site were performed to identify the causes of the oil leakage phenomenon. As a result, the separation of the material components was determined as the main cause of the oil leakage phenomenon based on the changes in the surface conditions, and verification of this was conducted. The evaluation results confirmed that the filler component of the asphalt mastic subsided with the lapse of the settling time, and that the difference ratio of the filler contents of the upper and lower specimens was up to 23.8% after day 28. Based on these results, a hypothesis on the oil leakage mechanism of asphalt mastic was established, and then modeling of the entire process of oil leakage was performed.