• Bulletin of the Korean Chemical Society
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• 제35권12호
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• pp.3465-3474
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• 2014

Porous silica particles are the most prevailing raw material for stationary phases of liquid chromatography. During a long period of time, various methodologies for production of porous silica particles have been proposed, such as crashing and sieving of xerogel, traditional dry or wet process preparation of conventional spherical particles, preparation of hierarchical mesoporous particles by template-mediated pore formation, repeated formation of a thin layer of porous silica upon nonporous silica core (core-shell particles), and formation of specific silica monolith followed by grinding and calcination. Recent developments and applications of useful porous silica particles will be covered in this review. Discussion on sub-$3{\mu}m$ silica particles including nonporous silica particles, carbon or metal oxide clad silica particles, and molecularly imprinted silica particles, will also be included. Next, the individual preparation methods and their feasibilities will be collectively and critically compared and evaluated, being followed by conclusive remarks and future perspectives.

• 대한기계학회논문집
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• 제15권1호
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• pp.285-291
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• 1991

본 연구에서는 800 1pm인 대유량을 처리하고 공기중 1.8~4.5$\mu\textrm{m}$ 입자를 효율 적으로 선별하여 농축시키는 슬릿형 2단 가상충돌기를 설계 제작하고 그 성능이 평가 되었다. 즉, 첫째단과 둘째단에서 4.5$\mu\textrm{m}$과 1.8$\mu\textrm{m}$이 각각 50%의 효율로 분리되도록 설계되었다. 즉, 첫째단과 둘째단에서 4.5$\mu\textrm{m}$과 1.8$\mu\textrm{m}$이 각각 50%의 효율로 분리되도 록 설계한다. 설계인자(design parameter)들을 결정하기 위하여 먼저 슬릿형 노즐의 1단 가상충돌기의 분리효율(separation efficiency)에 대한 실험을 통하여 50% 커트오 프 Stokes수를 구하고, 이를 기초로 하여 2단 가상 충돌기의 주요치수와 작동조건을 결정하였다.

• 한국재료학회:학술대회논문집
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• 한국재료학회 2011년도 춘계학술발표대회
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• pp.8.2-8.2
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• 2011

This talk demonstrates diverse patterned structures utilizing in-situ self-organization and phase separation of the materials into an ordered fashion. The patterned structures in this talk include electrospun nanofibers and electrosprayed microparticles embedding small particles. The positions of the small particles are in-situ controlled during the electrohydrodynamic process by the interaction with the polymer matrix. Another topic of the talk includes selective deposition of spin-coated materials on a corrugated surface that was prepared by buckling of polymer thin films. Solution are strong tendency to be positioned in the trench area of the surface, which facilitates the fabrication of micropatterns of diverse materials.

• 한국세라믹학회지
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• 제11권1호
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• pp.23-28
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• 1974

1. Stage crushing by jaw crusher, steel mortar, and ball mill in turn has shown an inclination to increase the distribution of andalusite in coarse particles as well as to increase that of micas in fine particles. 2. Water elutriation was effective for the removal of muscovite and magnetic separation was effective for that of Mg-Fe micas such as biotte and chlorite. The process of concentration and that of purification are diagramatized respectively as follows: Concentration; Raw andalusite${\lightarrow}$Crushing${\lightarrow}$Screening${\lightarrow}$Water elutriation${\lightarrow}$Magnetic separation Purification; Concentrated andalusite${\lightarrow}$Calcination${\lightarrow}$Ball milling${\lightarrow}$Screening${\lightarrow}$Water elutriation${\lightarrow}$Magnetic separation${\lightarrow}$Acid washing.

• 대한기계학회:학술대회논문집
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• 대한기계학회 2008년도 추계학술대회A
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• pp.1683-1684
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• 2008

For direct detection of microbes in air, samples have to be collected but environmental particles such as dust are also trapped in such samples. Therefore the isolation of target bacteria from non-biological materials of similar size is of great importance in the identification of such organisms. Dielectrophoresis is an emerging technique that can rapidly separate cells in microfluidics. In this paper we proposed a new method for the separation of airborne microbes using condensation and dielectrophoresis. This system could be used as a continuous flow through separation system for various particles and utilized as a pretreatment technique for microbe detection.

• 분석과학
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• 제22권1호
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• pp.75-81
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• 2009

흐름 장-흐름 분획법을 개선한 방식의 흐름 장-흐름 분획장치를 이용하여 아주 적은 농도의 입자를 포함하는 지하수의 실험이 가능하였다. 또한 침강 장-흐름 분획법을 조합하여 상대적으로 크기가 큰 입자들을 분리함으로써 보다 넓은 영역의 입자들을 분리 및 분석할 수 있었다. 이렇게 장-흐름 분획법을 이용한 환경적인 측면의 연구의 가능성을 확인하였다. 각 시료의 크기 별 분포를 비교하고 크기별 분리를 확인하고자 광학 현미경을 사용하였다. 실험의 결과들은 입자크기분포를 결정하기 위한 가능성을 보여주었다. 다양한 분석 기술들의 조합으로 인해 그 효율성이 매우 증대할 수 있다는 것을 확인하였다. 또한, 본 연구를 통하여 입자 크기별 분리를 위한 장-흐름 분획법의 응용 가능성을 충분히 확인할 수 있었다. 앞으로 더욱 세밀한 실험과 시스템의 최적화에 노력을 기울인다면 흐름 장-흐름 분획법의 여러 부수 기술들을 조합하여 자연수 내의 입자들을 분리하고 분석할 수 있는 표준분석방법을 개발하고 제시할 수 있을 것으로 기대된다.

• Bulletin of the Korean Chemical Society
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• 제31권10호
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• pp.2943-2948
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• 2010

Silica monolith powders were prepared by a new procedure where ground powders of proper size distribution were obtained without sieving. An initiator was attached to this ground monolith and polystyrene was bound by reversible addition-fragmentation chain transfer polymerization to give a new stationary phase. The separation efficiency of this phase was found better than that of the polystyrene bound phase based on conventional silica particles and that of the C18 bound silica monolith powders.

• 센서학회지
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• 제19권2호
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• pp.112-117
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• 2010

A high-throughput sorting (HTS) system has been designed to separate target particles using a negative dielectrophoretic (n-DEP) force. The system consists of a meso-sized channel and a cantilever-type electrode(CE) array designed to separate a large number of target particles by discerning subtle difference of weight and dielectric material property of the particles. Using the polystyrene beads with various sizes of 10, 25 and $50{\mu}m$, the developed system exhibits high-throughput sorting of about 200 beads/sec and more than 80 % of separation efficiency.

• 한국환경복원기술학회지
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• 제5권3호
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• pp.1-8
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• 2002

Clayey paddy soils should be mixed with other good coarse soils to be used as a material for the lining, or, embankment. However, it has been difficult to separate soil particles from each other because of the internal cohesion in the soil gradation(separation) characteristics of the fine soil were investigated by various laboratory tests including the slaking durability test. Degradation rate of the soil were dependent upon the clay content and the initial water content before the submergence. The amount of degradations decreased as initial water content increased with exponential functions. The dried specimens separated into the particles after 24 hours of the submergence and specimens which water contents were less than 10% also separated into the particles after 2, or 3 days of the submergence. Compaction curves and the unconfined strength were not varied before and after the submergence. However, unconfined strength decreased as water content increased.

• Korean Chemical Engineering Research
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• 제55권1호
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• pp.130-134
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• 2017

Organic aerosols dispersed in the atmosphere likely undergo phase separation. Such internally mixed particles are often described as comprising an organic phase and an aqueous phase separately. We studied the morphology of two liquid separated aerosols in the sub-microscale by using a simple thermodynamic model with Russian doll geometry. The morphology of particles can be easily predicted from the simple criteria on the surface tension and two algebraic equations (the volume constraint and Young equation). This result may give the potential explanation about the complex morphology of the organic airborne particles.