• Tribology and Lubricants
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• 제23권5호
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• pp.195-200
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• 2007

This paper presents the friction induced scuffing and wear defects analysis of a pin bushing bearing based on the chemical composition using a scanning microscopy (SEM) and an energy dispersive X-ray analyzer (EDX). The SEM/EDX system, which may provide good information on the surface thermal defects and chemical compositions, provides impurities such as an aluminum, a silicon, a ferrous component and an oxygen, especially. The EDX measured results show that the oxygen may reduce the strength and a hardness of a pin busing, which may lead to a scuffing and a seizure on the rubbing contact surface. The current technology fabricated by a sintering for a pin bushing bearing should be modified or changed to reduce the oxygen composition and the impurities in pin bushing materials.

• 한국표면공학회지
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• 제37권3호
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• pp.137-145
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• 2004

This study surveys the microscopic wear of CVD TiN coatings in repeated sliding, using the SEM Tribosystem as in-situ system. According to the research, the depth of wear groove and the specific wear amount are changed by the transition of the microscopic wear mode. This investigation leads to the fact that the change of wear characteristics produces the transition of the wear mode. In this survey, four modes are observed for CVD TiN coatings with the thickness of 1.6$\mu\textrm{m}$: ploughing, powder formation, flake formation and coating delimitation. The microscopic wear properties is quantitatively evaluated in terms with the microscopic wear mode and the specific wear amount. These relationships prove that the observation of wear modes with a SEM Tribosystem is useful to evaluate wear properties.

• 대한인간공학회지
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• 제20권3호
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• pp.47-60
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• 2001

The purpose of this paper is propose an analytical method for evaluating user satisfaction of Internet website and identifying casual relationships between user satisfaction of Internet website and performance measures as like revisit intention and complaints using the structural equation model (SEM). This paper is intended to identify critical evaluation factors of user satisfaction for Internet website to determine criteria for evaluating the website. and use the criteria to develop a SEM model for quantitatively evaluation of each factors effects of user preference. The SEM model used 5 latent variables for the evaluation factors of website user satisfaction and 2 latent variables for performance evaluation. 2 portal sites were evaluated to construct the SEM model. and 74 subjects participated the website evaluation using the walk-through and face-to face survey method. Analysis results showed that the SEM model was statistically significant for all the 2 websites evaluated.

• KSBB Journal
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• 제16권3호
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• pp.295-301
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• 2001

Thiobacillus ferrooxid,$\alpha$ns와 pyrite 광석을 연마하여 resin에 고정한 시편을 대상으로 침출 시간에 따른 표면의 특성 변화를 EPMA 및 SEM-EDS를 이용하여 이미지와 원소구성비율에 따라 살펴보았다. 침출이 진행됨에 따라 표면의 철성분은 전체적으로 증가한 반면 원소황은 감소하는 경향을 나타냈다. 고배율에 익한 SEM 이미지에서 침출이 진행됨에 따라 도덧모양의 생성물이 침출 13일 경과 시점에 서 나타나 23일 경과 후까지 자라났으나 30일 경과 시점 에서는 표면전체에 새로운 층 생성된 결과로 나타났다. SEM 이미지 상에서 spot과 배경 지접의 원소 구성비를 EDS에 의하여 분석한 후 비교한 결과 초기에는 원소 구성비의 차이가 큰 값을 보이나 침출이 증가함에 따라 좌이가 나 지 않으며 이는 칩풀이 진행됨에 따라 pyrite 표면변이 접차 생성불이 칩착 되는 것으로 볼 수 있었다.

• 대한인간공학회지
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• 제22권2호
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• pp.45-56
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• 2003

The purpose of this study is to develop the model including multiple causal relationship between factors to evaluate overall user satisfaction and develop an objective method to quantify the impacts and scores of each qualitative factors on overall user satisfaction using Structural Equation Model(SEM) and also test the feasibility to construct a comprehensive website evaluation model including qualitative and quantitative factors. The SEM model used 2 qualitative factors of usability and esthetic factors for the evaluation factors of user satisfaction and select 4 attributes of each factors using factor analysis. 3 shopping mall sites were evaluated to construct the SEM model, and 155 subjects participated the website evaluation using the walk-through and face-to-face survey method. Analysis results showed that the SEM model was statistically significant for all the 3 websites evaluated. Both the usability and esthetic factors showed significant effects to user satisfaction of websites and have positive correlation. The user satisfaction was more effected by the usability factor than esthetic factors, and the simplification and harmonization were the most critical attributes of the usability and esthetic factors.

• 한국진공학회:학술대회논문집
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• 한국진공학회 2014년도 제46회 동계 정기학술대회 초록집
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• pp.107.2-107.2
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• 2014

다양한 산업분야에서의 급격한 Packing Density 증가 추세로 인하여 영상분석기기 분야도 기술적으로 매우 진보되어왔다. 특히 전자현미경(SEM : Scanning Electron Microscope)은 반도체, 디스플레이 및 부품 소재의 고집적화와 더불어 기술의 발전 속도가 빠르게 이루어지고 있으며, 매우 고도화 되고 있다. 이에 따른 다양한 응용분야에서 전자현미경의 수요도 꾸준히 증가되고 있는 추세이다. 그러나 기초 과학기술을 기반으로 하는 전자현미경 산업분야는 높아진 국내 수요대비 자체 기술 발전이 미약한 실정이다. 이러한 현실속에서 국내 기술력으로 FE-SEM을 개발하였고 상용화를 눈앞에 두고 있다. 국산화된 FE-SEM은 Outer Lens방식으로 Schottky cathode와 60o conical Lens를 적용하여 고분해능을 구현함과 동시에 Scan generator, Auto-stepping및 Retarding 기능들도 추가 장착하여 제품경쟁력을 극대화 하고자 하였다. 본 발표는 개발된 FE-SEM의 기술적 특징과 개발 과정 및 결과를 소개하고자 하였다. 또한 해외 경쟁사들의 선행 기술동향 대비 현재 국내 기술 수준을 비교하여 향후 나아갈 방향을 고찰하고자 하였으며, 이를 기반으로 진행 중에 있는 초 저-가속전압 및 Semi In-Lens Optic구현을 위한 국내 기술개발 추진 현황도 간략하게 논하고자 한다. 이러한 고찰을 통하여 해외 선진 경쟁사 대비 후 발업체로써 낙후되어있는 국내기술의 격차를 빠르게 좁혀 나아가고 Global 경쟁력을 갖춘 제품을 구현하기 위하여 국내 전문가들과의 협력을 통한 선행 요소기술 및 차별화된 제품기술 확보 방법을 강구하고자 한다.

• Journal of the korean society of oceanography
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• 제39권4호
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• pp.243-250
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• 2004

Sediment microcosm experiments were conducted for 14 and 28 days using Zn spiked sediment to examine the changing distribution of bioavailab1e sediment-bound Zn at different SEM (simultaneously extracted metal)-Zn/ AVS (acid volatile sulfide) mole ratios as a function of time and amphipod density. In surficial sediments (0-1cm), AVS concentrations significantly decreased due to bioturbation and oxidation, while SEM-Zn concentrations remained unchanged. As a result, SEM-Zn/AVS ratios in the surface sediment were greater one although the ratios were designed as less than one initially. With increasing SEM-Zn/AVS ratios in surficial sediments, concentrations of potentially bioavailable $MgCl_2$extractable-Zn, NaOAc extractable-Zn and pore water-Zn significantly increased, while concentrations of SEM-Zn were not significantly varied. Results suggested that as AVS concentrations decreased, AVS bound Zn was partitioned to other sediment fractions (i.e. $MgCl_2$ and NaOAc extractable) and the pore water, resulting in changes in Zn bioavailability in surficial sediments. Concentrations of AVS, SEM-Zn and pore water-Zn remained unchanged in the deeper layers (>1 cm) of the sediment.

• 한국수소및신에너지학회논문집
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• 제16권3호
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• pp.238-243
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• 2005

Mg and Mg-based alloys are most important hydrogen storage materials. It is a lightweight and low-cost materials with high hydrogen storage capacity. However, the formation of hydride at high temperature, the deterioration effect, the hydriding and dehydriding kinetics are bad factor for application. In this study, Mg and Ni have been produced by hydrogen induced mechanical alloying(HIMA) process. The raw materials, Mg(purity 99.9%) chip and Ni(purity 99.95%) chip was prepared by using a planetary ball mill apparatus(FRITSCH pulverisette 5). The balls to chips mass ratio(BCR) are 30:1. The hydrogen pressure induced 2.0MPa and milling times were 12, 24, 48, 72, 96 hours with a rotating speed of 200rpm. X-ray diffraction(XRD) analysis was made to characterize the crystallite size and misfit strain. The crystallite size measured by laser particle size analysis(PSA). Microstructure changes were investigated by scanning electron microscopy(SEM) and the transmission electron microscopy(TEM). The hydrogen storage properties were evaluated by using an Sivert's type automatic pressure-composition-therm(PCT) apparatus.

• Applied Microscopy
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• 제42권2호
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• pp.111-114
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• 2012

The scanning electron microscopy is an ideal technique for examining plant surface at high resolution. Most hydrate samples, however, must be fix and dehydrate for observation in the scanning electron microscope. Because the microscopes operate under high vacuum, most specimens, especially biological samples, cannot withstand water removal by the vacuum system without morphological distortion. Cryo-techniques can observe in their original morphology and structure without various artifacts from conventional sample preparation. Rapid cooling is the method of choice for preparing plant samples for scanning electron microscopy in a defined physiological state. As one of cryo-technique, high-pressure freezing allows for fixation of native non-pretreated samples up to $200{\mu}M$ thick and 2 mm wide with minimal or no ice crystal damage for the freezing procedure. In this study, we could design to optimize structural preservation and imaging by comparing cryo-SEM and convention SEM preparation, and observe a fine, well preserved Arabidopsis stem's inner ultrastructure using HPF and cryo-SEM. These results would suggest a useful method of cryo-preparation and cryo-SEM for plant tissues, especially intratubule and vacuole rich structure.

• 대한화학회지
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• 제54권5호
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• pp.551-555
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• 2010

Cinnamomum Iners (Darchini, 쟈 바 계피), Elettaria Cardamomum (Elachi, 백두구, 소두구, 카다몬, 카도몬), Punica Granatum (Anar Dana, 석류), Curcuma Longa (Haldi, 터메릭, 투메릭, 심황, 울금, 울금은, 컬쿠마), Piper Nigrum (Kali Mirch, 페퍼, 페퍼블랙, 후추, 블랙 페퍼), Syzygium aromaticum (Loung, 클로브, 정향, 정향나무,), Capsicum Annum (Laal Mirch, 붉은 고추), Mentha Arvensis (Pahari Podina, 박하), Curcuma Zedoaria (Kachur, 가쥬츠, 봉출, 아출, 커큐머 제도) Zingiber officinale (Adrak, 건강, 생강, 진저) 그리고 Garam Masala (매운맛, 혼합물)은 SEM-EDS와 ICP-AES의 도움으로 그 속의 금속 성분을 위해 본 연구에서 분석되어졌다. 작은 농도는 ICP-AES로 찾아냈고 주된 농도는 SEM-EDS로 찾아냈다.