• Title/Summary/Keyword: Selective recovery

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Quantitative Evaluation of Optimized Fat-Suppression Techniques for T1 Weighted Cervical Spine MR Imaging: Comparison of TSE-CHESS and TSE-SPAIR (T1 강조 경추자기공명영상에 대한 최적의 지방소거기법의 정량적 평가: TSE-CHESS 과 TSE-SPAIR 의 비교)

  • Goo, Eun-Hoe
    • Journal of Digital Convergence
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    • v.11 no.11
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    • pp.529-536
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    • 2013
  • The purpose of this study is to know clinical usefulness for fat suppression of the body curved portion compared with TSE-CHESS and TSE-SPAIR technique. A total of 25 normal volunteers without cervical spine disease were studied on a 3.0 T MRI scanner. As a quantitative analysis, PSNRs and CNRs were evaluated by using two methods for fat suppression of the body curved portion. As a results, PSNRs and CNRs for fat suppression were significantly greater for the TSE-SPAIR technique compared to TSE-CHESS technique. In conclusion, this study showed that a TSE-SPAIR technique has improved PSNRs and CNRs for evaluating of fat suppression in the body curved portion. These conclusions in the future will be provided information in diagnosis of fat suppression for the body curved portion.

A Study on Optimization of Nitric Acid Leaching and Roasting Process for Selective Lithium Leaching of Spent Batreries Cell Powder (폐 배터리 셀 분말의 선택적 리튬 침출을 위한 질산염화 공정 최적화 연구)

  • Jung, Yeon Jae;Park, Sung Cheol;Kim, Yong Hwan;Yoo, Bong Young;Lee, Man Seung;Son, Seong Ho
    • Resources Recycling
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    • v.30 no.6
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    • pp.43-52
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    • 2021
  • In this study, the optimal nitration process for selective lithium leaching from powder of a spent battery cell (LiNixCoyMnzO2, LiCoO2) was studied using Taguchi method. The nitration process is a method of selective lithium leaching that involves converting non-lithium nitric compounds into oxides via nitric acid leaching and roasting. The influence of pretreatment temperature, nitric acid concentration, amount of nitric acid, and roasting temperature were evaluated. The signal-to-noise ratio and analysis of variance of the results were determined using L16(44) orthogonal arrays. The findings indicated that the roasting temperature followed by the nitric acid concentration, pretreatment temperature, and amount of nitric acid used had the greatest impact on the lithium leaching ratio. Following detailed experiments, the optimal conditions were found to be 10 h of pretreatment at 700℃ with 2 ml/g of 10 M nitric acid leaching followed by 10 h of roasting at 275℃. Under these conditions, the overall recovery of lithium exceeded 80%. X-ray diffraction (XRD) analysis of the leaching residue in deionized water after roasting of lithium nitrate and other nitrate compounds was performed. This was done to determine the cause of rapid decrease in lithium leaching rate above a roasting temperature of 400℃. The results confirmed that lithium manganese oxide was formed from lithium nitrate and manganese nitrate at these temperatures, and that it did not leach in deionized water. XRD analysis was also used to confirm the recovery of pure LiNO3 from the solution that was leached during the nitration process. This was carried out by evaporating and concentrating the leached solution through solid-liquid separation.

Process Evaluation of Soil Washing Including Surfactant Recovery by Mathematical Simulation (계면활성제 재사용을 포함한 토양 세척 공정의 전산모사 평가)

  • Ahn, Chi-Kyu;Woo, Seung-Han;Park, Jong-Moon
    • Journal of Soil and Groundwater Environment
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    • v.13 no.1
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    • pp.32-42
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    • 2008
  • A surfactant recovery and reuse process by selective adsorption with activated carbon was proposed to reduce surfactant cost in a soil washing process. Mathematical model simulation was performed for the whole process, which consists of soil washing, soil recovery, and soil re-washing. The optimal range of surfactant dosage was $6{\sim}10$-fold critical micelle concentration in soil. The efficiency of surfactant reuse process was decreased with increasing the dosage of activated carbon. Effectiveness factor for activated carbon significantly altered the efficiency of the reuse process unlike effectiveness factor for soil. Total requirement of surfactant was reduced to 20-30% with the reuse process compared to the conventional soil washing process. The contamination of wastewater after soil washing was reduced with the reuse process. This mathematical model can be used to estimate performance of the whole process of soil washing including surfactant recovery and to obtain optimal ranges of operating conditions without extra labor-intensive experimental works.

A Study to Recover Si from End-of-Life Solar Cells using Ultrasonic Cleaning Method (초음파 세척법을 이용한 사용 후 태양광 셀로부터 Si 회수 연구)

  • Lee, Dong-Hun;Go, Min-Seok;Wang, Jei-Pil
    • Resources Recycling
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    • v.30 no.5
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    • pp.38-48
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    • 2021
  • In this study, we determine the optimal process conditions for selectively recovering Si from a solar cell surface by removal of impurities (Al, Zn, Ag, etc.). To selectively recover Si from solar cells, leaching is performed using HCl solution and an ultrasonic cleaner. After leaching, the solar cells are washed using distilled water and dried in an oven. Decompression filtration is performed on the HCl solution, and ICP-OES (Inductively Coupled Plasma Optical Emission spectroscopy) full scan analysis is performed on the filtered solution. Furthermore, XRD (X-ray powder diffraction), XRF (X-ray fluorescence), and ICP-OES are performed on the dried solar cells after crushing, and the purity and recovery rate of Si are obtained. In this experiment, the concentration of acid solution, reaction temperature, reaction time, and ultrasonic intensity are considered as variables. The results show that the optimal process conditions for the selective recovery of Si from the solar cells are as follows: the concentration of acid solution = 3 M HCl, reaction temperature = 60℃, reaction time = 120 min, and ultrasonic intensity = 150 W. Further, the Si purity and recovery rate are 99.85 and 99.24%, respectively.

Highly Efficient Biogas Upgrading Process Using Polysulfone Hollow Fiber Membrane at Low Temperature (폴리술폰 중공사막을 이용한 바이오가스 고순도화 고효율 저온 분리 공정)

  • Kim, Se Jong;Han, Sang Hoon;Yim, Jin Hyuk;Lee, Chung Seop;Chang, Won Seok;Kim, Gill Jung;Ha, Seong Yong
    • Membrane Journal
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    • v.32 no.2
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    • pp.140-149
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    • 2022
  • In this study, the conditions of low temperature and high pressure of biogas upgrading process using polysulfone membrane have been designed and tested to achieve the high recovery and efficiency corresponding to those of the highly selective polymeric materials. Polysulfone hollow fiber membrane with 4-component dope solution was spun via non-solvent induced phase separation. The hollow fiber membrane was mounted into a 1.5 inch housing. The effective area was 1.6 m2, and its performance was examined in various operation temperatures and pressures. CO2 and CH4 permeances were 412 and 12.7 GPU at 20℃, and 280 and 3.6 GPU at -20℃, respectively, while the CO2/CH4 selectivity increased from 32.4 to 77.8. Single gas test was followed by the mixed gas experiments using single-stage and double stage where the membrane area ratio varied from 1:1 to 1:3. At the single-stage, CH4 purity increased and the recovery decreased as the stage-cut increased. At the double stage, the area ratio of 1:3 showed the higher CH4 recovery as decreasing the operation temperature at the same purity of CH4 97%. Finally, polysulfone hollow fiber membranes have yielded of both CH4 purity and recovery of 97% at -20℃ and 16 barg.

Selective Recovery of the SSD TRIM Command in Digital Forensics (디지털 포렌식 관점에서 SSD TRIM 명령의 선별적 복구)

  • Hwang, Hyun Ho;Park, Dong Joo
    • KIPS Transactions on Computer and Communication Systems
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    • v.4 no.9
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    • pp.307-314
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    • 2015
  • Recently, market trends of auxiliary storage device HDD and SSD are interchangeable. In the future, the SSD is expected to be used more popular than HDD as an auxiliary storage device. The TRIM command technique has been proposed and used effectively due to the development of the SSD. The TRIM command techniques can be used to solve the problem of Freezing SSD that operating system cooperates with the SSD. The TRIM command techniques are performed in the idle time of the internal SSD that are actually deleted when a user deletes the data. However, in the point of view of computer forensics, the digital crime is increasing year by year due to lack of data recovery. Thus, this rate of arrest is insufficient. In this paper, I propose a solution that selectively manages data to delete based on advantage of the stability and the write speed of the TRIM command. Through experiments, It is verified by measuring the performance of the traditional method and selected method.

Precipitation of Magnesium Sulfate from Concentrated Magnesium Solution for Recovery of Magnesium in Seawater (해수 중 마그네슘 회수를 위한 마그네슘 농축액으로부터 황산마그네슘의 석출)

  • Cho, Taeyeon;Kim, Myoung-Jin
    • Resources Recycling
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    • v.25 no.4
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    • pp.32-41
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    • 2016
  • The precipitation test, which is the last step of magnesium recovery process consisting of three processes (pre-precipitation, selective dissolution of magnesium, precipitation) is performed to obtain magnesium sulfate powder from seawater. In the study, we succeed in precipitating the magnesium sulfate by adding acetone into the solution of magnesium over 4 times concentrated from seawater. The yield efficiency of magnesium sulfate increases with increasing pH and the ratio of added acetone. More than 99% of magnesium is obtained as magnesium sulfate hydrate ($MgSO_4{\cdot}6H_2O$) under the following conditions; pH 1.0 ~ 1.5, and the ratio of solution and acetone 1 : 1.5 (v:v). The acetone used in the precipitation process is recovered by the fractional distillation.

Simultaneous determination of fluorometholone and tetrahydrozoline hydrochloride in ophthalmic suspension by HPLC

  • Pham, Thuy-Vy;Mai, Xuan-Lan;Song, Ha-Ram;Ahn, Soo-Bin;Cha, Min-Jeong;Kang, Jong-Seong;Woo, Mi Hee;Na, Dong-Hee;Chun, In-Koo;Kim, Kyeong Ho
    • Analytical Science and Technology
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    • v.31 no.2
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    • pp.88-95
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    • 2018
  • A simple, sensitive, and selective high-performance liquid chromatography (HPLC) method was developed and validated for the simultaneous quantification of fluorometholone (FLU) and tetrahydrozoline hydrochloride (THZ) in combined ophthalmic formulations. The effects of several factors, including detection wavelength, buffer pH, buffer concentration, and organic solvent concentration, on the performance of the method were investigated. The performance of the developed method was validated in accordance with the requirements of the International Conference on Harmonization. The linearity of the calibration curves in the desired concentration range was high for both FLU and THZ ($r^2=0.9999$). The accuracy and precision of the method were determined by a recovery study at analyte concentrations of 80 %, 100 %, and 120 %. The recovery was 99.60-100.17 % for both analytes, with a relative standard deviation less than 1.0 % at any concentration level. The validated results indicate that the new HPLC method could be successfully applied for the simultaneous determination of FLU and THZ in ophthalmic suspensions.

Clinical Outcomes of Spontaneous Spinal Epidural Hematoma : A Comparative Study between Conservative and Surgical Treatment

  • Kim, Tackeun;Lee, Chang-Hyun;Hyun, Seung-Jae;Yoon, Sang Hoon;Kim, Ki-Jeong;Kim, Hyun-Jib
    • Journal of Korean Neurosurgical Society
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    • v.52 no.6
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    • pp.523-527
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    • 2012
  • Objective : The incidence of spontaneous spinal epidural hematoma (SSEH) is rare. Patients with SSEH, however, present disabling neurologic deficits. Clinical outcomes are variable among patients. To evaluate the adequate treatment method according to initial patients' neurological status and clinical outcome with comparison of variables affecting the clinical outcome. Methods : We included 15 patients suffered from SSEH. Patients were divided into two groups by treatment method. Initial neurological status and clinical outcomes were assessed by the American Spinal Injury Association (ASIA) impairment scale. Also sagittal hematoma location and length of involved segment was analyzed with magnetic resonance images. Other factors such as age, sex, premorbid medication and duration of hospital stay were reviewed with medical records. Nonparametric statistical analysis and subgroup analysis were performed to overcome small sample size. Results : Among fifteen patients, ten patients underwent decompressive surgery, and remaining five were treated with conservative therapy. Patients showed no different initial neurologic status between treatment groups. Initial neurologic status was strongly associated with neurological recovery (p=0.030). Factors that did not seem to affect clinical outcomes included : age, sex, length of the involved spinal segment, sagittal location of hematoma, premorbid medication of antiplatelets or anticoagulants, and treatment methods. Conclusion : For the management of SSEH, early decompressive surgery is usually recommended. However, conservative management can also be feasible in selective patients who present neurologic status as ASIA scale E or in whom early recovery of function has initiated with ASIA scale C or D.

Studies on Selective Separation of Highly Motile Bovine Sperm (고활력우정자(高活力牛精子)의 선택적(選擇的) 분리(分離)에 관한 연구(硏究))

  • Kim, Myung-cheol
    • Korean Journal of Veterinary Research
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    • v.24 no.2
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    • pp.245-266
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    • 1984
  • As a fundamental study to increase the reproductive efficiency in cattle, highly motile sperm were separated and collected from raw semen, extended semen and frozen semen by different methods using various concentrations of bovine serum albumin or Tyrode's solution. Various characteristics and light microscopic and electron-microscopic morphology of sperm separated by different methods were compared. The results obtained were as follows; 1. The sperm separated from raw semen using bovine serum albumin showed significantly high value in motility, motile sperm count, percent of normal sperm and progressive motility, as compared with control sperm and revealed the highest sperm recovery rate when separated with 6% bovine serum albumin. 2. The sperm motility, percent of normal sperm and progressive motility of the highly motile sperm frozen after being separated from raw semen with bovine serum albumin, showed significantly high value than those of a control sperm and especially found the highest value when separated with 20% bovine serum albumin. 3. Light-microscopic percent of abnormality was significantly low in the prefrozen and postfrozen highly motile sperm separated with bovine serum albumin, as compared with control sperm. 4. Electron-microscopic finding of the highly motile sperm separated with bovine serum albumin showed low percent of deformity in the dilatation and vesiculation of cell membrane, in dilatation and density loss of acrosome than in those of control sperm. 5. It was impossible to separate the highly motile sperm from frozen semen with bovine serum albumin, but it was possible with Tyrode's solution. 6. Recovery rate of highly motile sperm from raw semen extended semen and frozen semen was the highest when the sperm pellet stood in Tyrde's solution for 80 minutes. 7. The highly motile sperm separated from raw semen, extended semen and frozen semen with Tyrode's solution showed significantly high value in motility, progressive motility and percent of normal sperm, as compared with control sperm. 8. Highly motile sperm, when separated from raw semen, extended semen and frozen semen with Tyrode's solution, showed significantly low percent of microscopic abnormality as compared with control sperm.

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