• Title/Summary/Keyword: Sealing materials

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Sealing Ability of Three Different Materials Used as Retrograde Filling

  • Park, Ji-Hoon;Kang, Seung-Bok;Choi, Yong-Hoon;Bae, Ji-Hyun
    • Journal of Korean Dental Science
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    • v.5 no.2
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    • pp.60-67
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    • 2012
  • Purpose: To test the apical leakage prevention performance of three different materials through protein leakage procedures using bovine serum albumin (BSA) and Bradford protein reagent. Materials and Methods: A total of 60 human single-rooted teeth were divided into 4 groups, and conventional root canal filling was done. The root was cut 3 mm from the apex, and a cavity was formed. Proroot MTA (MTA), Fuji II LC (GI), Fuji II LC with XP bond (GIA), and Caviton (CA) were used as experimental materials to fill the cavity in a retrograde filling manner. The extent of BSA leakage was then measured with a ultraviolet visible spectrophotometer 24, 48, and 72 hours after filling. Result: After 24 hours, among the 15 teeth of each group, 2 in MTA, 4 in GI, 3 in GIA, and 7 in CA showed leakage. After 48 hours, 3 in MTA, 5 in GI, 5 in GIA, and 10 in CA had leakage and discoloration. After 72 hours, among the 15 teeth of each group, 3 in MTA, 6 in GI, 5 in GIA, and 10 in CA showed leakage. The leakage in the CA group was greater than that in the MTA group at 48 and 72 hours based on Fisher's exact test (P=0.025), and the difference was statistically significant. Similarly, the leakage in the CA group was greater than that in the MTA group over time based on the Kaplan-Meier survival estimate (P=0.011), and the difference was statistically significant. Conclusion: Glass ionomer, glass ionomer after adhesive application, and MTA all showed leakage. Caviton showed greater leakage compared to MTA 48 and 72 hours after filling, and the difference was statistically significant; thus suggesting that Caviton is not appropriate as retrograde filling material considering its sealing ability.

A Study on the sealing Characteristic of Automobile Waterproof Connector (자동차용 방수커넥터의 밀봉특성에 관한 연구)

  • Ko, Young-Bae;Park, Hyung-Pil;Lee, Jeong-Won;Cha, Baeg-Soon
    • Journal of the Korea Academia-Industrial cooperation Society
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    • v.15 no.4
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    • pp.1859-1864
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    • 2014
  • Liquid silicone rubber(LSR) has been applied to various products such as electronic devices owing to its excellent thermal and chemical resistance. Hyperelastic materials, however, have properties distinguished from general metal materials. Hyperelastic materials show elastic behaviors in the range of large deformation in which load has the nonlinear relation with deformation. In addition, they have characteristics of nonlinearity, incompressibility, in large scale. On account of such characteristics, there are many difficulties in design and production using these materials. In this study, the load-deformation relation obtained from tension and compression tests was applied to finite element analysis in order to design waterproof connectors for automobiles. Furthermore, the effectiveness of the finite element analysis was confirmed by comparing the results of analysis with those of performance tests.

HISTOPATHOLOGIC STUDY OF FURCATION PERFORATIONS REPAIRED WITH SOME MATERIALS (치근이개부 천공부위에 대한 수종수복재의 치유효과에 관한 조직병리학적 연구)

  • Hong, Han-Pyo;Hong, Chan-Ui;Shin, Dong-Hoon
    • Restorative Dentistry and Endodontics
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    • v.20 no.2
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    • pp.610-626
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    • 1995
  • Perforations especially in the furcations during endodontic treatment have notably detrimental effect on prognosis. The purpose of this study was to compare radiographically and histologically the sealing ability and the tissue responses of amalgam, Ketac-Silver, IRM, Vitapex, and mineral trioxide aggregate(MTA) used to repair furcation perforations. Thirty two experimental furcation perforations were created in the mandibular premolars of 6 mongrel dogs and immediately repaired with experimental materials. The animals were sacrificed after 16 weeks and radiographic and histopathologic results were evaluated. The following conclusions were drawn within the limits of the experimental results; 1. All materials tested in this experiment revealed a certain degree of extrusion into the periodontal space. 2. Both amalgam and Ketac-Silver showed the greatest degree of inflammation and bone resorption(p<0.0001). There was no significant difference between the amalgam and Ketac-Silver groups. 3. Both IRM and Vitapex showed a markedly milder degree of inflammatin and less bone resorption than amalgam or ketac-siver(p<0.00005). both IRM and vitapex showed the same respone. 4. MTA showed the least degree of Inflammation and bone resorption(p<0.05). The results of this experiment indicate that among the different materials tested, MTA appeared to be the best material for sealing furcation perforations, although the radiographic and histopathologic differences between the MTA and Vitapex groups were not statistically significant. But further studies with a larger sample are needed to have the exact conclusions.

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SURFACE ROUGHNESS AND MICROLEAKAGE OF CLASS V COMPOSITE RESTORATIONS : EFFECT OF SURFACE SEALING (치경부 5급 와동 수복물의 표면 거칠기와 미세누출에 관한 연구 : 표면 전색의 효과)

  • Kim, Min-Jeong;Lee, Mi-Jeong;Yu, Mi-Kyung;Park, Soo-Joung;Lee, Kwang-Won
    • Restorative Dentistry and Endodontics
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    • v.30 no.1
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    • pp.22-30
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    • 2005
  • The purpose of this study was to compare the effect of surface sealing materials on microleakage and surface roughness in Class V composite restorations. Twenty five standardized Class V cavity preparations were made on the facial surface of human premolars and were randomly assigned to 5 groups. The teeth were restored with Z-250 after applying Single Bond. Following 7 days storage in distilled water at $37^{\circ}C$, the restorations were sealed as following systems : No sealing ; Single Bond Adhesive ; Biscover ; Fortify ; Optiguard. Then, toothbrush abrasion test was conducted using a wear testing machine. Surface roughness was measured by means of profilometer before and after toothbrushing and the results were statistically analysed by using a paired t-test and ANOVA. The bonded interfaces and the changes of surface roughness were examined by SEM. For microleakage test, specimens were stained in a $2\%$ methylene blue solution, then longitudinally sectioned and analyzed for leakage at occlusal and cervical interfaces using stereomicroscope. The results were statistically analysed by using a Kruskal-Wallis and Mann-Whitney U test. Surface roughness was increasing in all groups after toothbrushing, but no statistically significant differences. In SEM observation, surface sealant was partially retained and partially detached in bonded interfaces. Especially, microgap was identified in cervical margins. In microleakage test, there was better seal in the enamel region and a significant difference between groups at occlusal margin. Control group and Single Bond group had significantly better marginal seal at enamel margin than cervical margin.

Dependence of Xe Plasma Flat Fluorescent Lamp On the Electrode Gap and Dielectric Layer Thickness

  • Kang, Jong-Hyun;Lee, Yang-Kyu;Heo, Sung-Taek;Oh, Myung-Hoon;Lee, Dong-Gu
    • 한국정보디스플레이학회:학술대회논문집
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    • 2007.08b
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    • pp.1519-1521
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    • 2007
  • In this work, a coplanar-type plasma flat fluorescent lamp having cross type of electrode was fabricated by screen printing and sealing technique. Cross type of electrode with a dielectric layer were screen-printed on a rear glass plate, and then fired at $550^{\circ}C$. Phosphor was printed on and fired at $450^{\circ}C$. Finally, the lamp was sealed by frit glass at $450^{\circ}C$. The lamp of cross electrode type was studied depending on the electrode gap and the thickness of dielectric layer.

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MARGINAL LEAKAGE TEST ON HI-POL COMPOSITE RESIN (국산 하이폴 복합레진의 변록누출에 관한 실험적 연구)

  • Lim, Sung-Sam
    • The Journal of the Korean dental association
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    • v.15 no.11
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    • pp.757-761
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    • 1977
  • The purpose of this study was to evaluate the marginal sealing ability of Hipol composite resin. Using freshly extracted human teeth and 2% acquous methylene blue, the marginal leakage of dye in restorative materials such as Hi-pol, Adaptic, Nuvasystem, Epolite and Amalgam was investigated at 37℃ and under temperature cycling between 4℃ and 60℃. The results were as follows; 1. All the filling materials revealed the penetration of dye between cavity walls and restorations. 2. Hi-pol and Adaptic showed more marginal leakage than other materials and the degree of dye penetration in Hi-pol was similar to that of Adaptic. 3. Nuva system showed the least marginal leakage at 37℃ and under temperature cycling between 4℃ and 60℃. 4. Under temperature cycling, all materials showed a slight increase in marginal leakage except Epolite, which showed the greastest change in leakage.

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Investigating the Tensile-Shear of Dissimilar Materials Joined Using the Hybrid SPR Technique (Hybrid SPR 접합을 적용한 이종소재 인장전단에 관한 연구)

  • Yu, Kwan-jong;Choi, Du-bok;Kim, Jae-yeol
    • Journal of the Korean Society of Manufacturing Process Engineers
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    • v.19 no.9
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    • pp.33-39
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    • 2020
  • Self-piercing rivets are often used in the automotive industry, among other industries, as mechanical components to join multiple materials such as aluminum alloys. Self-piercing rivets have a strong sealing property, although there is considerable scope for their performance improvement. In this study, to enhance the performance of self-piercing rivets, the hybrid self-piercing riveting (SPR) technique, using the existing SPR and structural adhesive, was proposed. Moreover, heterogeneous material specimens subjected to the hybrid SPR technique were manufactured and tested. The joint strength of the test pieces of different materials was evaluated through finite element analyses.

Development of Miniature Quad SAW Filter Bank based on PCB Substrate

  • Lee, Young-Jin;Kim, Chang-Il;Paik, Jong-Hoo
    • Transactions on Electrical and Electronic Materials
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    • v.9 no.1
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    • pp.33-37
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    • 2008
  • This paper describes the development of a new $5.0{\times}3.2mm$ SAW filter bank which is consist of 12 L, C matching components and 4 SAW bare chips on PCB substrate with CSP technology. We improved the manufacturing cost by removing the ceramic package through direct flip bonding of $LiTaO_3$ SAW bare chip on PCB board after mounting L, C passive element on PCB board. After that we realized the hermitic sealing by laminating the epoxy film. To confirm the confidentiality and durability of the above method, we have obtained the optimum flip bonding & film laminating condition, and figured out material property and structure to secure the durability & moisture proof of PCB board. The newly developed super mini $5.0{\times}3.2mm$ filter bank shows the superior features than those of existing products in confidence, electrical, mechanical characters.

Effect of Sealant Materials on Oxygen Permeation in Perovskite Oxide Membrane (밀봉 재료에 따른 페롭스카이트 막의 산소투과 특성)

  • Kim, Jong Pyo;Park, Jung Hoon;Yoon, Yeoil
    • Applied Chemistry for Engineering
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    • v.19 no.4
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    • pp.382-387
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    • 2008
  • $Ba_{0.5}Sr_{0.5}Co_{0.8}Fe_{0.2}O_{3-{\delta}}$ oxide was synthesized by polymerized complex method. Dense membrane of perovskite oxide was prepared using as-prepared powder by pressing and sintering at $1080^{\circ}C$. Leakage test was conducted on the membrane sealed by gold ring, Pyrex ring or Pyrex powder as a sealing material. The oxygen permeation flux of $Ba_{0.5}Sr_{0.5}Co_{0.8}Fe_{0.2}O_{3-{\delta}}$ membrane increased with increasing temperature and was $0.74mL/min{\cdot}cm^2$ at $900^{\circ}C$. In the case of the membrane applied by sealing material, oxygen permeation flux of the membrane using gold ring at $950^{\circ}C$ was higher than that using Pyrex materials because the undesired spreading of Pyrex glass materials in the membrane led to the reduction of effective permeation area. Microphotograph analysis results for the membrane after permeation test confirmedthe diffusion of Pyrex glass seal into the membrane.