• 제목/요약/키워드: Sample-loading

검색결과 308건 처리시간 0.023초

The Effect of Sample Handling on the Rheological Measurement of Regenerated Silk Fibroin Formic Acid Solution using Parallel Plate Geometry

  • Cho, Hee-Jung;Um, In-Chul
    • International Journal of Industrial Entomology and Biomaterials
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    • 제22권1호
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    • pp.5-10
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    • 2011
  • The effect of sample handling condition on the rheological measurement of regenerated silk fibroin formic acid solution using parallel plate geometry was investigated. In case of loading method, the loading by pouring sample solution resulted in the best reproducibility of rheological measurement. Loading with spoon showed a high variance of viscosity value at low shear rate region ($0.01{\sim}1sec^{-1}$) while loading with syringe exhibited a low reproducibility of viscosity at high shear region ($1{\sim}100sec^{-1}$) with a disappearance of shear thinning phenomenon. It was revealed that the sample loading with small extra amount lead to the most reproducible result. The sample loading with the exact amount for the measuring plate resulted in a lack of reproducibility of high shear viscosity, while the loading with large extra volume produced a limited consistency of low shear viscosity. It was turned out that 3 min. of waiting time before measurement was the optimum condition for reliable result. When the waiting time was less than 1 min., the low shear viscosity was obtained with a lack of consistency. On the other hand, the sample solution started drying when the waiting time increased up to 5 min.

Effect of Sample-loading on Fractionation Efficiency (FE) in a Large Scale Splitter-less Gravitational SPLITT Fractionation (GSF)

  • Lee, Seung-Ho;Lee, Ji-Yeon;Lee, Tae-Woo;Jung, Euo-Chang;Cho, Sung-Kwang
    • Bulletin of the Korean Chemical Society
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    • 제32권12호
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    • pp.4291-4296
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    • 2011
  • Gravitational SPLITT fractionation (GSF) provides separation of colloidal particles into two subpopulations in a preparative scale. Conventionally, GSF is carried out in a thin rectangular channel having two inlets and two outlets at the top and bottom of the channel, respectively. And the channel is equipped with two flow-splitters, one between the top and bottom inlets and another between the top and bottom outlets. A large scale splitter-less GSF system had been developed, which was designed to operate in the full feed depletion (FFD) mode. In the FFD mode, there is only one inlet through which the sample is fed, thus preventing the sample dilution. In this study, the effect of the sample-loading (in the unit of g/hr) on the fractionation efficiency (FE, number% of particles in a GSF fraction that have the sizes expected by theory) of the new large scale splitter-less FFD-GSF system was investigated. The system was tested in the sample-loading range of 3.0-12.0 g/hr with polyurethane latex beads (PU) and sea-sediment. It was found that there is an optimum range in the sample-loading for a FFD-GSF separation. It was also found that there is a general tendency of FE decreasing as the concentration of the sample suspension increases.

휨 모멘트에 대한 오이의 응력이완(應力弛緩) 특성(特性) (Stress Relaxation Properties of Cucumber under Bending Moment)

  • 송천호;김만수;박종민
    • Journal of Biosystems Engineering
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    • 제18권3호
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    • pp.262-269
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    • 1993
  • Stress relaxation behaviors of the cucumber under bending moment were tested with UTM at three levels of loading rate and initial deflection ratio. Sample cucumber was selected from three cultivars of cucumber, Cheongjangmadi, Baekdadagi, and Gyeousalicheongjang, because these cultivars are the most popular grown cultivars in Korea. When the bending moment was applied to the cucumber sample, the effective span between simple supports was held a constant value of 116mm with consideration of the selected sample length. The objectives of this study were to develop the rheological models such as linear and nonlinear models of the stress relaxation for the cucumber samples, and to investigate the effects of loading rate and initial deflection ratio on the stress relaxation behavior of the cucumber. The results of this study may be summarized as follows : 1. Stress relaxation behavior of the cucumber could be well described by the generalized Maxwell model for each level of deflection ratio. But the stress relaxation behavior of the sample was found to be initial deflection ratio and time dependent, and it was represented the nonlinear viscoelastic model as a function of initial deflection ratio and time. 2. Stress relaxation behavior of the cucumber samples was very highly affected by the loading rate and the initial deflection ratio. The more loading rate and initial deflection ratio resulted in the more initial bending stress and after stress relaxation progressed more rapidly. 3. At the same test conditions, it was found that the stress relaxation rate of Cheongjangmadi was faster than that of other cultivars.

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GPS 항재밍을 위한 적응 배열 안테나의 성능 분석 (Performance Analysis of Adaptive Array Antenna for GPS Anti-Jamming)

  • 정태희
    • 한국군사과학기술학회지
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    • 제16권3호
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    • pp.382-389
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    • 2013
  • In anti-jamming GPS receiver, adaptive signal processing techniques in which the radiation pattern of adaptive array antenna of elements may be adaptively changed used to reject interference, clutter, and jamming signals. In this paper, I describes adaptive signal processing technique using the sample matrix inversion(SMI) algorithm. This adaptive signal processing technique can be applied effectively to wideband/narrowband anti-jamming GPS receiver because it does not consider the satellite signal directions and GPS signal power level exists below the thermal noise. I also analyzed the effects of covariance matrix sample size and diagonal loading technique on the system performance of five-element circular array antenna. To attain near optimum performance, more samples required for calculation covariance matrix. Diagonal loading technique reduces the system nulling capability against low-power jamming signals, but this technique improves robustness of adaptive array antenna.

Effects of loading conditions on the fatigue failure characteristics in a polycarbonate

  • Okayasu, Mitsuhiro;Yano, Kei;Shiraishi, Tetsuro
    • Advances in materials Research
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    • 제3권3호
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    • pp.163-174
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    • 2014
  • In this study, fatigue properties and crack growth characteristics of a polycarbonate (PC) were examined during cyclic loading at various mean stress (${\sigma}_{amp}$) and stress amplitude (${\sigma}_{mean}$) conditions. Different S vs. N and da/dN vs. ${\Delta}K$ relations were obtained depending on the loading condition. The higher fatigue strength and the higher resistance of crack growth are seen for the PC samples cyclically loaded at the higher mean stress and lower stress amplitude due to the low crack driving force. Non-linear S - N relationship was detected in the examination of the fatigue properties with changing the mean stress. This is attributed to the different crack growth rate (longer fatigue life): the sample loaded at the high mean stress with lower stress amplitude. Even if the higher stress amplitude, the low fatigue properties are obtained for the sample loaded at the higher mean stress. This was due to the accumulated strain energy to the sample, where severe plastic deformation occurs instead of crack growth (plasticity-induced crack closure). Shear bands and discontinuous crack growth band (DGB) are observed clearly on the fracture surfaces of the sample cyclically loaded at the high stress amplitude, where the lower the ${\sigma}_{mean}$, the narrower the shear band and DGB. On the other hand, final fracture occurred instantly immediately after the short crack growth occurs in the PC sample loaded at the high mean with the low ${\sigma}_{amp}$, i.e., tear fracture, in which the shear bands and DGB are not seen clearly.

Suggesting a new testing device for determination of tensile strength of concrete

  • Haeri, Hadi;Sarfarazi, Vahab;Hedayat, Ahmadreza
    • Structural Engineering and Mechanics
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    • 제60권6호
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    • pp.939-952
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    • 2016
  • A compression to tensile load transforming (CTT) device was developed to determine indirect tensile strength of concrete material. Before CTT test, Particle flow code was used for the determination of the standard dimension of physical samples. Four numerical models with different dimensions were made and were subjected to tensile loading. The geometry of the model with ideal failure pattern was selected for physical sample preparation. A concrete slab with dimensions of $15{\times}19{\times}6cm$ and a hole at its center was prepared and subjected to tensile loading using this special loading device. The ratio of hole diameter to sample width was 0.5. The samples were made from a mixture of water, fine sand and cement with a ratio of 1-0.5-1, respectively. A 30-ton hydraulic jack with a load cell applied compressive loading to CTT with the compressive pressure rate of 0.02 MPa per second. The compressive loading was converted to tensile stress on the sample because of the overall test design. A numerical modeling was also done to analyze the effect of the hole diameter on stress concentrations of the hole side along its horizontal axis to provide a suitable criterion for determining the real tensile strength of concrete. Concurrent with indirect tensile test, the Brazilian test was performed to compare the results from two methods and also to perform numerical calibration. The numerical modeling shows that the models have tensile failure in the sides of the hole along the horizontal axis before any failure under shear loading. Also the stress concentration at the edge of the hole was 1.4 times more than the applied stress registered by the machine. Experimental Results showed that, the indirect tensile strength was clearly lower than the Brazilian test strength.

The effectiveness of geosynthetic reinforcement, tamping, and stoneblowing of railtrack ballast beds under dynamic loading: DEM analysis

  • Lobo-Guerrero, Sebastian;Vallejo, Luis E.
    • Geomechanics and Engineering
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    • 제2권3호
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    • pp.161-176
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    • 2010
  • Discrete Element Method (DEM) simulations were developed to investigate the effectiveness of geosynthetic reinforcement and the effectiveness of maintenance techniques performed on a simulated ballast bed subjected to dynamic loading. The results from four samples subjected each one to a total of 425 load cycles are presented: one unreinforced and unmaintained sample, one unmaintained but reinforced sample, one unreinforced sample subjected to maintenance in the form of stoneblowing after 200 load cycles, and one unreinforced sample subjected to maintenance in the form of tamping after 200 load cycles. The obtained values of permanent deformation as a function of the applied number of load cycles for the four cases are presented together allowing a comparison of the effectiveness of each technique. Moreover, snapshots of the simulated track sections are presented at different moments of the simulations. The simulations indicated that the geosynthetic reinforcement may not be beneficial for the analyzed case while stoneblowing was the most effective maintenance technique.

낙동강 모래의 반복응력이력에 의한 거동 (Behaviour of Nak-dong River Sand on Cyclic Stress History)

  • 김영수;박명렬;김병탁;이상복
    • 한국지반공학회:학술대회논문집
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    • 한국지반공학회 2000년도 가을 학술발표회 논문집
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    • pp.295-302
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    • 2000
  • Earthquakes not only produce additional load on the structures and underlying soil, but also change the strength characteristics of the soil. Therefore, in order to analyze soil structures for stability, the behaviour after earthquake must be considered. In this paper, a series of cyclic triaxial tests and monotonic triaxial tests were carried out to investigate the undrained shear strength and liquefaction strength characteristics of Nak-Dong River sand soils which were subjected to cyclic loading. The sample was consolidated in the first stage and then subjected to stress controlled cyclic loading with 0.1Hz. After the cyclic loading, the cyclic-induced excess pore water pressure was dissipated by opening the drainage valve and the sample was reconsolidated to the initial effective mean principal stress(p/sub c/'). After reconsolidation, the monotonic loading or cyclic loading were applied to the specimen. In the results, the undrained shear strength and liquefaction strength characteristics depended on the pore pressure ratio(Ur=U/p/sub c/'). The volume change following reconsolidation can be a function of cyclic-induced excess pore water pressure and the maximum double amplitude of axial strain.

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Simulation of the effect of inclusions length and angle on the failure behavior of concrete structure under 3D compressive test: Experimental test and numerical simulation

  • Mohammad Saeed, Amini;Vahab, Sarfarazi;Kaveh, Asgari;Xiao, Wang;Mojtaba Moheb, Hoori
    • Steel and Composite Structures
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    • 제46권1호
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    • pp.53-73
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    • 2023
  • Man-made structure materials like concrete usually contain inclusions. These inclusions affect the mechanical properties of concrete. In this investigation, the influence of inclusion length and inclination angle on three-dimensional failure mechanism of concrete under uniaxial compression were performed using experimental test and numerical simulation. Approach of acoustic emission were jointly used to analyze the damage and fracture process. Besides, by combining the stress-strain behavior, quantitative determination of the thresholds of crack stress were done. concrete specimens with dimensions of 120 mm × 150 mm × 100 mm were provided. One and two holes filled by gypsum are incorporated in concrete samples. To build the inclusion, firstly cylinder steel tube was pre-inserting into the concrete and removing them after the initial hardening of the specimen. Secondly, the gypsum was poured into the holes. Tensile strengths of concrete and gypsum were 2.45 MPa and 1.5 MPa, respectively. The angle bertween inclusions and axial loadind ary from 0 to 90 with increases of 30. The length of inclusion vary from 25 mm to 100 mm with increases of 25 mm. Diameter of the hole was 20 mm. Entirely 20 various models were examined under uniaxial test. Simultaneous with experimental tests, numerical simulation (Particle flow code in two dimension) were carried out on the numerical models containing the inclusions. The numerical model were calibrated firstly by experimental outputs and then failure behavior of models containing inclusions have been investigated. The angle bertween inclusions and axial loadind vary from 0 to 90 with increases of 15. The length of inclusion vary from 25 mm to 100 mm with increases of 25 mm. Entirely 32 various models were examined under uniaxial test. Loading rate was 0.05 mm/sec. The results indicated that when inclusion has occupied 100% of sample thickness, two tensile cracks originated from boundaries of sample and spread parallel to the loading direction until being integrated together. When inclusion has occupied 75% of sample thickness, four tensile cracks originated from boundaries of sample and spread parallel to the loading direction until being integrated together. When inclusions have occupied 50% and 25% of sample thickness, four tensile cracks originated from boundaries of sample and spread parallel to the loading direction until being integrated together. Also the inclusion was failed by one tensile crack. The compressive strength of samples decease with the decreases of the inclusions length, and inclusion angle had some effects on that. Failure of concrete is mostly due to the tensile crack. The behavior of crack, was affected by the inclusion length and inclusion number.

Experimental and numerical investigation of expanded polystyrene (EPS) geofoam samples under monotonic loading

  • Khalaj, Omid;Siabil, Seyed Mohammad Amin Ghotbi;Azizian, Mehran;Tafreshi, Seyed Naser Moghaddas;Masek, Bohuslav;Kepka, Miloslav;Kavalir, Tomas;Krizek, Michal;Jirkova, Hana
    • Geomechanics and Engineering
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    • 제22권6호
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    • pp.475-488
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    • 2020
  • The recent increase in the use of Expanded Polystyrene (EPS) geofoam in construction and geotechnical projects has driven researchers to investigate its behavior, more deeply. In this paper, a series of experimental tests to investigate the stress-strain behavior and the mechanical properties of EPS blocks, under monotonic axial loading are presented. Four different densities of cylindrically shaped EPS with different dimensions are used to investigate the effects of loading rate, height and diameter, as well as the influence of the density of EPS on the stress-strain response. The results show that increasing the height of the EPS samples leads to instability of the sample and consequent lower resistance to the applied pressure. Large EPS samples show higher Young's modulus and compressive resistance due to some boundary effects. An increase in the rate of loading can increase the elastic moduli and compressive resistance of the EPS geofoam samples, which also varies depending on the density of the samples. It was also determined that the elastic modulus of EPS increases with increasing EPS density. By implementing an efficient numerical procedure, the stress-strain response of EPS geofoam samples can be reproduced with great accuracy. The numerical analysis based on the proposed method can used to evaluate the effect of different factors on the behavior of EPS geofoam.