• 제목/요약/키워드: STS/Al/STS

검색결과 111건 처리시간 0.027초

하이브리드 코팅 시스템을 이용한 $CrAlC_xN_{1-x}$ 코팅의 합성과 기계적 특성 (Synthesis and mechanical properties of $CrAlC_xN_{1-x}$ coatings by a hybrid coating system)

  • 최지환;홍영수;김광호
    • 한국표면공학회:학술대회논문집
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    • 한국표면공학회 2009년도 추계학술대회 초록집
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    • pp.200-200
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    • 2009
  • 아크이온플래이팅 기술과 DC 마그네트론 스퍼터링 기술이 결합된 하이브리드 코팅 시스템을 이용하여 STS 304와 Si 기판에 4성분계 CrAlCxN1-x 코팅을 증착하였다. 합성된 CrAlCxN1-x 코팅은 주로 유도결합형로 f구성되었다. CrAlCxN1-x 코팅의 carbon 함량이 0.17 at.%일 때 약 34 GPa을 나타내었으며 마찰계수는 carbon 함량이 0에서 1 at.%로 증가함에 따라 0.82에서 0.38까지 크게 감소하였다. 이는 코팅 표면과 steel 볼 사이에 amorphous carbon layer가 형성되어 고체윤활제로 작용한 것으로 사료된다.

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Detection of Al3+ by fluorescent turn-on nitrogen/sulphur-binary doped carbon dots

  • Siti Raudhatul Kamali;Chang-Nan Chen;Tai-Huei Wei
    • 분석과학
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    • 제36권4호
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    • pp.161-169
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    • 2023
  • In this study, a straightforward and precise nitrogen/sulphur-codoped carbon dots (N/S-CD) was produced using a microwave irradiation approach. The N/S-CD was formulated from succinic acid (SA), bis-(3-aminopropyl)-amine (BAPA), and sodium thiosulphate (STS) as sources of carbon, nitrogen, and sulphur, respectively. The synthesized N/S-CD established a valuable quantum yield (QY) of 70 % and was sensitive to aluminium ion (Al3+) with a detection limit of 0.21 µM and a linear concentration range of 0-100 µM. When detecting Al3+ in real water samples, the N/S-CD resulted in a satisfactory recovery in the range of 91.14 %-103.37 %. Thus, the proposed study is very promising for Al3+ detection in environmental water samples.

레이저피닝을 이용한 스테인리스강의 표면 경도 강화 (Enhancement of Surface Hardness of Stainless Steel by Laser Peening)

  • 임현택;이명화;김필규;박종복;정성호
    • 한국레이저가공학회지
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    • 제12권3호
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    • pp.18-22
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    • 2009
  • Experimental results for the laser shock peening of stainless steels, duplex stainless steel and STS304, for the enhancement of surface hardness are reported. A high power Nd:YAG laser (532 nm, 2nd harmonics) was used to irradiate the workpiece in water at the irradiances of 5, 10, $15\;GW/cm^2$. The surface of a workpiece was covered with Fe or Al foil for protection of the original surface and reduction of laser reflection. The laser pulse densities were varied from $25\;pulse/mm^2$ to $75\;pulse/mm^2$. In the case of the STS304, the surface hardness increased with increasing pulse density and the maximum increase of about 29% was achieved using Fe foil at $10\;GW/cm^2$ and $75\;pulse/mm^2$ conditions. The maximum increase in surface hardness of duplex stainless steel was about 8% at $10\;GW/cm^2$ and $75\;pulse/mm^2$ with also Fe foil. In the case of the Al foil, less increase of surface hardness was obtained, possibly due to the thermal expansion effect.

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롤 아연된 STS-Al-Mg 이종금속판재의 온도와 변형률속도에 따른 1축인장 변형특성 (Temperature and Strain Rate Dependent Tension Properties of Stainless Steel-Aluminum-Magnesium Multilayered Sheet Fabricated by Roll Bonding)

  • 황범규;이광석;홍순익;이영선
    • 소성∙가공
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    • 제20권3호
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    • pp.257-264
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    • 2011
  • Multilayer(clad) sheets, composed of two or more materials with different properties, are fabricated using the roll-bonding process. A good formability is an essential property for a multilayered sheet in order to manufacture parts by plastic deformation. In this study, the influences of temperature and strain rate on the plastic properties of stainless steel-aluminum-magnesium multilayered(STS-Al-Mg) sheets were investigated. Tensile tests were performed at various temperatures and strain rates on the multilayered sheet and on each separate layer. Fracture of the multilayered sheet was observed to be temperature-dependent. At the base temperature of $200^{\circ}C$, all materials fractured simultaneously. At lower temperatures, the Mg alloy sheet fractured earlier than the other materials. Conversely, the other materials fractured earlier than the Mg alloy sheet at higher temperatures. The uniform and total elongations of the multilayered sheet were observed to be higher than that of each material at a temperature of $250^{\circ}C$. Larger uniform elongations were obtained for higher strain rates at constant temperature. The same trend was observed for the Mg alloy sheet, which exhibited the lowest elongation among the three materials. The tensile strengths and elongations of the single layer sheets were compared to those of the multilayer material. The strength of the multilayered sheet was successfully calculated by the rule of mixture from the values of each single layer. However, no simple correlation between the elongation of each layer and that of the multilayer was obtained.

무인기용 레큐퍼레이터 소재의 용접부에 대한 고온 피로수명 예측 (High Temperature Fatigue Life Prediction for Welded Joints of Recuperator Material for UAV)

  • 이상래;김재환;김재훈
    • 한국추진공학회지
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    • 제23권2호
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    • pp.111-117
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    • 2019
  • 본 논문은 경량 및 고효율 레큐퍼레이터를 구성하는 0.1 mm 이하의 두께를 지닌 전열판의 용접부에 대한 실험적 연구이다. 특히 해당 용접부에 대한 수명을 알아내기 위해 고온환경에서 피로특성을 실험을 통하여 알아내기로 하였다. 실험은 레큐퍼레이터의 소재로 주로 선정되는 두가지 재질에 대해 (STS347, AL20-25+nb) 실시하였으며, 시편은 실제 제작에 사용되는 방법과 ASTM에서 권고하는 규격을 준용하여 제작하였다. 그리고 상온과 고온에서 해당 시료의 기계적 특성을 평가하고자, 기계적 물성치를 시험하는 MTS-810 과 고온환경을 부여하기 위한 고온로를 이용하였다. 시험은 각 시편에 대해 상온 및 고온 환경에서 인장시험을 실시하였으며, 나타난 인장강도의 50%, 40%, 30%, 20% 그리고 10% 에 해당하는 하중을 응력비 0.1로 설정하여 피로시험을 시행하였다. 마지막으로 실험을 통해 나타난 피로수명 특성을 레큐퍼레이터의 운전조건에서 발생하는 하중에 따르는 응력과 비교하여 무인기 시스템이 요구하는 운전시간에 대비하여 해당 용접부들의 수명을 평가하였다.

D.C. Magnetron Sputter를 이용한 (Ti, Al)N 피막의 고온산화특성 (High Temperature Oxidation Characteristics of the (Ti, Al)N Coating on the STS 304 by D.C. Magnetron Sputtering)

  • 최장현;이상래
    • 한국표면공학회지
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    • 제25권5호
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    • pp.235-252
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    • 1992
  • (Ti, Al)N films were deposited on 304 stainless steel sheet by D.C. magnetron sputtering using Al target and Ti plate. The high temperature oxidation of (T, Al)N films with the variation of composition has been investigated. The chemical composition of (Ti, Al)N films with the variation of composition has been investigated. The chemical composition of (Ti, Al)N films was similar to the sputter area ratio of titanium to aluminum target by means of EDS and AES survey. The high temperature oxidation test of (Ti, Al)N showed that (Ti, Al)N has better high temperature resistance than TiN and TiC films. TiC films were cracked at 40$0^{\circ}C$ in air TiN films quickly were oxidised at $600^{\circ}C$, were spalled more than $700^{\circ}C$. But (Ti, Al)N films are relatively stable to$ 900^{\circ}C$. The good resistance to high temperature oxida-tion of (Ti, Al)N films are due to the formation of dense Al2O3 and TiO2 oxide layer. Especially, Al2O3 oxide layer is more important. The results obtained from this study show, it is believe that the (Ti, Al)N film by D.C. magnetron sputtering is promising for the use of high temperature and wear resistance mate-rials.

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Al 압출재 및 SUS 2층열차 차체의 강도해석 비교 검토 (The Strength Comparisons between Double deck Car body Structures with Al Extruded Panels and SUS)

  • 황원주;김형진;강부병;허현무
    • 한국철도학회:학술대회논문집
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    • 한국철도학회 2002년도 추계학술대회 논문집(II)
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    • pp.801-806
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    • 2002
  • The operation of double deck train have increased in many countries such as Japan france, and the Netherlands as efficient, safe and convenient alternative transportation systems. Because of continuous concentration of population into Seoul metropolitan and serious traffic jam, the number of passengers using the commuter train have been increased rapidly. Considering these situations, we can find one of the solutions for heavy traffic problems through double deck trains. Stainless steel, and aluminum extruded panel are used to reduce the weight of double deck train. In this paper we compare the results of structural analysis of the double deck car body structures with Al extruded panels and stainless steel. We hope the results of this study may be used as basic guidelines in designing double deck trains in the future.

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${Al}_{2}{O}_{3}$/304스트레인레스강 접합체 계면구조가 접합강도에 미치는 영향 (The Errect of Interfacial Structure on the Bonding Strength in ${Al}_{2}{O}_{3}$/304 Joint)

  • 김병무;강정윤;이상래
    • 한국재료학회지
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    • 제3권3호
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    • pp.282-291
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    • 1993
  • 첨가원소를 달리한 두 종류의 삽입금속 Cu-10tw% Ti합금과 Cu-7.5wt% Zr 합금을 사용하여 알루미나와 304 스테인레스강을 활성브레이징법으로 접합하였을 때 두 접합체 계면의 반응층생성구조를 비교조사하여 다으모가 같은 결과를 얻었다. Cu-10tw% Ti삽입금속을 사용한 접합체의 알루미나쪽 반응층은 단층구조를 이루고 있었으나 Cu-7.5wt% Zr삽입금속을 사용한 경우 반응층은 이중구조를 이루고 있었다. 이는 두 종류의 서로 다른 삽입금속이 용융상태에서 알루미나 표면에 갖는 젖음성(wettability)차이에 기인하는 것으로 사료되며 이러한 반응층의 생성구조는 접합강도에 지대한 영향을 미치는 것으로 확인되었다. Cu-10wt% Ti 삽입금속을 사용한 경우 모든 접합조건에서 열응력에 의한 모서리 균열(dege crack)이 관찰되었으나 Cu-7.5wt% Zr 삽입금속을 사용한 경우 적정 접합조건을 선정하면 반응층의 이중구조를 통애 열응력을 완화시킴으로써 균열발생을 억제하여 1323K $\times$ 0.6Ks의 접합조건에서 비교적 높은 약 86MPa의 전단강도값을 얻을 수 있었다.

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생체용 Ti-Zr-Pd계 합금의 양극분극특성 (Anodic Polarization Properties of Ti-Zr-Pd Based Alloys for Biomedical Applications)

  • 정종현
    • 대한치과기공학회지
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    • 제23권1호
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    • pp.21-30
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    • 2001
  • For biomedical applications. Ti-X%Zr-Y%Pd(X: $10{\sim}20$, Y:0.2 or 0.4) based alloys not containing harmful Al and V were newly designed, and polarization curves for their alloys were measured at $37^{\circ}C$ in 5% HCl solution in order to understand effects of Zr on the corrosion. From the results of anodic polarization behavior, it was found that the corrosion resistance increased with increasing Zr content. The results show their potential to develope Ti-based alloys for biomedical materials. The Ti-20%Zr-0.2%Pd alloy shows excellent corrosion resistance and was superior to those of the Ti. Ti-6%Al-4%V ELI alloy, Co-30%Cr-6%Mo alloy and STS 316L stainless steel.

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분말시스압연법에 의한 CNT 강화 Al기 복합재료의 제조 및 평가 (Fabrication and Evaluation of Carbon Nanotube Reinforced Al Matrix Composite by a Powder-in-sheath Rolling Method)

  • 이성희;홍동민
    • 한국분말재료학회지
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    • 제21권1호
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    • pp.50-54
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    • 2014
  • A powder-in-sheath rolling method was applied to a fabrication of a carbon nano tube (CNT) reinforced aluminum composite. A STS304 tube with an outer diameter of 34 mm and a wall thickness of 2 mm was used as a sheath material. A mixture of pure aluminum powders and CNTs with the volume contents of 1, 3, 5 vol was filled in the tube by tap filling and then processed to 73.5% height reduction by a rolling mill. The relative density of the CNT/Al composite fabricated by the powder-in-sheath rolling decreased slightly with increasing of CNTs content, but exhibited high value more than 98. The grain size of the aluminum matrix was largely decreased with addition of CNTs; it decreased from $24{\mu}m$ to $0.9{\mu}m$ by the addition of only 1 volCNT. The average hardness of the composites increased by approximately 3 times with the addition of CNTs, comparing to that of unreinforced pure aluminum. It is concluded that the powder-in-sheath rolling method is an effective process for fabrication of CNT reinforced Al matrix composites.