• 한국축산식품학회지
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• 제34권6호
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• pp.749-756
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• 2014

A rapid and simple analytical method for L-carnitine was developed for infant and toddler formulas by liquid chromatography tandem mass spectrometry (LC-MS/MS). A 0.3 g of infant formula and toddler formula sample was mixed in a 50 mL conical tube with 9 mL water and 1 mL 0.1 M hydrochloric acid (HCl) to chemical extraction. Then, chloroform was used for removing a lipid fraction. After centrifuged, L-carnitine was separated and quantified using LC-MS/MS with electrospray ionization (ESI) mode. The precursor ion for L-carnitine was m/z 162, and product ions were m/z 103 (quantitative) and m/z 85 (qualitative), respectively. The results for spiked recovery test were in the range of 93.18-95.64% and the result for certified reference material (SRM 1849a) was within the range of the certificated values. This method could be implemented in many laboratories that require time and labor saving.

• 통합자연과학논문집
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• 제7권4호
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• pp.241-252
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• 2014

A series of N-benzoylated ligands incorporating three different benzoyl groups 2,2'-(benzoyliminodiethylene)-4-substituted phenols ($L^{1,4,7}$), 2,2'-(4-nitrobenzoyliminodiethylene)-4-substituted phenols ($L^{2,5,8}$) and 2,2'-(3,5-dinitrobenzoyliminodiethylene)-4-substituted phenols ($L^{3,6,9}$) were synthesized and characterized by IR, $^1H$ NMR, $^{13}C$ NMR and mass spectroscopy. The In vitro antibacterial activity of investigated ligands were tested against human pathogenic bacteria such as four Gram (-) Enterococcus faecalis, Pseudomonas aeruginosa, Staphylococcus aureus, Vibrio cholera, Vibrio harveyi and two Gram (+) Staphylococcus aureus, Streptococcus mutans. Furthermore, docking studies were undertaken to gain insight into the possible binding mode of these compounds with the binding site of the topoisomerase II (PDB: 4FM9) enzyme which is involved in DNA superhelicity and chromosome seggregation. The N-benzoylated derivatives $L^{5,7,8}$ have significant anticancer activity as Topoisomerase inhibitors. The ligands $L^5$ and $L^8$ were tested for their anticancer activity against human liver adenocarcinoma (HepG2) cell line with the MTT assay.

• Bulletin of the Korean Chemical Society
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• 제25권8호
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• pp.1156-1160
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• 2004

The technique of an on-line preconcentration by the direct sulfide precipitation has been developed. Sn was homogeneously precipitated by sulfide, which was generated in situ from the hydrolysis of thioaceteamide. Precipitate was collected on a filter in the line and dissolved out instantaneously by KOH to be sent to an ICP. The enrichment factor was 4 with the sampling speed of 15/hr for 1.0 mL of sample. It was increased to more than 40 times when the sampling volume was increased to 10 mL with the sampling speed of 5/hr. $Sn^{2+}/Sn^{4+}$ could be separately determined with the on-line precipitation technique. The method was applied to the analysis of NIST SRM 1566 Oyster sample and yielded good agreement with the certified value.

• 한국정보처리학회:학술대회논문집
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• 한국정보처리학회 2016년도 춘계학술발표대회
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• pp.10-13
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• 2016

정부는 K-ICT 클라우드 활성화를 위해 정부 3.0 클라우드 추진 계획을 발표하고 관련 제도와 법률을 제정하여 클라우드 서비스 도입을 위한 정책을 추진하고 있다. 그러나 공공 분야의 클라우드 컴퓨팅 도입은 기존의 법률, 제도, 관행의 통제로 인해 미미한 실정이다. 공공 기관의 클라우드 컴퓨팅 도입 활성화를 위해 중요한 부분은 클라우드 컴퓨팅의 성능과 품질 등에 대한 특성을 파악하는 것이다. 클라우드 컴퓨팅의 특성을 알아야만 적격의 클라우드 컴퓨팅 사업자 선정이 가능하게 된다. 유럽 연합(European Commission)에서는 클라우드 컴퓨팅의 특성을 서비스 성능과 품질에 대한 일반특성, 기술성, 경제성으로 분류하고 있다. 그러나 클라우드 도입을 위한 설계 시 공공 기관 담당자는 클라우드 특성의 각 부문별 하위 항목에 대한 상세한 내용과 수준까지 객관적으로 평가하기 어렵다. 이러한 문제를 해결하고자 본 연구는 클라우드 컴퓨팅의 성능과 품질 및 기술 특성을 파악하여 각 특성에 대한 가중치를 구하고 우선순위 측정을 통해 사업자 선정을 위한 평가 기준으로 적용하는 기법을 제안한다.

• Advances in Energy Research
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• 제6권2호
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• pp.145-160
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• 2019

The world population reaches to about 7.7 billion in 2018 from 6.2 billion in 2000. This much growth in population results in increased energy demand and increased food supply. As the conventional energy sources are limited. These may deplete soon if consumed at this rate. So, the world is switching towards the utilization of non-conventional sources of energy. Energy from sun is the best method as it can not only solve the energy issue but also helps in meeting food demand by conserving it. Greenhouses are made for the purpose of food conservation. Various types of solar dryers are developed by researchers till now and still the effort is being putted to make them more efficient. Hybrid greenhouse is also effort toward utilization of solar energy in more efficient way. The paper presents the heat and mass transfer analysis of hybrid greenhouse solar dryer developed by different researchers till now. The review helps the researcher in understanding the heat and mass transfer taking place inside the hybrid greenhouse and how it can be further improved.

• Journal of international Conference on Electrical Machines and Systems
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• 제1권1호
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• pp.47-53
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• 2012

A novel 6/5 switched reluctance motor (SRM) with short flux path is presented in this paper. The concept of this proposed motor is a novel SR motor with six stator and five rotor poles. The stator is constructed with three independent and physically separate C-core segments, and the rotor is composed of five poles. This motor, with a new selection for the number of stator/rotor poles, achieves a short flux path, which reduces the magnetomotive force required to drive the motor. To verify the performance of the proposed motor, a comparison with conventional SR motors with the same dimensions is executed. The comparison demonstrates that the proposed motor offers better performance in terms of maximum torque production. Furthermore, Finite Element Analysis (FEA) and Matlab/Simulink software are used to predict and simulate the performance of the proposed motor.

• Bulletin of the Korean Chemical Society
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• 제31권12호
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• pp.3663-3667
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• 2010

Acetaminophen (N-acetyl-p-aminophenol) is one of the most popular analgesic and antipyretic drugs. An isotope dilution mass spectrometric method based on LC/MS was developed as a candidate reference method for the accurate determination of acetaminophen in pharmaceutical product. After spiking an isotope labeled acetaminophen (acetyl-$^{13}C_2$, $^{15}N$-acetaminophen) as an internal standard, tablet extracts were analyzed by LC/MS in a selected reaction monitoring (SRM) mode to detect ions at m/z $152{\rightarrow}110$ and m/z $155{\rightarrow}111$ for acetaminophen and acetyl-$^{13}C_2$, $^{15}N$-acetaminophen, respectively. The repeatability and reproducibility of the developed ID/LC-MS method were tested for the validation and assessment of metrological quality of the method.

• Environmental Engineering Research
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• 제18권1호
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• pp.3-8
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• 2013

Collision cell technology-inductively coupled plasma-mass spectrometry (CCT-ICP-MS) was used to measure the concentrations of approximately 19 elements associated with airborne PM2.5 samples that were collected from a roadside sampling station in Daejeon, Korea. Standard reference material (SRM 2783, air particulate on filter media) of the National Institute of Standards and Technology was used for the quality assurance of CCT-ICP-MS. The elemental concentrations were compared statistically with the certified (or recommended) values. The patterns of distribution were clearly distinguished between elements with their concentrations ranging over four orders of magnitude. If compared in terms of enrichment factors, it was found that toxic trace elements (e.g., Sb, Se, Cd, As, Zn, Pb, and Cu) of anthropogenic origin are much more enriched in PM2.5 samples of the study site. To the contrary, the results of the correlation analysis showed that PM2.5 concentrations can exhibit more enhanced correlations with the elements (e.g., Fe, K, Si, and Ti) arising from earth's crust. The findings of strong correlations between PM2.5 and the elements of crustal origin may be directly comparable with the dominant role of those species by constituting a major fraction of even PM2.5 as well as PM10 at the roadside area.

• 조명전기설비학회논문지
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• 제23권6호
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• pp.89-95
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• 2009

최근에는 파워툴(power tools)과 가전 제풀에 있어서 전자적인 전류(commutation)를 사용하는 새로운 형태의 브러시리스 전동기인 플럭스 스위칭 전동기(Flux switching motor)에 대한 관심이 점차적으로 증가되고 있으며, 특히 팬과 펌프 시장에 있어서는 그린 정책으로 인하여 플럭스 스위칭 전동기에 대한 관심이 급격히 증가되고 있다. 플럭스 스위칭 전동기는 유도전동기에 비해서는 높은 전력 밀도(power density)와 상대적으로 높은 효율, 그리고 브러시리스 DC 전동기에 비해서는 간단한 전동기 구조와 가격 경쟁력이라는 장점을 가지고 있다. 따라서 본 논문에서는 팬 용도로 제작된 12/6 폴을 가지는 플럭스 스위칭 전동기의 드라이브 설계와 동작원리에 대해서 나타내고, 팬 용도로 제작된 프로토타입 플럭스 스위칭 전동기의 타당성을 검증하기 위해서 IMS320F2812 DSP와 일반적인 인버터를 이용한 실험 결과를 제시한다.

• 전력전자학회논문지
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• 제12권1호
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• pp.74-80
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• 2007

본 논문에서는 2상 여자 방식으로 구동하는 전압형 인버터 스위치에 발생한 개방 고장을 검출하는 기법을 제안한다. 제안된 기법은 인버터 각 상의 하단 스위치에 전압 센서를 사용하여 동작 모드에 따라 개방 고장을 판별한다. 이는 구현이 간단하고 빠른 고장 판별이 가능하며 부하의 영향을 거의 받지 않기 때문에, 시스템의 신뢰성을 향상시킨다. 또한 4-스위치 인버터 구동을 적용한 재구성을 통하여 고장 발생시에도 고장의 영향을 최소화 하면서 연속적인 운전을 가능하게 했다. 제안된 고장 검출 알고리즘의 타당성은 실험결과로 검증한다.