• 제목/요약/키워드: SEM morphology

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승화법으로 성장된 AlN 결정의 성장 양상에 관한 연구 (A study on the growth morphology of AlN crystals grown by a sublimation process)

  • 강승민
    • 한국결정성장학회지
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    • 제19권5호
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    • pp.242-245
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    • 2009
  • 종자결정을 사용하지 않고 AlN 결정을 승화법으로 성장하였으며, 결정이 성장되는 양상을 고찰하였다. AlN 결정으로 성장된 상은 다결정 상이었으며, 약 $60\sim160\;{\mu}m$의 크기를 가졌으며, $0.2\sim0.5\;{\mu}m/hr$의 성장 속도로 성장되었다. 성장된 결정구조는 AlN 결정의 결정 구조가 반영된 육방정계의 결정상으로 성장되었음을 관찰하였으며, 주상 구조(columnar structure)로 성장된 후 횡적 성장(lateral growth)하는 양상을 보이면서 대형화됨을 알 수 있었다. 성장된 결정의 표면에서는 다량의 pinhole이 관찰되었으며, 광학현미경과 SEM을 이용하여 성장 morphology의 변화과정을 고찰하였다.

Salix viminalis의 화분형태(花粉形態)에 관(關)한 연구(硏究) (A Contribution to the Pollen Morphology of Salix viminalis L.)

  • 김계환
    • 한국산림과학회지
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    • 제66권1호
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    • pp.64-67
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    • 1984
  • 버드나무속(屬)은 최근(最近) 바이오매스 측면(側面)의 에너지 생산(生産)과 제지산업(製紙産業) 등(等)에 그 중요성(重要性)이 증가(增加)되고 있으며 유전적(遺傳的)인 개량(改良)과 화분(花粉) 알레르기의 예방(豫防) 연구(硏究) 등(等)에 화분형태(花粉形態)의 조사(調査)가 요구(要求)되는 바 Salix viminalis의 화분형태(花粉形態)에 관(關)하여 광학현미경(光學顯微鏡)과 주사형(走査型) 전자현미경(電子顯微鏡)으로 조사(調査)하였다.

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Dyeing Study on DMF-Modified Polyesters for Morphology Characterization

  • Park, Myung-Ja
    • The International Journal of Costume Culture
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    • 제5권2호
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    • pp.53-65
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    • 2002
  • Morphology of polyester fiber was physically modified by solvent treatment. PET fiber was treated with N,N-dimethylformamide (DMF) at 100, 120, $140^{circ}C$ for 10 minutes without tension. The structural changes in the morphology of DMF-induced modified PET fiber were FTIR and SEM analysis. Also dyeing behavior of DMF-treated polyester fibers with various disperse dyes was studied to detect changes of amorphous area in fine structure. DMF treatment resulted in increases in total void content, degree of crystallinity, trans isomer content, chain folding, segmental mobility and molecular packing, but it resulted in decreases in amorphous orientation, intermolecular forces and individual void size through longitudinal shrinkage, lateral welling and removal of oligomers. Void-size distribution could be estimated from the dye uptake with various sizes of disperse dyes. In contrast to the large increases in dye uptake with small dye molecules, there is no and little dye uptake with the bulkiest dye, which means that void size is bigger or smaller than the volume of each dye. Diffusion rates of dye molecules showed increases. This dyeing study revealed that the disperse dyeing is very effective method for characterizing the internal morphology of polyester fiber.

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Magnesium Thin Films Possessing New Corrosion Resistance by RF Magnetron Sputtering Method

  • Lee, M.H.;Yun, Y.S.;Kim, K.J.;Moon, K.M.;Bae, I.Y.
    • Corrosion Science and Technology
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    • 제3권4호
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    • pp.148-153
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    • 2004
  • Magnesium thin flims were prepared on cold-rolled steel substrates by RF magnetron sputtering technique. The influence of argon gas pressure and substrate bias voltage on their crystal orientation and morphology of the coated films were investigated by scanning electron microscopy (SEM) and X-ray diffraction, respectively. And the effect of crystal orientation and morphology of magnesium films on corrosion behaviors was estimated by measuring anodic polarization curves in deaerated 3%NaCl solution. From the experimental results, all the sputtered magnesium films showed obviously good corrosion resistance to compare with 99.99% magnesium target of the sputter-evaporation metal. Finally it was shown that the Corrosion-resistance of magnesium films can be improved greatly by controlling the crystal orientation and morphology with effective use of the plasma sputtering technique.

Structural Transcription of Organogels to Mesoporous Silicas: A Chain-length Dependent Morphology and Pore Texture

  • Huang, Yaqun
    • Bulletin of the Korean Chemical Society
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    • 제33권11호
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    • pp.3711-3718
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    • 2012
  • Here, we report a chain-length dependent morphology and pore structure tailing of mesoporous silica templated from organogels, which is formed by primary alkylamine and ethylene glycol at room temperature. As the chain length of alkylamine changes from 12 to 18, the resulted materials exhibit a morphology change from layers to spheres and platelets, respectively. SEM and TEM observation revealed that these shapes appear to be inherited from their parent organogels. Further pore structure characterization by nitrogen sorption analysis demonstrates that all the resulted silicas exhibit typical IV isotherms indicative of uniform mesopores, and their pore sizes are dependent on the chain length of alkylamine used.

Morphological transformations during drying of surfactant-nanofluid droplets

  • Osman, Abdulkadir;Shahidzadeh, Noushine;Stitt, Hugh;Shokri, Nima
    • Journal of Industrial and Engineering Chemistry
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    • 제67권
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    • pp.92-98
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    • 2018
  • The effect of surfactants with different chain length on the drying dynamics of nanosized dispersion droplets and on the final morphology of the grains formed after water evaporation is investigated experimentally. An acoustic levitator was used to examine the drying dynamics of single droplets and SEM imaging was used to characterise the morphology of the final dried grains. Results show that the drying of drops with high molecular weight surfactants leads to more irregular grains and that the grain morphology is related to surface tension driven instability of the evaporating droplets which may lead to formation of hollow dried grains.

Morphology of the Gastric Mill of Nyctiphanes australis(Euphausiacea, Crustacea)

  • SUH Hae-Lip
    • 한국수산과학회지
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    • 제22권4호
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    • pp.214-218
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    • 1989
  • SEM observation revealed that the gastric mill of Nyctiphanes australis consists of paired cluster spines and paired lateral teeth, while the filter-press is absent. The morphology of the gastric mill was extremely constant; the numbers of both setiform processes of cluster spines and serrated spines of lateral teeth increased with increasing body length. The cluster spines of N. australis consisted of a single row of stout setiform processes but the lateral teeth comprised a large projection with small serrated spines. The cluster spines are symmetrical in setiform process distribution, however, the lateral teeth are asymmetrical in number of serrated spines.

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강도래과(강도래목) 2 종에 대한 성충 및 란의 외부형태 관찰 (Observation of the Adults and Eggs of Two Species of the Family Perlidae(Plecoptera) to Korea)

  • 나철호;백순기;조영관
    • Animal Systematics, Evolution and Diversity
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    • 제7권1호
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    • pp.101-110
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    • 1991
  • 1989년과 1990년의 봄철에 전남,북과 경남일원의 신간계류에서 채집된 강도래 과의 Oyamia coreana Okamoto와 Kiotina decorata(Zwick) 2종에 대한 성충의 외부형태와 난의 전자현미경에 의한 미세구조 관찰을 실시하였다.

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Relationship between the maxillofacial skeletal pattern and the morphology of the mandibular symphysis: Structural equation modeling

  • Ahn, Mi So;Shin, Sang Min;Yamaguchi, Tetsutaro;Maki, Koutaro;Wu, Te-Ju;Ko, Ching-Chang;Kim, Yong-Il
    • 대한치과교정학회지
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    • 제49권3호
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    • pp.170-180
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    • 2019
  • Objective: The purpose of this study was to investigate the relationship between the facial skeletal patterns and the shape of the mandibular symphysis in adults with malocclusion by using a structural equation model (SEM). Methods: Ninety adults who had malocclusion and had records of facial skeletal measurements performed using cone-beam computed tomography were selected for this study. The skeletal measurements were classified into three groups (vertical, anteroposterior, and transverse). Cross-sectional images of the mandibular symphysis were analyzed using generalized Procrustes and principal component (PC) analyses. A SEM was constructed after the factors were extracted via factor analysis. Results: Two factors were extracted from the transverse, vertical, and anteroposterior skeletal measurements. Latent variables were extracted for each factor. PC1, PC2, and PC3 were selected to analyze the variations of the mandibular symphyseal shape. The SEM was constructed using the skeletal variables, PCs, and latent variables. The SEM showed that the vertical latent variable exerted the most influence on the mandibular symphyseal shape. Conclusions: The relationship between the skeletal pattern and the mandibular symphysis was analyzed using a SEM, which showed that the vertical facial skeletal pattern had the highest effect on the shape of the mandibular symphysis.