• Title/Summary/Keyword: SEM : scanning electron microscope

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Lignin Degradation of Pine Wood by Unidentified Decay Fungi and Observation by Scanning Electron Microscope (미동정 부후균에 의한 소나무재의 Lignin 분해와 주사전자현미경(SEM)을 이용한 관찰)

  • Park, Heon;Min, Kyeong-Heui
    • Journal of the Korean Wood Science and Technology
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    • v.31 no.4
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    • pp.71-80
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    • 2003
  • The lignin degrading fungi were isolated from decayed woods and fruiting bodies gathered in forest area. Lignin degradation ability was investigated by Klason lignin of microbial treated pine wood. Among selected fungi, CJ-6 had 49.48% Klason lignin loss which was greater than 40.58% shown by Trametes versicolor that it is known as a typical lignin degrading fungus. Also, the biodegradation process and morphological features of degraded pine wood by selected fungi were observed with the scanning electron microscope. At the stage of 20 days incubation, mycelia invasion was observed without any failure of wood structure. At 60 days, wood decay was gone in some degree and one part of tracheid and ray wall was destroyed. At 100 days, tracheid wall was severely destroyed, and distinction between ray cell was difficult as cell wall was decayed much.

Durability Test and Micro-Damage Formation of Rubber Hose for Automotive Hydraulic Brake (자동차 유압브레이크용 고무호스의 내구성 시험 및 미세손상에 관한 연구)

  • Kwak, Seung-Bum;Choi, Nak-Sam;Lim, Young-Han
    • Composites Research
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    • v.21 no.1
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    • pp.40-45
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    • 2008
  • Rubber hose assembly for automotive hydraulic brake during operation is subject to combined stresses of cyclic pressure, cyclic bending and torsion as well as thermal load. The rubber hose is composed of ethylene-propylene diene monomer(EPDM) rubber layers reinforced by polyvinyl acetate(PVA) braided fabrics. A durability tester with loading rigs for inducing the above cyclic stresses was used to investigate failure mechanisms in the rubber hose assembly. Failure examination was performed at every 100 thousands cycles of bending and torsion. Hose samples were sectioned with a diamond-wheel cutter and then polished. The polished surface was observed by optical microscope and scanning electron microscope (SEM). Some interfacial delamination with a length of about 1mm along the interface between EPDM rubber and PVA fabrics was shown at the test cycles of 400,000. The delamination induced some cracking into the outer rubber skin layer to leading the final rupture of the hose.

Tensile Properties of Hybrid Fiber-Reinforced Reactive Powder Concrete After Exposure to Elevated Temperatures

  • Li, Haiyan;Liu, Gang
    • International Journal of Concrete Structures and Materials
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    • v.10 no.1
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    • pp.29-37
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    • 2016
  • The paper presents a research project on the tensile properties of RPC mixed with both steel and polypropylene fibers after exposure to $20-900^{\circ}C$. The direct and the indirect tensile strength (in bending) were measured through tensile experiment on dog-bone specimens and bending experiment on $40{\times}40{\times}160mm$ prisms. RPC microstructure was analyzed using scanning electron microscope. The results indicate that, steel fibers can significantly improve the tensile performance of hybrid fiber-reinforced RPC, whereas polypropylene fibers have no obvious effect on the tensile performance. With increasing temperature, the flexural and axial tensile strength of hybrid fiber-reinforced RPC substantially decrease linearly, which attributes to the deteriorating microstructure. Based on the experimental results, equations are established to express the decay of the flexural and tensile strength with increasing temperature.

A Study on the Residual Stress and Microstructure of Autofrettaged SCM440 High Strength Steel (자긴가공된 SCM440 고강도강의 잔류응력 및 미세구조 분석에 관한 연구)

  • Kim, J.H.;Shim, W.S.;Lee, Y.S.;Cha, K.U.;Hong, S.K.
    • Proceedings of the KSME Conference
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    • 2008.11a
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    • pp.311-316
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    • 2008
  • Thick-walled cylinders, such as a cannon or nuclear reactor, are autofrettaged to induce advantageous residual stresses into pressure vessels and to increase operating pressure and the fatigue lifetimes. As the autofrettage level increases, the magnitude of compressive residual stress at the bore also increases. The purpose of the present paper is to predict the accurate residual stress of SCM440 high strength steel using the Kendall model which was adopted by ASME Code. Hydraulic pressure process was applied and thick-walled cylinders were autofrettaged up to 30% overstrain levels. Electro polishing was performed to get more accurate data. Residual stresses were measured by X-ray diffraction method. The autofrettaged surface which was plastically deformed analyzed using a scanning electron microscope(SEM). Although there were some differences in measured residual stress and numerical, there is a tendency to agree.

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Behavior of elastomer TPVs' Mechanical Properties According to Injection Molding Conditions (엘라스토머 TPV의 사출성형조건에 따른 기계적 물성)

  • Han S. R.;Kim J. H.;Jeon S. G.;Lee G. H.;Jeong Y. D.
    • Proceedings of the Korean Society for Technology of Plasticity Conference
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    • 2005.10a
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    • pp.265-268
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    • 2005
  • Thermoplastic elastormer (TPE) has many advantages such as high flexibility, high elasticity and high elongation, etc. TPE is easily molded such as plastic materials, therefore, many TPE parts are applied as home appliances and mechanical parts. However, if TPE is once molded, its mechanical properties are changed by injection molding conditions such as melt temperature, mold temperature, injection pressure and holding pressure, etc. In this study, the influences of the injection molding condition on the mechanical properties of thermoplastic vulcanizates(TPVs), which is one of the TPE, were investigated. By the injection molding experiment, as increasing the melt temperature, the tensile strength, shrinkage and hardness decreased. By the scanning electron microscope (SEM) analyzing the TPVs' crystallization, the morphology was affected by the melt temperature.

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The Tissue Types of Stroma in Some Species of Hypoxylon (Hypoxylon속 자낭자좌 조직의 형태 연구)

  • Lee, Yang-Soo
    • Applied Microscopy
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    • v.27 no.4
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    • pp.453-460
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    • 1997
  • The tissue types of stromata were observed intensively in four species of Hypoxylon under a scanning electron microscope (SEM). These stromata were sectioned with a freezing fracture method for observation. Several tissue types were recognized and stable in each species. This study presents the most intensive observation of tissue types of each layer of stromata. It will be useful for taxonomic criteria for the species level. However, the tissue types can not be major taxonomical criteria for the genus Hypoxylon.

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A Study on the Dielectric Properties of Silicone Rubber due to Hardness Variation (경도 변화에 따른 실리콘 고무의 유전 특성에 관한 연구)

  • Lee, Sung-Ill
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.25 no.11
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    • pp.916-921
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    • 2012
  • This research measured the dielectric properties of silicone rubber with various hardness in 100 Hz~3 MHz, $30{\sim}170^{\circ}C$ conditions. When the hardness increases from 65 degree to 75 degree, the dielectric loss increased within frequency range of 100 kHz~3 MHz and was a little change in dielectric loss within temperature range of $90^{\circ}C{\sim}170^{\circ}C$. Thermogravimetric Analysis (TGA) showed the weight change rate increased a little while heated until $800^{\circ}C$. Scanning Electron Microscope (SEM) measurement showed that Aluminium Trihydroxide($AlOH_3$) which acts as a reinforcement agent reduced the size of the particles as the hardness increased.

Performance of Al-Zn Coating by Arc Thermal and Plasma arc Thermal Spray Processes in 3.5% NaCl Solution (3.5% NaCl에서 Arc Thermal and Plasma Arc Spray 공법이 적용된 Al- Zn 코팅 강재의 내 식 성능 평가에 관한 연구)

  • Jannat, Adnin Raihana;Lee, Han-Seung
    • Proceedings of the Korean Institute of Building Construction Conference
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    • 2021.11a
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    • pp.17-18
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    • 2021
  • In the present study, Al-Zn coating was deposited by Arc thermal (AT) and plasma arc thermal (PAT) spray processes, and their corrosion characteristics were studied in 3.5% NaCl through electrochemical impedance spectroscopy (EIS), scanning electron microscope (SEM) and mechanical tests. The bond adhesion result showed that plasma arc sprayed coating had a higher value attributed to compact, dense, and less porous coating compared to arc thermal spray coating which contains defects/pores and uneven morphology as revealed by scanning electron microscope analysis. Electrochemical results revealed that the plasma arc sprayed coating had a high polarization resistance at early stage of immersion, suggesting its excellent corrosion protection performance.

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Synthesis and Self-healing Properties of Waterborne Polyurethane Based on Polycarbonate and Polyether Polyol (폴리카보네이트계 및 폴리에테르계 폴리올 기반 자가치유 기능 수분산 폴리우레탄 합성과 특성)

  • Kwon, Seon-Young;Park, Soo-Yong;Paik, In Kyu;Chung, Ildoo
    • Journal of Adhesion and Interface
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    • v.23 no.1
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    • pp.8-16
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    • 2022
  • In this study, self-healable waterborne polyurethane (SH-WPU) as shoes and coating materials with self-healable disulfide functionalities was synthesized by mixing polyether polyol to impart excellent durability and heat resistance and polycarbonate polyol to impart excellent mechanical properties. The synthesized SH-WPU was characterized by fourier transform-infrared spectroscopy (FT-IR), and physical and self-healing properties were confirmed through universal testing machine (UTM) and scanning electron microscope (SEM) measurements. Tensile strength and hardness were increased and elongation was decreased by using polycarbonate polyol. In addition, as a result of comparison of thermal properties, thermal stability has been increased as the content of polycarbonate polyol increased. The healing efficiency showed the highest efficiency when poly(tetramethylene ether)glycol : polycarbonate polyol = 0.75 : 0.25, and it was confirmed that the damaged part was healed through surface observation using a microscope and SEM.