• Title/Summary/Keyword: Room temperatures

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Fabrication and Characterization of TiNi Shape Memory Alloy Fiber Reinforced 6061 Aluminum Matrix Composite by Using Hot Press (핫프레스법에 의한 TiNi/Al6061 형상기억복합재료의 제조 및 기계적 특성에 관한 연구)

  • Park, Dong-Sung;Lee, Jun-Hee;Lee, Guy-Chang;Park, Young-Chul
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.26 no.7
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    • pp.1223-1231
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    • 2002
  • Al alloy matrix composite with TiNi shape memory fiber as reinforcement has been fabricated by hot pressing to investigate microstructures and mechanical properties. The analysis of SEM and EDS showed that the composites have shown good interface bonding. The stress-strain behavior of the composites was evaluated at temperatures between 363K and room temperature as a function of prestrain, and it showed that the yield stress at 363K was higher than that of the room temperature. Especially, the yield stress of this composite increases with increasing the amount of prestrain, and it also depends on the volume fraction of fiber and heat treatment. The smartness of the composite is given due to the shape memory effect of the TiNi fiber which generates compressive residual stress in the matrix material when heated after being prestrained. Microstructural observation has revealed that interfacial reactions occur between the matrix and fiber, creating two intermetallic layers.

A Study on the Superplasticity of Zn-Al Alloy using Dynamic Materials Model (동적재료모델을 이용한 Zn-Al 합금의 초소성 변형거동 연구)

  • Jung, J.Y.;Ha, T.K.;Chang, Y.W.
    • Transactions of Materials Processing
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    • v.18 no.4
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    • pp.317-322
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    • 2009
  • Superplastic deformation behavior of a Zn-0.3 wt.% Al was investigated. Grain sizes of $1{\mu}m$ and $10{\mu}m$ were obtained by a thermomechanical treatment. A series of load relaxation and tensile tests were conducted at various temperatures ranging from RT ($24^{\circ}C$) to $200^{\circ}C$. A large elongation of 1400% was obtained at room temperature in the specimens with the grain size of $1{\mu}m$. In the case of specimens with the grain size of $10{\mu}m$, relatively lower elongation at room temperature was obtained and, as the temperature increases above $100^{\circ}C$, a high elongation of about 400 % has been obtained at $200^{\circ}C$ under the strain rate of $2{\times}10^{-4}/s$. Dynamic materials model (DMM) has been employed to explain the contribution from GBS of Zn-Al alloy. Power dissipation efficiency for GBS was evaluated as above 0.4 and found to be very close to the unity as strain rate decreased and temperature increased, suggesting that GBS could be regarded as Newtonian viscous flow.

Fracture Toughness Embrittlement by Hydride in Zr-2.5Nb Pressure Tube (Zr-2.5Nb 압력관의 수화물에 의한 파괴인성 취화에 관한 연구)

  • Oh, Dong-Joan;Ahn, Sang-Bok;Park, Soon-Sam;An, Chang-Yun;Kim, Young-Suk
    • Proceedings of the KSME Conference
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    • 2000.11a
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    • pp.93-98
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    • 2000
  • Unpredictable failures can occur due to the DHC (delayed hydride cracking) or the degradation of fracture toughness by hydride embrittlement in CANDU pressure tube which can result from the absorption of hydrogen or deuterium in the high temperature coolant. To investigate the hydride embrittlement of CANDU Zr-2.5Nb pressure tube, the transverse tensile test and the fracture toughness test were performed from room temperature to $300^{\circ}C$ using three different specimens which have an AR (As Received), 100, and 200 ppm hydrogen. As the amount of absorbed hydrogen was increased, the transverse yield strength and the ultimate tensile strength were also increased. In addition, as the test temperature became higher they were decreased linearly. While, at room temperature, the hydrogenbsorbed specimens represented the embrittlement which resulted in sudden decreasing of fracture toughness, the fracture characteristics became ductile such as AR specimen at high temperatures. Through the observation of fracture surface using SEM, it was found that the stress state of mixed mode could be related to the fissure which was believed to decrease the global fracture toughness.

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Microstructure and Elevated Temperature Strength of W-ZrC Composites with Micrometric and Nanosized ZrC Particles (서로 다른 입자크기의 ZrC가 첨가된 W-ZrC 복합체의 미세구조 및 고온강도에 관한 연구)

  • Han, Yoon Soo;Ryu, Sung-Soo
    • Journal of Powder Materials
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    • v.21 no.6
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    • pp.415-421
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    • 2014
  • W-10vol.%ZrC composites reinforced by micrometric and nanosized ZrC particles were prepared by hot-pressing of 25 MPa for 2 h at $1900^{\circ}C$. The effect of ZrC particle size on microstructure and mechanical properties at room temperature and elevated temperatures was investigated by X-ray diffraction analysis, scanning electron microscope and transmission electron microscope observations and the flexural strength test of the W-ZrC composite. Microstructural analysis of the W-ZrC composite revealed that nanosized ZrC particles were homogeneously dispersed in the W matrix inhibiting W grain growth compared to W specimen with micrometric ZrC particle. As a result, its flexural strength was significantly improved. The flexural strength at room temperature for W-ZrC composite using nanosized ZrC particle being 740 MPa increased by around 2 times than that of specimen using micrometric ZrC particle which was 377 MPa. The maximum strength of 935 MPa was tested at $1200^{\circ}C$ on the W composite specimen containing nanosized ZrC particle.

Effect of Natural Antioxidant Sources on Oxidation of Olive Flounder (Paralichthys olivaceus) and Fish Feed during Storage

  • Cho, Sung-Hwoan
    • Fisheries and Aquatic Sciences
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    • v.13 no.3
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    • pp.231-235
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    • 2010
  • The effects of various natural antioxidant sources on oxidation of olive flounder (Paralichthys olivaceus) and fish diet during storage was determined. Juvenile fish were distributed among 18 flow-through tanks (40 fish per tank). Six experimental diets were prepared in triplicate: control (CT), antitox (AT), green tea extract (GE), fig extract (FE), Haeroc product (HP) and by-product of green tea (BG). The experimental diets were stored at two temperatures: room temperature ($26.8^{\circ}C$) for 14 days and frozen ($-30^{\circ}C$) for 16 weeks. Thirty fish were sampled from each tank at the end of the 8-week feeding trial. Whole bodies of fish were homogenized and stored in a home freezer ($-9.6^{\circ}C$) for 24 weeks. Acid values (AVs) and peroxide values (POVs) of the diets and frozen fish during storage were monitored. AVs of the experimental diets tended to increase with the storage period except for that of the HP diet at room temperature. POVs from FE, CT, and BG diets peaked at day 7 and then decreased through the remainder of the experiment. AVs of the experimental diets and fish increased with time at $-30^{\circ}C$ and $-9.6^{\circ}C$. Results of this study show that by-products of green tea and Haeroc product seem to have potential as antioxidants in fish feed to inhibit oxidation of both the feed and fish during storage.

A New Way to Prepare MoO3/C as Anode of Lithium ion Battery for Enhancing the Electrochemical Performance at Room Temperature

  • Yu, Zhian;Jiang, Hongying;Gu, Dawei;Li, Jishu;Wang, Lei;Shen, Linjiang
    • Journal of Electrochemical Science and Technology
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    • v.7 no.2
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    • pp.170-178
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    • 2016
  • Composited molybdenum oxide and amorphous carbon (MoO3/C) as anode material for lithium ion batteries has been successfully synthesized by calcining polyaniline (PANI) doped with ammonium heptamolybdate tetrahydrate (AMo). The as prepared electrode material was characterized by X-ray diffraction (XRD), Fourier transform infrared spectroscopy (FT-IR) and field emission scanning electron microscopy (FE-SEM). The electrochemical performance of the anode was investigated by galvanostatic charge/discharge, cyclic voltammetry (CV), and electrochemical impedance spectroscopy (EIS). The MoO3/C shows higher specific capacity, better cyclic performance and rate performance than pristine MoO3 at room temperature. The electrochemical of MoO3/C properties at various temperatures were also investigated. At elevated temperature, MoO3/C exhibited higher specific capacity but suffered rapidly declines. While at low temperature, the electrochemical performance was mainly limited by the low kinetics of lithium ion diffusion and the high charge transfer resistance.

Preservation of Takju by Pasteurization (저온살균법에 의한 탁주의 보존성 증진)

  • 배상면;김헌진;고영희;오태광
    • Microbiology and Biotechnology Letters
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    • v.18 no.3
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    • pp.322-325
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    • 1990
  • During transportation and preservation of Takju, alcohol fermentation has continued to produce $C0_2$ from residual sugar and frequently spoiled owing to bacterial contaminants wich produce organic acids. The authors could preserve Takju for more than 50 days at room temperature by pasteurization without any changes of quality. For the optimal condition of pasteurization, fresh Takju was heated at various temperatures and times. D-Value of the Saccharomyces sp. which isolated from Takju collected at seoul area was 19 see at $55^{\circ}C$. Non-spore forming bacterial contaminants, most of which known to cause acid-spoilage, were decreased when heated at $55^{\circ}C$ for 5 min. The optimal pasteurization condition of Takju was at $55^{\circ}C$ for 10 min. Spore forming bacterial contaminants, considered to be EuciiLw sp., were not sterilized after pasteurized at the optimal condition. However, the spore-forming bacteria could not increase any more and also not cause increment of acidity during preservation even at room temperature for 50 days. Reducing sugar was increased during storage of Takju after pasteurization. This suggests that the residual glucoamylase in Takju is still active after pasteurizsation and keep sweet taste.

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Effects of Phytic Acid Content, Storage Time and Temperature on Lipid Peroxidation in Muscle Foods (근육식품에서 지방산화에 대한 피틴산, 저장기간 및 온도의 영향)

  • 이범준;김영철;조명행
    • Journal of Food Hygiene and Safety
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    • v.14 no.1
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    • pp.27-33
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    • 1999
  • Phytic acid, making up 1~5% of the composition of many plant seeds and cereals, is known to form iron-chelates and inhibit lipid peroxidation. Thiobarbituric acid reactive substances (TBARS), as an indication of lipid peroxidation, were measured in beef round, chicken breast, pork loin, and halibut muscle after the meats were stored for 0, 1, 3, 5, and 7 days at various temperatures [frozen (~2$0^{\circ}C$), refrigerator (4$^{\circ}C$), and room temperature ($25^{\circ}C$)]. Phytic acid effectively inhibited lipid peroxidation in beef round, chicken breast, halibut, and pork loin muscle (p<0.05). The inhibitory effect of phytic acid was dependent on concentration, storage time, and temperature. At frozen temperature, the inhibitory effect of phytic acid was minimal, whereas at room temperature, the inhibitory effect of phytic acid was maximal, probably due to the variation of the control TBARS values. At the concentration of 10 mM, phytic acid completely inhibited lipid peroxidation in all the muscle foods by maintaining TBARS values close to the level of the controls, regardless of storage time or temperature (p<0.05). The rate of lipid peroxidation was the highest in beef round muscle, although they had a close TBARS value at 0 day. Addition of phytic acid to lipid-containing foods such as meats, fish meal pastes, and canned seafoods may prevent lipid peroxidation, resulting in improvement of the sensory quality of many foods and prolonged shelf-life.

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Fabrication of excimer laser annealed poly-si thin film transistor by using an elevated temperature ion shower doping

  • Park, Seung-Chul;Jeon, Duk-Young
    • Electrical & Electronic Materials
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    • v.11 no.11
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    • pp.22-27
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    • 1998
  • We have investigated the effect of an ion shower doping of the laser annealed poly-Si films at an elevated substrate temperatures. The substrate temperature was varied from room temperature to 300$^{\circ}C$ when the poly-Si film was doped with phosphorus by a non-mass-separated ion shower. Optical, structural, and electrical characterizations have been performed in order to study the effect of the ion showering doping. The sheet resistance of the doped poly-Si films was decreased from7${\times}$106 $\Omega$/$\square$ to 700 $\Omega$/$\square$ when the substrate temperature was increased from room temperature to 300$^{\circ}C$. This low sheet resistance is due to the fact that the doped film doesn't become amorphous but remains in the polycrystalline phase. The mildly elevated substrate temperature appears to reduce ion damages incurred in poly-Si films during ion-shower doping. Using the ion-shower doping at 250$^{\circ}C$, the field effect mobility of 120 $\textrm{cm}^2$/(v$.$s) has been obtained for the n-channel poly-Si TFTs.

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Wear and Oxidation Charateristics of Two Phase Intermetallic Compounds (다상 금속간 화합물의 내마모 및 내산화 특성)

  • Lee, Jong-Hun;Bae, Jong-Uk;Lee, Sang-Yul
    • 연구논문집
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    • s.28
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    • pp.183-192
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    • 1998
  • The wear and oxidation resistance of two phase nickel aluminides was investigated. Wear tests of various heat-treated specimens at room temperature and at $500^{\circ}C$ were performed under no lubricant condition in air by using a ball-on-disk type tribotester. Isothermal oxidation tests were made at $1100^{\circ}C$ in air flowing at the rate of 70cc/min and at $1000^{\circ}C$ in air by using TGA. Experimental results from wear tests showed that nickel aluminide with a higher content of Al had an improved wear resistance at both temperatures. Also the examination of the wear tracks after wear test at both room temperature and $500^{\circ}C$ indicated that regardless of the alloy compositions the wear tracks of the two phase nickel aluminides showed an abrasive type wear The improved oxidation resistance observed in the Ni-34at%Al alloy could to be attributed to the microstructural difference between the aluminides. An accelerated oxidation along the thin layer of $Ni_3AL$ along the grain boundary observed in the microstructure of the Ni-32at%Al aluminide could be attributed to the poor oxidation resistance.

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