• Title/Summary/Keyword: Retention loss

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Pigment Stability of Lavers Porhyra tenera Kjellman during Processing and Storage (김의 가공 저장중에 있어서의 색소의 안정도)

  • LEE Kang-Ho
    • Korean Journal of Fisheries and Aquatic Sciences
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    • v.2 no.2
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    • pp.105-133
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    • 1969
  • The stability of three major pigments in lavers, namely chlorophylls, carotenoids, and phy-cobilins, during processing and storage was studied. The results of the pigment retention in fresh lavers during storage at low temperatures, of heat lability during heat treatment, and of the pigment loss during storage are summarized as follows: 1. The contents of chlorophyll a, xanthophyll (lutein+zeaxanthin), and carotene ($\alpha-+\beta-carotene$) averaged 1,525, 627, and $409{\mu}g/g$ of dry samples respectively The comparative composition of four carotenoids, lutein, $\beta-carotene$, zeaxanthin, and $\alpha-carotene$, was 35.9, 33.7, 12.2, and $5.8\%$ respectively. 2. In storage of fresh lavers at room ternperature ($20-25^{\circ}C$), 2 to $5^{\circ}C$, and $-15^{\circ}C$, the pigments generally were retained more at 2 to $5^{\circ}C$ than others while carotene only showed more retention at $-15^{\circ}C$ than at 2 to $5^{\circ}C$. Phycocyanin tended to decrease more rapidly than phyco-erythrin at low temperatures. 3. In regard to heat treatment of both dried and wet materials at 40, 60, 80, $100^{\circ}C$ respectively, the pigments were more stable at lower temperatures than at higher temperatures in both cases of materials. Carotenoids were retained more in wet materials than in the sun dried. Xanthophylls showed higher heat stability than carotenes. Phycoerythrin was considered more heat labile than phycocyanin, particularly at higher temperatures. 4. In storage of heat treated lavers for 50 days at room temperature, the retention of pigments appeared differently in accordance with the temperatures of treatment The materials treated at $60^{\circ}C$ showed better relention of pigments than those treated at the other temperatures. Degradation rate of xanthopllylls, carotenes, and phycobilins was decreased in the materials treated at higher temperatures, showing a tendency of great pigment retention even for a long period storage. Chlorophyll il was retained more in sun dried materials whereas xanthophyll and carotene were retained more in the wet. 5. In order to maintain a higher pigment stability during storage, the materials must be treated at $60^{\circ}C$ in a dryer with rapid ventilation until the moisture level reaches about $6.0\%$. In case of treatment at a higher temperature than $60^{\circ}C$, they must be treated for a short period of time to minimize pigment degradation by heat. 6. The lavers treated with the solutions of pH around 7.8 showed a higher retention of chlorophyll a. When treated with the solutions of algal extracts such as agar and alginic acid, uniform layer of laver sheets and better surface gloss of dried layers were obtained.

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Effect of High Calcium Diet on the Zinc and Copper Balance in Korean Female Adolescents (청소년기 여자에서 고칼슘 섭취가 아연과 구리 평형에 미치는 영향)

  • 최보영;남혜경;황용주;김선희
    • Journal of the Korean Society of Food Science and Nutrition
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    • v.30 no.5
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    • pp.894-899
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    • 2001
  • Intakes and excretions of zinc and copper were determined for 8 female adolescents (aged 16.4$\pm$0.5 y; body mass index 20.4$\pm$1.3kg/$m^2$; body fat 33.3$\pm$2.5%; bone mineral density of lumbar spine in L2-L4; 0.96$\pm$0.08g/$\textrm{cm}^2$) when they consumed diets basal and high in calcium for 6 days each. All subjects consumed a basal Ca diet containing 800 mg, Korean RDA level of the subjects, and a high Ca diet containing 1200mg, RDA plus 2 SDs of calcium intake. The diets provided 58% of energy intake as carbohydrate, 25% as fat, and 17% as protein. Food, urine and fecal samples were collected during the last 3 days of each feeding period and were assayed. Mean daily intakes on the basal and high calcium diets, respectively, were 6.57 and 6.37 mg for zinc and 910 and 812 $\mu\textrm{g}$for copper. Fecal excretion of copper and zinc in relation to intake was significantly greater on the high calcium than on the basal calcium diet. Hence, apparent absorption rate was significantly lowered from 98.7% on the basal calcium diet to 97.9% on the high calcium diet for zinc from 66.3% to 56.4% for copper, respectively. Urinary loss of copper was not detectable but that of zinc was 0.38mg on the basal diet and 0.47mg on the high calcium diet. Copper retention was 899$\pm$105$\mu\textrm{g}$/day on the basal calcium diet and 792$\pm$20.8$\mu\textrm{g}$/day on the high calcium diet, and zinc retention was 3.95$\pm$0.91mg/day and 3.11$\pm$0.89mg/day. Thus, copper and zinc retention was significantly decreased on the high calcium diet (p<0.05). Summarizing the results, apparent absorption and retention of zinc and copper were significantly decreased by calcium supplementation. Therefore, it is suggested that interactions among minerals should be considered in determining RDA.

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A study on Calcination Characteristics of Powdered Oyster Shell (굴패각 재활용 방안에 관한 기초연구 -굴패각 소성가공특성-)

  • Kim, Jong-Oh;Lee, Sang Eun;Lee, Chang-Ho
    • Journal of the Korea Organic Resources Recycling Association
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    • v.15 no.1
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    • pp.143-148
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    • 2007
  • The objective of this study was to investigate the proper conditions of calcination and calcium extraction from powdered oyster shell. The physical characteristics such as particle size distribution, surface morphology, and thermal gravity were examined. The following result were obtained. As the powdered oyster shell was ignited in high temperature of $650^{\circ}C$ to $950^{\circ}C$, the calcination reactions was effectively progressed. The amount of weight loss during calcination would be matched with the generation of carbon dioxide gas. In the calcination of powdered oyster shell, the amount of weight loss increased according to the increased of calcination temperature and the decrease of mean particle size. It was founded that the proper temperature and retention time of calcination was $850^{\circ}C$ and 40 minute. In the extraction of calcium into liquid form using acid addition, the calcination oyster shell was more effective than the non-calcinated shell. The liquid calcium extraction technique using the calcinated oyster shell needed more researches considering cost evaluation.

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Effect of Chlorine Dioxide on Freshness of 'Maehyang' Strawberries during Export

  • Kim, Hye Min;Hwang, Seung Jae
    • Horticultural Science & Technology
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    • v.34 no.4
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    • pp.626-633
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    • 2016
  • The objective of this study was to assess the effect of precooling and application of gaseous $ClO_2$ on the retention of freshness and quality of 'Maehyang' strawberry fruits intended for export. 'Maehyang' strawberry fruits (Fragaria ${\times}$ ananassa Duch.) were grown in commercial greenhouses and then harvested. Fruits of uniform and medium size at 60% ripeness were selected and assigned to one of four treatment groups: non-treatment (control), precooling only (PO), gaseous $ClO_2$ only (GCO) or precooling combined with gaseous $ClO_2$ (P + C). Weight loss was lowest in the PO treatment and greatest in the GCO treatment after export. Compared to the control and PO treatment groups, strawberry fruits in the GCO treatment group maintained high brightness and high chroma. Six days after shipping, fruits in the P + C treatment group had the highest soluble solids content, even as high as $10.05^{\circ}Brix$; the lowest value was observed in the PO treatment. The incidence rate of gray mold in strawberry fruits was 20% and 17% in the control and the PO treatment, respectively; in the GCO treatment, the incidence rate of gray mold amounted to 10%. No gray mold was observed in the P + C treatment group. These results indicate that gaseous $ClO_2$ treatment combined with precooling (P + C) was effective in maintaining the freshness of 'Maehyang' strawberry fruits intended for export from South Korea to Hong Kong.

WATER ACTIVITY AND PIGMENT DEGRADATION IN DRIED LAVERS STORED AT ROOM TEMPERATURE (건해태(김) 저장시의 수분활성과 색소분해반응)

  • LEE Kang-Ho;CHOI Ho-Yeon
    • Korean Journal of Fisheries and Aquatic Sciences
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    • v.6 no.1_2
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    • pp.27-36
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    • 1973
  • The effect of water activity on degradation of pigments in dried lavers, Porphyra tenera Kjellm. was examined when stored at room temperature for fifty days. Chlorophyll pigment was extracted with methanol-petroleum ether mixture solvent(2:1 v/v), partitioned in ether, and analysed spectrophotometrically at 662 nm as chlorophyll a. The degradation products of chlorophyll were isolated on sugar-starch column(85:15 w/w) with n-propanol-petroleum ether solution(1:200 v/v) as a developing solvent. The isolated green colored zones were analysed individually at the wavelengths of 650, 662, and 667 nm as allomerized product, chlorophyll a retained, and pheophytin formed respectively. Carotenoida were also extracted with the methanol mixture solvent, partitioned in ether, and finally redissolved in acetone after the evaporation of ether in a rotary vacuum evaporator. The total carotenoid content was measured as lutein at 450 nm. From the results, it is noted that the rate of chlorophyll degradation reached a minimum at 0.11 to 0.33 water activity while progressively increased at higher moisture levels resulting in rapid conversion of chlorophyll to pheophytin. At lower activity, autocatalysed oxidizing reaction like allomerization seemed prevailing the acid catalysed conversion reaction. The loss of carotenoid pigment was also greatly reduced at the range of 0.22 to 0.34 water activity with much faster oxidative degradation at both higher and extremely lower moisture levels. These two moisture levels indicated above at which the both pigments exhibited maximum stability are considerably higher than the BET monolayer moisture which appeared 7.91 percent on dry basis at Aw=0.10 calculated from the adsorption isothermal data of the sample at $20^{\circ}C$. The rate of pigment loss in heat treated samples at 60 and $100^{\circ}C$ for 2 hours prior to storage somewhat decreased, particularly at higher moisture levels although the final pigment retention was not much stabilized.

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Mechanical Properties of Mortar Containing Bio-Char From Pyrolysis (바이오숯을 함유한 모르타르의 역학적 특성)

  • Choi, Won Chang;Yun, Hyun Do;Lee, Jae Yeon
    • Journal of the Korea institute for structural maintenance and inspection
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    • v.16 no.3
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    • pp.67-74
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    • 2012
  • Bio-char, obtained from biomass as a by-product of the pyrolysis process, is used successfully as a soil amendment and carbon sequester in this limited study. Recent and active research from literatures has extended the application of bio-char in the industry to promote sustainability and help mitigate the negative environmental impacts caused by carbon emissions. This study aims to investigate the feasibility of high-carbon bio-char as a carbon sequester and/or admixture in mortar and concrete to improve the sustainability of concrete. This paper presents the experimental results of an initial attempt to develop a cement admixture using bio-char. In particular, the effects of the water retention capacity of bio-char in concrete are investigated. The chemical and mechanical properties (e.g., the chemical components, microstructure, concrete weight loss, compressive strength and mortar flow) are examined using sample mortar mixes with varying replacement rates of cement that contains hardwood bio-char. The experimental results also are compared with mortar mixes that contain fly ash as the cement substitute.

Complication incidence of two implant systems up to six years: a comparison between internal and external connection implants

  • Chae, Sung-Wook;Kim, Young-Sung;Lee, Yong-Moo;Kim, Won-Kyung;Lee, Young-Kyoo;Kim, Su-Hwan
    • Journal of Periodontal and Implant Science
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    • v.45 no.1
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    • pp.23-29
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    • 2015
  • Purpose: This study was conducted to compare the cumulative survival rates (CSRs) and the incidence of postloading complications (PLCs) between a bone-level internal connection system (ICS-BL) and an external connection system (ECS). Methods: The medical records of patients treated with either a ICS-BL or ECS between 2007 and 2010 at Asan Medical Center were reviewed. PLCs were divided into two categories: biological and technical. Biological complications included >4 mm of probing pocket depth, thread exposure in radiographs, and soft tissue complications, whereas technical complications included chipping of the veneering material, fracture of the implant, fracture of the crown, loosening or fracture of the abutment or screw, loss of retention, and loss of access hole filling material. CSRs were determined by a life-table analysis and compared using the log-rank chi-square test. The incidence of PLC was compared with the Pearson chi-squared test. Results: A total of 2,651 implants in 1,074 patients (1,167 ICS-BLs in 551 patients and 1,484 ECSs in 523 patients) were analyzed. The average observation periods were 3.4 years for the ICS-BLs and 3.1 years for the ECSs. The six-year CSR of all implants was 96.1% (94.9% for the ICS-BLs and 97.1% for the ECSs, P=0.619). Soft tissue complications were more frequent with the ECSs (P=0.005) and loosening or fracture of the abutment or screw occurred more frequently with the ICS-BLs (P<0.001). Conclusions: Within the limitations of this study, the ICS-BL was more prone to technical complications while the ECS was more vulnerable to biological complications.

A Case Report of RED II Distraction Osteogenesis and Early Rigid Fixation by Minimal Invasive Approach Le Fort III Osteotomy in Crouzon's Disease (크루존씨 병에서 최소침습 절개법 Le Fort III 절골술을 통한 RED II 골 신연술 후 조기 고정 1례)

  • Kim, Young Seok;Lee Linton, Jina;Park, Beyoung Yun
    • Archives of Plastic Surgery
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    • v.34 no.1
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    • pp.123-127
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    • 2007
  • Purpose: Rigid external distraction(RED) is a highly effective technique for correction of maxillary hypoplasia in patients with cleft or syndromic craniosynostosis. Despite many advantages of RED, it also has the problem of relapse as the conventional advancement surgery. Bicoronal approach, that is the common approach to gain access to the craniofacial skeleton, had some morbidity, such as hair loss, sensory loss, wide scar and temporal hollowing. We present our clinical experience of RED distraction with minimal invasive approach and early rigid fixation to overcome these disadvantages. Methods: A 27-year-old female patient with Crouzon's disease underwent Le Fort III osteotomy and RED device application through the minimal invasive direct skin incisions. After the latent period of 5 days, distraction was undertaken until proper convexity and advancement were obtained. During the rigid retention period, inflammation occurred on the right cheek, and proper conservative managements were done including continuous irrigation. To maintain the stability of distraction, early rigid fixation was undertaken on the osteotomy sites through another skin incisions. Preoperative and postoperative orthodontic treatments were performed. Serial photographs and cephalometric radiographs were obtained preoperatively, after distraction and 6 months after distraction. Results: The cephalometric analysis demonstrated postoperatively significant advancement of the maxilla and improvement of facial convexity. After 6-month follow-up period, the maxilla was stable in the sagittal plane and no relapse was found. Facial scars were not noticeable and other deformity and morbidity did not occur. Conclusion: This effective and stable technique will be a good alternative for the patients who need large amount of distraction and for adult patients with severe maxillary hypoplasia or syndromic craniosynostosis.

The influence of ultrasound and adenosine 5'-monophosphate marination on tenderness and structure of myofibrillar proteins of beef

  • Zou, Ye;Yang, Heng;Zhang, Muhan;Zhang, Xinxiao;Xu, Weimin;Wang, Daoying
    • Asian-Australasian Journal of Animal Sciences
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    • v.32 no.10
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    • pp.1611-1620
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    • 2019
  • Objective: The aim was to investigate the influence of ultrasound and adenosine 5'-monophosphate (AMP) marination (UAMP) on tenderness and structure of myofibrillar proteins of beef. Methods: Five groups, the untreated meat (Control), deionized water marination (DW), ultrasound followed by DW (UDW), AMP marination (AMP), and ultrasound followed by AMP (UAMP) were studied. Myofibrillar fragmentation, cooking loss, shear force, thermograms, histological observation of meats and myofibrillar proteins properties were investigated in these different treatments. Results: The results showed that UAMP significantly increased myofibrillar fragmentation index from 152 (Control), 231 (AMP), and 307 (UDW) to 355 (p<0.05), respectively. The lowest cooking loss, shear force and peak denaturation temperature were observed in UAMP. In histological observation, UDW and UAMP had more fragmented muscular bundles than the others. Furthermore, a drastic increase in ${\alpha}$-helix and decrease in ${\beta}$-sheet of myofibrillar proteins was observed in UAMP, implying the disaggregation of protein samples. The synchronous fluorescence spectra of myofibrillar proteins in UAMP suggested the combination of ultrasound and AMP could accelerate the unfolding molecular structure and destroying hydrophobic interactions. The results of circular dichroism and synchronous fluorescence spectra for myofibrillar proteins coincided with the microstructures of beef. Conclusion: The results indicate that ultrasound combined with AMP improved meat tenderness not only by disruption in muscle integrity, increasing water retention, but also altering their spatial structure of myofibrillar proteins.

Washing Treatment Effects on Cotton and Kenaf Blend Fabrics (면섬유와 케나프섬유를 혼방한 직물과 편성물에 대한 워싱 처리 효과)

  • Lee, Hye-Ja;Yoo, Hye-Ja;Lim, Hee-Jeong
    • Journal of the Korean Society of Clothing and Textiles
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    • v.34 no.3
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    • pp.448-458
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    • 2010
  • Kenaf has a rigid and rough touch that inhibits the use of it as a textile material; therefore, this study developed a novel textile material using kenaf. Kenaf and cotton were blended in the ratio of 3:7 and manufactured as 20' spun yarn that was compared to 20's spun yarn made of 100% cotton. Both kenaf/cotton-blended and 100% cotton spun yarn were constructed as plain woven and knitted fabrics. Four kinds of fabrics were prepared as follows. Plain kenaf/cotton-woven fabrics, plain cotton-woven fabrics, kenaf/cotton jersey, and cotton jersey. A cellulase washing process was carried out to reduce the character of kenaf/cotton-blended fabrics, rigid, and rough touch. All fabrics were pretreated with NaOH. NaOH at the concentrations of 0, 0.25, 1.25, and 2.25mol/L, and cellulase at concentrations of 0, 1, 3 and 5g/L were used since the pretreatment of NaOH has a higher efficiency of weight loss than $Na_2CO_3,\;K2CO_3$ and Triton X-100. The ratio of weight loss, tensile strength, stiffness, drape property, and surface appearance were measured in order to evaluate the efficiency of the washing treatment on fabrics. Kenaf/cotton-blended fabrics exhibited more rigid and rough features than cotton fabrics. A cotton jersey showed significant differences in the degree of stiffness and drape properties. When all fabrics were treated with 1.25mol/L of NaOH and 3g/L of cellulase, kenaf/cotton-blended fabrics showed a higher retention ratio of tensile strength than cotton fabrics after washing despite the increased weight l08s of kenaf-blended fabrics compared to cotton fabrics. The ratio of weight loss for all fabrics was well correlated with flexibility. The washing treatment process made woven fabrics more flexible than knitted fabrics, because the stiffness of woven fabrics made the rubbing actions stronger. Kenaf/cotton-blended fabrics showed a significantly higher ratio of weight loss and more reduction in stiffness than cotton fabrics after the washing treatment. This might be due to the lack of cohesiveness and easy elimination from fabrics. The drape property of kenaf-blended fabrics was superior to cotton fabrics.