• Title/Summary/Keyword: Reinforced particles

Search Result 236, Processing Time 0.025 seconds

FRACTURE TOUGHNESS OF VARIOUS CORE MATERIALS

  • Lee Shin-Won;Lee Sun-Hyung;Yang Jae-Ho;Han Jung-Suk;Lee Jai-Bong
    • The Journal of Korean Academy of Prosthodontics
    • /
    • v.39 no.6
    • /
    • pp.682-697
    • /
    • 2001
  • This investigation evaluated the fracture toughness($K_{IC}$) of eight currently available core materials, and relate the fracture toughness value to fractography analysis and surface characteristics using a atomic force microscope (AFM). Single-edge notched (SEN) test specimens (n=10) and compact tension (CT) test specimens (n=10) were prepared conforming to the ASTM Standard E-399 for a high copper amalgam, three composite core materials (Core-Max II, Core Paste, Bisfil Core), two reinforced composite core materials (Ti-Core, Ti-Core Natural), a resin-modified glass ionomer core material (Vitremer), and a conventional glass ionomer core material (Ketac-Molar). The specimens were tested with an Instron Universal Testing Machine. The maximum loads were measured to calculate the fracture toughness ($K_{IC}$). Thereafter, fracture surfaces of SEN specimens of each material were investigated for fractography analysis using scanning electron microscope. And, disc-shaped specimens with 1mm thickness were fabricated for each material and were investigated under AFM for surface morphology analysis. The results were as follows: 1. Bisfil Core showed the highest mean fracture toughness regardless of test methods. 2. For the tooth-colored materials, Ti-Core Natural exhibited the highest fracture toughness. 3. Ketac Molar showed a significantly low fracture toughness when compared with the amalgam and the composite resin core materials(p<0.05). 4. The fracture toughness values obtained with the single-edge notched test, except Ketac Molar, were higher than those obtained in the compact tension test. 5. SEM revealed that the fracture surface of high fracture toughness material was rougher than that of low fracture toughness material. 6. AFM revealed that the surface particles of the composite resins were smaller in size, with a lower surface roughness than the glass ionomer core materials.

  • PDF

Fabrication and Characterization of Composite Sealants for Low Temperature (600∼650°C)SOFCs (저온작동 (600∼650°C) SOFC용 복합밀봉재 제조 및 평가)

  • Lim, Hyun-Yub;Kim, Hyoung-Chul;Choi, Sun-Hee;Kim, Hae-Ryoung;Son, Ji-Won;Lee, Hae-Weon;Lee, Jong-Ho
    • Journal of the Korean Ceramic Society
    • /
    • v.45 no.12
    • /
    • pp.802-806
    • /
    • 2008
  • A proper sealant for low temperature SOFCs should show zero or low leak rates to avoid direct mixing of the fuel and oxidant gases or leakage of fuel gas during the operation of SOFCs. Furthermore, it should be chemically and/or mechanically stable in both oxidizing and reducing environments and chemically compatible with other fuel cell components. In the present work, we developed a novel compressed seal gasket of glass-based composite reinforced with ceramic particulate particles, which can efficiently control the viscous flow of glass matrix as well as the crystallization of glass phase. This novel sealing gasket showed excellent gas tightness under very low compressive load which would be suitable for the operation of SOFCs in the temperature range $600{\sim}650^{\circ}C$.

Prediction Method of Dispersion Condition for Reinforced Epoxy in Nano SiC Particles Using Capacitance Measurement (Capacitance 측정법을 이용한 나노 SiC 에폭시 복합재료의 내부 강화재 분산 예측방법)

  • Kwon, Dong-Jun;Wang, Zuo-Jia;Kim, Je-Jun;Jang, Key-Wook;Park, Joung-Man
    • Composites Research
    • /
    • v.26 no.6
    • /
    • pp.337-342
    • /
    • 2013
  • The good dispersion of nano-materials in epoxy matrix was important parameter for the reinforcement effect, and the evaluation of dispersion degree was to prove it. This work was studied to predict the dispersion condition of nano-SiC powders in SiC/epoxy composites using capacitance measurement. Capacitance was defined to be the electric capacity in proportional to electron charge of the measuring section. In case of nano-SiC powders, the electron charge of SiC/epoxy composites was higher than that of neat epoxy resin. Capacitance was evaluated for each section of SiC/epoxy composites. The prediction of dispersion condition was verified by using capacitance measurement. Dispersion condition of nano-SiC powders in epoxy matrix was evaluated with two different dispersion methods, i.e., sonication and stirring methods. The dispersion degree was also verified with the tensile strength correlating to capacitance.

Microstructure and Wear Property of $Al-5Mg-X(Si,Cu,Ti)/SiC_p$ Composites Fabricated by Pressureless Infiltration Method (무가압 침투법에 의해 제조된 $Al-5Mg-X(Si,Cu,Ti)/SiC_p$ 복합재료의 조직 및 마멸특성)

  • Woo, Kee-Do;Kim, Sug-Won;Ahn, Haeng-Keun;Jeong, Jin-Ho
    • Journal of Korea Foundry Society
    • /
    • v.20 no.4
    • /
    • pp.254-259
    • /
    • 2000
  • Metal matrix composites(MMCs) reinforced with hard particles have many potential application in aerospace structures, auto parts, semiconductor package, heat resistant panels, wear resistant materials and so on. In this work, the effect of SiC partioel sizes(50 and 100 ${\mu}m$) and additional elements such as Si, Cu and Ti on the microstructure and the wear property of $Al-5Mg-X(Si,Cu,Ti)/SiC_p$ composites produced by pressureless infiltration method have been investigated using optical microscopy, scanning eletron microcopy(SEM) with EDS(energy dispersive spectrometry), hardness test, X-ray diffractometer(XRD) and wear test. In present study, the sound $Al-5Mg-X(Si,Cu,Ti)/SiC_p$(50 and 100 ${\mu}m$) composites were fabricated by pressureless infiltration method. The $Al-5Mg-0.3Si-O.1Cu-O.1Ti/SiC_p$ composite with $50 {\mu}m$ size of SiC particle has higher hardness and better wear property than any other composite with $100{\mu}m$ size of SiC particle produced by pressureless infiltration method. The hardness and wear property of $Al-5Mg/SiC_p$(50 and 100 ${\mu}m$) composites were enhanced by the addition of Si, Cu and Ti in Al-5%Mg matrix alloy.

  • PDF

Experimental Assessment of Mechanical Properties of Geo-grid Reinforced Material and Long-Term Performance of GT/HDPE Composite

  • Seo, Jung-Min;Min, Kyung-Ho;Hwang, Beong-Bok;Lee, In-Chul;Ruchiranga, Jayasekara Vishara;Jeon, Han-Yong;Jang, Dong-Hwan;Lim, Joong-Yeon
    • Advanced Composite Materials
    • /
    • v.17 no.3
    • /
    • pp.247-258
    • /
    • 2008
  • This paper is concerned with the long-term performance of geo-textile (GT) composites in terms of creep deformation and frictional properties. Composites of PVA GT and HDPE GM were made to investigate the advanced properties of long-term performance related to waste landfill applications. The same experiments were also performed for typical polypropylene and polyester GT and compared to PVA GT/HDPE GM composites. We also develop high performance GT composites with GM by using PVA GT, which is capable of improving the frictional properties and thus enhances long-term performance of GT composites. Experimental study reveals that the friction coefficient of GT composites is relatively large compared with those of polyester and polypropylene non-woven GT as long as the friction media has similar size to the particles of domestic standard earth. In addition, the geo-composites bonded with geo-grid by a chemical process were investigated experimentally in terms of strain evaluation and creep response values. Geo-grid plays an important role as a reinforcing material. Three kinds of geo-grid were prepared as strong yarn polyester and they were woven type, non-woven type, and wrap knitted type. The sample geo-grids were then coated with PVC. The rib tensile strength tests were conducted to evaluate geo-grid products in terms of tensile strength with regard to single rib. The test was performed according to GRI-GGI. It was concluded again from the experiments that the tensile and creep strains of the geo-grid showed such stable values that the geo-grid prepared in this study could protect geo-textile partially in practical structures.

Evaluation of Adhesion Property of Epoxy Adhesive with Different Surface Roughness of GFRC (유리섬유강화 복합재료의 표면거칠기에 따른 에폭시 접착제의 접착강도 평가)

  • Kim, Jong-Hyun;Shin, Pyeong-Su;Lee, Sang-Il;Park, Joung-Man
    • Journal of Adhesion and Interface
    • /
    • v.21 no.1
    • /
    • pp.27-33
    • /
    • 2020
  • Adhesion property of epoxy adhesive was evaluated with different surface roughness of glass fiber reinforced composite (GFRC) and optimized condition of surface roughness was confirmed. Different sizes of alumina (Al2O3) particles were blasted to GFRC to control surface roughness of GFRC using sand blasting method. The surface roughness was measured and quantified via surface roughness tester. Contact angle was measured using four types of different solvents. Surface energies and work of adhesion between epoxy adhesive and GFRCs were calculated with different surface roughness of GFRC. Adhesion property between epoxy adhesive and GFRCs was evaluated using single lap shear test and adhesion property increased with surface roughness of GFRC. The fracture surface of GFRCs was observed to evaluate adhesion property. Finally, the optimized roughness condition of GFRCs was confirmed.

The Study on the Assesment Greenhouse Gases and Air Pollutants of Diesel Vehicle according to Ambient Temperature and Driving Condition (대기온도와 운전조건에 따른 디젤자동차의 차량 온실가스 및 대기오염물질 배출특성에 관한 연구)

  • Kim, Ki-Ho;Kim, Sung-Woo;Lee, Min-Ho;Oh, Sang-Gi;Lee, Seung-Ho
    • Journal of Power System Engineering
    • /
    • v.18 no.6
    • /
    • pp.77-83
    • /
    • 2014
  • As the interest on the air pollution is gradually risen up at home and abroad, their vehicle emission regulations have been reinforcing by steps. PM regulation was also reinforced 4times for the last 13years and has been applied to SI vehicles after EURO 5. Additionally, knowing that small particles of PM can easily penetrate deep into lungs PM number was added on the regulation from EURO5+ and is applied to CI vehicles. Also, PN regulation is going to be applied to SI vehicles. But, because the regulation is appled to only a general test mode of each countries that is performed at $25{\pm}5^{\circ}C$, it is unclear whether the regulation can work on the other ambient temperature conditions or not. In this paper, to know that exhaust emission characteristics at the special conditions CI vehicles(CRDi w, w/o DPF) were tested using 5-cycle mode, NEDC mode at 5-ambient temperatures (35, 25, 0, -7 and -15) and the exhaust emission test results were discussed. The results show that the vehicle with DPF emits much low PM(and PM number) on all of the test mode. However, NOx of the other mode was emitted higher than regulation mode. Also. NOx was sharply increased according to decreasing Ambient Temperature.

Effects of Interface Boundary Strength on Wear and Wear Transition during Sliding in Silicon Carbide Ceramics (탄화규소계 세라믹스에서 미끄럼시의 마모 및 마모천이에 미치는 계면강도의 영향)

  • Kim, Dong-Jin;Park, Seong-Khil;Ryu, Hyun;Um, Chang-Do;Cho, Seong-Jai;Kim, Seock-Sam
    • Tribology and Lubricants
    • /
    • v.11 no.4
    • /
    • pp.21-27
    • /
    • 1995
  • The effects of interface boundary strength on wear and wear transition during sliding have been investigated in silicon carbide ceramics. Three different microstructures, i.e., solid state sintered silicon carbide, liquid phase sintered silicon carbide and liquid phase sintered silicon carbide composite reinforced with TiB$_{2}$ particulates, were designed by hot pressing. Examinations of crack patterns and fracture modes indicated that interface boundaries were relatively strong between silicon carbide grains in the solid state sintered silicon carbide, intermediate in the liquid phase sintered silicon carbide and weak between silicon carbide grains and TiB$_{2}$ particles in the composite. Wear data and examinations of worn surfaces revealed that the wear behavior of these silicon carbide ceramics could be significantly affected by the interface strength. In the solid state sintered silicon carbide, the wear occurred by a grooving process. In the liquid phase sintered silicon carbide and composite, on the other hand, an abrupt transition in wear mechanism from initial grooving to grain pull-out process occurred during the test. The transition occurred significantly earlier in the composite than in the carbide.

Electrical and Mechanical Properties of Carbon Particle Reinforced Rubber for Electro-Active Polymer Electrode (전기활성 고분자 전극용 탄소입자 강화고무의 전기적 및 기계적 특성)

  • Lee, Jun Man;Ryu, Sang Ryeoul;Lee, Dong Joo
    • Transactions of the Korean Society of Mechanical Engineers A
    • /
    • v.37 no.12
    • /
    • pp.1465-1471
    • /
    • 2013
  • The electrical and mechanical properties of room temperature vulcanized (RTV) silicone rubber composites are investigated as functions of multi-walled carbon nanotube (CNT), carbon black (CB), and thinner content. The thinner is used to improve the CNT and CB dispersion in the matrix. The electrical and mechanical properties of the composite with CNT are improved when compared to the composite with CB at the same content. As the thinner content is 80 phr, the electric resistance of the composite decreases significantly with the CNT content and shows contact point saturation of CNT at 2.5 phr. As the thinner content increases, the dispersion of conductive particles improves; however, the critical CB content increases because of the reduction in the CB weight ratio. It is believed that an electrode that needs good flexibility and excellent electrical properties can be manufactured when the amount of CNT and CB are increased with the thinner content.

Study on the Microstructure and Mechanical Properties of High Volume Fraction TiB2-Al1050 Metal Matrix Composites (고체적률 TiB2-Al1050 금속복합재료의 미세조직 및 기계적 특성 연구)

  • Ko, Seongmin;Park, Hyeonjae;Lee, Yeong-Hwan;Shin, Sangmin;Lee, Donghyun;Jo, Ilguk;Lee, Sang-Bok;Lee, Sang-Kwan;Cho, Seungchan
    • Composites Research
    • /
    • v.32 no.1
    • /
    • pp.1-5
    • /
    • 2019
  • In this study, Al1050 composites reinforced with uniformly dispersed, high volume fraction $TiB_2$ particles were fabricated by liquid pressing process and analyzed to microstructure, mechanical properties. Hardness, ultimate tensile strength and compressive yield strength of the 56 vol.% $TiB_2$-Al1050 composite increased to 10, 4.5 and 9.8 times, respectively, compared with those of the Al1050 due to dispersion hardening effect of uniformly dispersed $TiB_2$ in the Al matrix.